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#\#CIF_1.0 ################################################################################ # # # This CIF is a part of the B-IncStrDB # # (Bilbao Incommensurate Structures Database) # # http://www.cryst.ehu.eus/bincstrdb/ # # # # Please note that the structure of the CIF file may differ from the one # # deposited, as it may have been modified to comply with the standard. The # # file has been validated against official dictionaries as well as local # # dictionaries including non-standard data names used by SHELXL (Sheldrick, # # G. M. (2008). Acta Cryst. A 64, 112-122) and JANA (Petricek, V., Dusek, M. # # and Palatinus, L. (2014), Z. Kristallogr. 229, 345-352). # # # # For comments and/or criticisms, please e-mail to administrador-bcs@ehu.es # # # ################################################################################ data_global _journal_name_full 'IUCrJ' _journal_year 2025 _journal_volume 12 _journal_issue 6 _journal_page_first 670 _journal_page_last 682 _journal_paper_doi https://doi.org/10.1107/S2052252525007547 _publ_contact_author_name 'Weil, Matthias' _publ_contact_author_address ;Institute for Chemical Technologies and Analytics Division of Applied Solid State Chemistry TU Wien Getreidemarkt 9/E164-05-1 A-1060 Vienna Austria ; _publ_contact_author_email matthias.weil@tuwien.ac.at # Loop of author details _publ_section_title ;New structural insights into Fe~2~P~2~O~7~ - unravelling an unresolved dispute and three reversible phase transitions ; loop_ _publ_author_name _publ_author_address 'Stoger, Berthold' ;X-Ray Centre TU Wien Getreidemarkt 9 A-1060 Vienna Austria ; 'Weil, Matthias' ; Institute for Chemical Technologies and Analytics Division of Applied Solid State Chemistry TU Wien Getreidemarkt 9/E164-05-1 A-1060 Vienna Austria ; 'Glaum, Robert' ;Department of Inorganic Chemistry University of Bonn Gerhard-Domagk-Strasse 1 D-53121 Bonn Germany ; 'Fejfarova, Karla' ;Institute of Physics ASCR v.v.i. Na Slovance 2 182 21 Praha 8 Czechia ; 'Petricek, Vaclav' ;Institute of Physics ASCR v.v.i. Na Slovance 2 182 21 Praha 8 Czechia ; 'Dusek, Michal' ;Institute of Physics ASCR v.v.i. Na Slovance 2 182 21 Praha 8 Czechia ; 'Libowitzky, Eugen' ;Department of Mineralogy and Crystallography University of Vienna Josef-Holaubek-Platz 2 A-1090 Vienna Austria ; 'Fuglein, Ekkehard' ;Applications Laboratory NETZSCH-Geratebau GmbH Wittelsbacherstrasse 42 D-95100 Selb Germany ; #============================================================================== data_alpha1_standardsetting #============================================================================== # 5. CHEMICAL DATA _chemical_name_systematic ? _chemical_name_common ? _chemical_formula_moiety ? _chemical_formula_structural ? _chemical_formula_analytical ? _chemical_formula_iupac ? _chemical_formula_sum 'Fe2 O7 P2' _chemical_formula_weight 285.6 _chemical_melting_point ? _chemical_compound_source ? _chemical_absolute_configuration . #======================================================================= # 6. CRYSTAL DATA _space_group_crystal_system triclinic _space_group_name_H-M_alt 'P -1' _space_group_name_Hall '-P 1' _space_group_IT_number 2 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,-y,-z _cell_length_a 5.58850(16) _cell_length_b 6.3545(3) _cell_length_c 7.3692(16) _cell_angle_alpha 81.400(10) _cell_angle_beta 86.007(9) _cell_angle_gamma 72.204(3) _cell_volume 246.29(6) loop_ _twin_individual_id _twin_individual_mass_fraction_refined _twin_individual_twin_matrix_11 _twin_individual_twin_matrix_12 _twin_individual_twin_matrix_13 _twin_individual_twin_matrix_21 _twin_individual_twin_matrix_22 _twin_individual_twin_matrix_23 _twin_individual_twin_matrix_31 _twin_individual_twin_matrix_32 _twin_individual_twin_matrix_33 ? ? ? ? ? ? ? ? ? ? ? _cell_formula_units_Z 2 _cell_measurement_reflns_used 25284 _cell_measurement_theta_min 2.80 _cell_measurement_theta_max 41.22 _cell_measurement_temperature 100 _cell_special_details ? _exptl_crystal_density_diffrn 3.8516 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_F_000 276 _exptl_crystal_type_of_structure cryst _exptl_absorpt_coefficient_mu 6.519 _exptl_crystal_description 'plate' _exptl_crystal_colour 'light brown' _exptl_crystal_size_max 0.060 _exptl_crystal_size_mid 0.037 _exptl_crystal_size_min 0.010 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; STOE LANA, absorption correction by scaling of reflection intensities. J. Koziskova, F. Hahn, J. Richter, J. Kozisek, "Comparison of different absorption corrections on the model structure of tetrakis(\m~2~-acetato)- diaqua-di-copper(II)", Acta Chimica Slovaca, vol. 9, no. 2, 2016, pp. 136 - 140. Afterwards a spherical absorption correction was performed within STOE LANA. ; _exptl_absorpt_correction_T_min 0.4543 _exptl_absorpt_correction_T_max 0.5419 #======================================================================= # 7. EXPERIMENTAL DATA _diffrn_measurement_device 'Eulerian 4-circle diffractometer' _diffrn_measurement_device_type 'STOE STADIVARI' _diffrn_detector 'EIGER2 1M CDTE' _diffrn_detector_type ? _diffrn_detector_area_resol_mean 13.33 _diffrn_source 'Axo_Mo' _diffrn_source_type ? _diffrn_radiation_probe x-ray _diffrn_source_target ? _diffrn_source_voltage 60 _diffrn_source_current 0.830 _diffrn_source_power 0.050 _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_monochromator 'Graded multilayer mirror' _diffrn_radiation_polarisn_norm -90 _diffrn_radiation_collimation '1.2 0.6 mm diameter' _diffrn_ambient_temperature 100 _diffrn_measurement_method 'rotation method, \w scans' _diffrn_measurement_details ; 1935 frames, detector distance = 45 mm ; _diffrn_reflns_number 15018 _diffrn_reflns_theta_min 2.8 _diffrn_reflns_theta_max 41.06 _diffrn_reflns_theta_full 41.01 _diffrn_measured_fraction_theta_max 0.98 _diffrn_measured_fraction_theta_full 0.98 _diffrn_reflns_av_R_equivalents 0.0161 _diffrn_reflns_av_unetI/netI 0.0132 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_h_max 10 _diffrn_reflns_limit_k_min -9 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_l_min -8 _diffrn_reflns_limit_l_max 13 _diffrn_reflns_reduction_process ? _diffrn_standards_number ? _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% ? loop_ _diffrn_standard_refln_index_h _diffrn_standard_refln_index_k _diffrn_standard_refln_index_l ? ? ? #_diffrn_reflns_av_sunetI_over_netI 0.0132 #======================================================================= # 8. REFINEMENT DATA _refine_special_details ? _reflns_number_total 3198 _reflns_number_gt 2830 _reflns_threshold_expression 'I>2\s(I)' _refine_ls_structure_factor_coef Fsqd _refine_ls_R_factor_gt 0.0168 _refine_ls_wR_factor_gt 0.0405 _refine_ls_R_factor_all 0.0202 _refine_ls_wR_factor_ref 0.0408 _refine_ls_goodness_of_fit_ref 1.2769 _refine_ls_goodness_of_fit_gt 1.3507 _refine_ls_restrained_S_gt ? _refine_ls_restrained_S_all ? _refine_ls_number_reflns 3198 _refine_ls_number_parameters 101 _refine_ls_number_restraints 0 _refine_ls_number_constraints 0 _refine_ls_weighting_scheme sigma _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.02P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_hydrogen_treatment ? _refine_ls_shift/su_max 0.0022 _refine_ls_shift/su_mean 0.0002 _refine_diff_density_max ? _refine_diff_density_min ? _refine_ls_extinction_method 'B-C type 1 Gaussian isotropic (Becker & Coppens, 1974)' _refine_ls_extinction_coef 130(30) _refine_ls_extinction_expression ? _refine_ls_abs_structure_details ? _refine_ls_abs_structure_Flack ? _refine_ls_abs_structure_Rogers ? loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Fe 0.3463 0.8444 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' O 0.0106 0.0060 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' P 0.1023 0.0942 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' _computing_data_collection ; X-Area Pilatus3_SV 1.31.194.0 (STOE, 2023) ; _computing_cell_refinement ; X-Area Recipe 2.0.2 (STOE, 2024) ; _computing_data_reduction ; X-Area Integrate 2.5.18.0 (STOE, 2024) X-Area LANA 2.8.4 (STOE, 2024) ; _computing_publication_material ; STOE & Cie GmbH, X-Area, software package for collecting single-crystal or multi-domain crystal data on STOE area-detector diffractometers, for image processing, for the correction and scaling of reflection intensities and for outlier rejection, version 2.4, Darmstadt 2024 ; #======================================================================= # 9. ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_adp_type _atom_site_U_iso_or_equiv _atom_site_site_symmetry_multiplicity _atom_site_occupancy _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_disorder_assembly _atom_site_disorder_group Fe1a Fe 0.23189(2) 0.84797(2) 0.306934(17) Uani 0.00402(3) 2 1 d . . . Fe1b Fe -0.17832(2) 0.65341(2) 0.158440(17) Uani 0.00363(3) 2 1 d . . . P1a P 0.30718(4) 0.31844(4) 0.40545(3) Uani 0.00323(5) 2 1 d . . . P1b P 0.72307(4) 0.19797(4) 0.10898(3) Uani 0.00310(5) 2 1 d . . . O1a O 0.14313(12) 0.55312(10) 0.33618(9) Uani 0.00479(15) 2 1 d . . . O1b O 0.87765(12) -0.04010(10) 0.17448(9) Uani 0.00465(15) 2 1 d . . . O2a O 0.40161(12) 0.30369(11) 0.59740(8) Uani 0.00484(15) 2 1 d . . . O2b O 0.55895(12) 0.21262(10) -0.05143(9) Uani 0.00520(15) 2 1 d . . . O3a O 0.18749(13) 0.14056(11) 0.38785(9) Uani 0.00687(16) 2 1 d . . . O3b O 0.88492(12) 0.35431(10) 0.06697(9) Uani 0.00496(15) 2 1 d . . . O4 O 0.55648(13) 0.28457(11) 0.28032(9) Uani 0.00705(16) 2 1 d . . . loop_ _atom_site_aniso_label _atom_site_aniso_type_symbol _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Fe1a Fe 0.00420(5) 0.00321(5) 0.00499(5) -0.00137(4) -0.00098(4) -0.00062(3) Fe1b Fe 0.00371(5) 0.00343(5) 0.00411(5) -0.00135(4) -0.00003(3) -0.00100(3) P1a P 0.00351(8) 0.00311(8) 0.00302(8) -0.00092(6) -0.00028(6) -0.00027(6) P1b P 0.00315(8) 0.00287(8) 0.00326(8) -0.00102(6) 0.00005(6) -0.00016(6) O1a O 0.0047(2) 0.0034(2) 0.0059(2) -0.00088(18) -0.00104(18) 0.00041(18) O1b O 0.0047(2) 0.0031(2) 0.0058(2) -0.00081(18) -0.00105(18) 0.00028(18) O2a O 0.0046(2) 0.0065(2) 0.0035(2) -0.00166(18) -0.00069(18) -0.00062(18) O2b O 0.0047(2) 0.0063(2) 0.0047(2) -0.00178(19) -0.00115(18) -0.00053(18) O3a O 0.0082(3) 0.0046(2) 0.0088(3) -0.0029(2) -0.0020(2) -0.0010(2) O3b O 0.0056(2) 0.0045(2) 0.0058(2) -0.00307(18) 0.00054(18) -0.00078(18) O4 O 0.0058(2) 0.0090(3) 0.0059(2) -0.0015(2) 0.00244(19) -0.0024(2) #======================================================================= # 10. MOLECULAR GEOMETRY loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_1 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Fe1a O1a . . 2.0580(7) ? Fe1a O1b . 1_465 2.1397(7) ? Fe1a O2a . 2_666 2.1005(7) ? Fe1a O2b . 2_665 2.1668(10) ? Fe1a O3a . 1_565 1.9756(8) ? Fe1b O1a . . 2.1742(8) ? Fe1b O1b . 1_465 2.0860(7) ? Fe1b O2a . 2_566 2.1201(9) ? Fe1b O2b . 2_565 2.1903(7) ? Fe1b O3b . 1_455 2.0325(7) ? Fe1b O3b . 2_665 2.2463(9) ? P1a O1a . . 1.5254(6) ? P1a O2a . . 1.5238(9) ? P1a O3a . . 1.5033(8) ? P1a O4 . . 1.5921(8) ? P1b O1b . . 1.5194(6) ? P1b O2b . . 1.5209(8) ? P1b O3b . . 1.5229(8) ? P1b O4 . . 1.5795(8) ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_2 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag O1a Fe1a O1b . . 1_465 79.99(3) ? O1a Fe1a O2a . . 2_666 94.08(3) ? O1a Fe1a O2b . . 2_665 93.57(3) ? O1a Fe1a O3a . . 1_565 149.50(3) ? O1b Fe1a O2a 1_465 . 2_666 169.60(3) ? O1b Fe1a O2b 1_465 . 2_665 92.81(3) ? O1b Fe1a O3a 1_465 . 1_565 92.99(3) ? O2a Fe1a O2b 2_666 . 2_665 78.95(3) ? O2a Fe1a O3a 2_666 . 1_565 96.36(3) ? O2b Fe1a O3a 2_665 . 1_565 116.53(3) ? O1a Fe1b O1b . . 1_465 78.59(3) ? O1a Fe1b O2a . . 2_566 85.93(3) ? O1a Fe1b O2b . . 2_565 163.49(3) ? O1a Fe1b O3b . . 1_455 96.62(3) ? O1a Fe1b O3b . . 2_665 83.59(3) ? O1b Fe1b O2a 1_465 . 2_566 87.48(3) ? O1b Fe1b O2b 1_465 . 2_565 96.72(3) ? O1b Fe1b O3b 1_465 . 1_455 156.35(3) ? O1b Fe1b O3b 1_465 . 2_665 81.59(3) ? O2a Fe1b O2b 2_566 . 2_565 78.01(3) ? O2a Fe1b O3b 2_566 . 1_455 115.48(3) ? O2a Fe1b O3b 2_566 . 2_665 166.15(3) ? O2b Fe1b O3b 2_565 . 1_455 93.76(3) ? O2b Fe1b O3b 2_565 . 2_665 111.59(3) ? O3b Fe1b O3b 1_455 . 2_665 74.84(3) ? O1a P1a O2a . . . 111.85(4) ? O1a P1a O3a . . . 113.24(4) ? O1a P1a O4 . . . 104.60(4) ? O2a P1a O3a . . . 113.17(4) ? O2a P1a O4 . . . 103.17(4) ? O3a P1a O4 . . . 109.93(4) ? O1b P1b O2b . . . 112.46(4) ? O1b P1b O3b . . . 112.18(4) ? O1b P1b O4 . . . 105.78(4) ? O2b P1b O3b . . . 111.76(4) ? O2b P1b O4 . . . 110.77(4) ? O3b P1b O4 . . . 103.34(4) ? Fe1a O1a Fe1b . . . 99.68(2) ? Fe1a O1a P1a . . . 128.53(4) ? Fe1b O1a P1a . . . 128.74(5) ? Fe1a O1b Fe1b 1_645 . 1_645 99.92(2) ? Fe1a O1b P1b 1_645 . . 128.13(5) ? Fe1b O1b P1b 1_645 . . 131.93(4) ? Fe1a O2a Fe1b 2_666 . 2_566 103.60(3) ? Fe1a O2a P1a 2_666 . . 127.94(4) ? Fe1b O2a P1a 2_566 . . 126.38(4) ? Fe1a O2b Fe1b 2_665 . 2_565 99.15(3) ? Fe1a O2b P1b 2_665 . . 113.70(4) ? Fe1b O2b P1b 2_565 . . 144.96(4) ? Fe1a O3a P1a 1_545 . . 146.26(4) ? Fe1b O3b Fe1b 1_655 . 2_665 105.16(3) ? Fe1b O3b P1b 1_655 . . 126.48(4) ? Fe1b O3b P1b 2_665 . . 126.78(4) ? P1a O4 P1b . . . 151.91(6) ? #======================================================================= # 11. STRUCTURE-FACTOR LIST loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_include_status 1 0 0 91.25 95.87 1.08 o 2 0 0 8024.29 7980.35 7.85 o 3 0 0 2743.58 2927.69 5.88 o 4 0 0 143.08 147.67 2.42 o 5 0 0 105.28 122.23 2.94 o 6 0 0 1.70 4.82 2.67 < 7 0 0 210.30 207.16 5.96 o 8 0 0 108.18 111.36 5.63 o 9 0 0 0.05 0.85 5.92 < -9 1 0 97.62 97.81 5.73 o -8 1 0 638.58 664.17 10.08 o -7 1 0 437.91 457.02 6.45 o -6 1 0 153.54 168.67 3.88 o -5 1 0 1898.35 1921.56 8.65 o -4 1 0 388.42 386.52 3.13 o -3 1 0 406.24 375.20 2.86 o -2 1 0 2.23 2.00 0.92 o -1 1 0 93.57 85.39 0.90 o 0 1 0 38.55 38.21 0.46 o 1 1 0 3.85 3.88 0.67 o 2 1 0 725.14 721.45 3.60 o 3 1 0 23.57 17.62 1.40 o 4 1 0 996.52 1017.87 4.45 o 5 1 0 2349.35 2416.06 9.33 o 6 1 0 1128.19 1208.27 7.87 o 7 1 0 1711.07 1821.18 10.99 o 8 1 0 2.63 2.96 4.80 < 9 1 0 1045.56 1072.15 12.42 o 10 1 0 77.01 73.41 13.89 o -9 2 0 99.76 93.10 10.36 o -8 2 0 69.34 72.68 6.26 o -7 2 0 209.05 210.70 5.13 o -6 2 0 17.39 17.41 3.29 o -5 2 0 247.22 245.98 3.92 o -4 2 0 30.82 24.56 2.13 o -3 2 0 1917.36 1757.99 4.62 o -2 2 0 1163.89 1134.36 3.37 o -1 2 0 1754.25 1472.82 2.70 o 0 2 0 6109.66 6061.47 4.55 o 1 2 0 14469.80 14651.10 8.03 o 3 2 0 3739.65 3767.97 8.94 o 4 2 0 1710.47 1734.91 6.96 o 5 2 0 166.85 166.54 4.11 o 6 2 0 398.47 411.77 5.65 o 7 2 0 0.67 -0.73 4.09 < 8 2 0 309.08 315.56 5.82 o 9 2 0 25.21 24.04 4.46 o 10 2 0 63.46 62.30 5.48 o -8 3 0 266.13 278.34 7.70 o -7 3 0 258.90 260.42 6.51 o -6 3 0 523.70 532.03 6.01 o -5 3 0 0.74 1.73 2.54 < -4 3 0 1954.07 1830.41 8.59 o -3 3 0 18.36 18.87 1.65 o -2 3 0 309.80 304.90 2.00 o -1 3 0 135.48 133.20 1.38 o 0 3 0 150.05 150.74 1.11 o 1 3 0 1.33 2.02 0.73 o 2 3 0 625.36 667.34 2.71 o 3 3 0 180.04 188.32 3.34 o 4 3 0 1498.63 1501.44 6.88 o 5 3 0 97.02 93.56 4.00 o 6 3 0 1973.76 1936.90 9.59 o 7 3 0 16.19 21.20 4.71 o 8 3 0 901.10 955.73 9.39 o 9 3 0 61.77 68.66 5.40 o 10 3 0 573.18 570.45 9.05 o -8 4 0 143.22 145.32 6.92 o -7 4 0 208.82 214.06 6.80 o -6 4 0 161.61 171.26 5.94 o -5 4 0 211.60 201.34 3.48 o -4 4 0 107.15 92.56 3.88 o -3 4 0 5.39 4.32 2.04 o -2 4 0 1655.53 1555.57 5.06 o -1 4 0 2381.27 2354.33 4.67 o 0 4 0 1872.43 1816.58 3.81 o 1 4 0 11285.80 11278.80 10.58 o 2 4 0 1747.13 1838.39 7.36 o 3 4 0 3767.62 3674.03 8.02 o 4 4 0 25.92 32.17 2.34 o 5 4 0 738.06 729.57 7.58 o 6 4 0 1.56 3.11 3.34 < 7 4 0 153.70 150.32 4.25 o 8 4 0 80.94 87.13 5.55 o 9 4 0 24.92 22.00 4.82 o 10 4 0 2.56 2.90 4.63 < -7 5 0 699.41 717.90 10.16 o -6 5 0 25.03 19.31 4.42 o -5 5 0 308.33 303.38 7.32 o -4 5 0 425.15 412.97 4.65 o -3 5 0 146.27 142.69 4.48 o -2 5 0 65.35 63.22 2.71 o -1 5 0 2.12 1.96 1.36 < 0 5 0 5.09 6.15 1.19 o 1 5 0 207.70 200.09 1.94 o 2 5 0 0.65 1.54 1.48 < 3 5 0 82.41 92.31 1.75 o 4 5 0 37.60 34.80 3.17 o 5 5 0 1387.91 1412.50 8.90 o 6 5 0 253.28 254.40 4.73 o 7 5 0 2057.72 2043.21 14.33 o 8 5 0 1124.18 1127.85 10.52 o 9 5 0 533.73 543.43 12.41 o 10 5 0 916.63 912.73 9.72 o -6 6 0 156.30 149.70 8.09 o -5 6 0 9.25 6.94 4.15 < -4 6 0 59.89 59.11 3.38 o -3 6 0 103.45 97.87 3.25 o -2 6 0 257.61 252.32 3.55 o -1 6 0 84.03 81.01 2.77 o 0 6 0 3362.92 3417.57 9.80 o 1 6 0 48.71 47.62 2.23 o 2 6 0 5429.95 5318.75 14.15 o 3 6 0 221.34 218.01 4.82 o 4 6 0 1463.90 1487.39 7.87 o 5 6 0 288.12 284.24 6.51 o 6 6 0 128.36 132.26 3.75 o 7 6 0 18.74 17.83 4.07 o 8 6 0 6.76 9.38 4.94 < 9 6 0 126.51 123.71 5.59 o -5 7 0 37.19 30.86 5.34 o -4 7 0 111.08 112.53 4.55 o -3 7 0 148.79 144.59 4.19 o -2 7 0 12.20 14.01 2.75 o -1 7 0 3.24 2.21 3.00 < 0 7 0 5.98 5.59 2.36 o 1 7 0 128.66 125.59 3.98 o 2 7 0 1.49 1.17 2.06 < 3 7 0 21.46 23.64 2.21 o 4 7 0 143.11 142.94 2.96 o 5 7 0 673.14 708.41 7.99 o 6 7 0 188.73 189.49 5.09 o 7 7 0 963.25 957.91 8.31 o 8 7 0 80.05 84.47 5.55 o 9 7 0 995.44 961.38 12.60 o -4 8 0 233.99 219.94 6.63 o -3 8 0 33.72 38.07 5.75 o -2 8 0 4.93 1.67 4.23 < -1 8 0 139.80 144.44 4.17 o 0 8 0 263.08 265.41 5.13 o 1 8 0 940.42 973.95 6.24 o 2 8 0 302.42 307.66 4.71 o 3 8 0 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10 185.55 186.59 10.78 o 7 3 10 11.25 10.78 15.24 < -4 4 10 135.77 129.86 5.36 o -3 4 10 18.16 19.10 3.32 o -2 4 10 59.58 58.69 3.92 o -1 4 10 1.49 -0.38 2.98 < 0 4 10 84.58 85.93 3.84 o 1 4 10 64.48 72.27 3.50 o 2 4 10 974.10 952.71 10.00 o 3 4 10 156.62 158.50 4.63 o 4 4 10 851.32 844.32 13.38 o 5 4 10 285.87 279.45 16.98 o 6 4 10 173.72 179.33 17.45 o 7 4 10 480.84 464.00 20.65 o -4 5 10 252.26 238.51 6.17 o -3 5 10 133.18 126.21 4.34 o -2 5 10 164.24 166.36 3.96 o -1 5 10 285.33 281.87 5.38 o 0 5 10 17.65 15.07 3.73 o 1 5 10 73.26 73.66 3.67 o 2 5 10 612.60 605.08 8.89 o 3 5 10 22.15 22.50 5.55 o 4 5 10 720.52 717.36 9.89 o 5 5 10 1.68 2.00 7.15 < 6 5 10 83.35 79.21 8.65 o 7 5 10 36.82 39.74 9.32 o -3 6 10 266.67 257.63 5.09 o -2 6 10 3.45 1.71 3.52 < -1 6 10 59.15 61.30 3.59 o 0 6 10 24.95 27.23 3.96 o 1 6 10 65.66 62.47 4.73 o 2 6 10 95.74 91.85 6.94 o 3 6 10 497.81 492.66 9.72 o 4 6 10 403.97 398.64 10.49 o 5 6 10 382.94 381.90 8.70 o 6 6 10 442.47 420.27 13.66 o 7 6 10 0.82 1.83 9.61 < -2 7 10 476.88 467.94 7.84 o -1 7 10 3.13 4.48 3.86 < 0 7 10 278.26 272.36 7.03 o 1 7 10 36.00 34.86 4.27 o 2 7 10 100.59 84.32 11.55 o 3 7 10 424.45 419.88 14.35 o 4 7 10 95.56 107.82 10.97 o 5 7 10 250.69 246.06 10.76 o 6 7 10 44.70 43.81 10.03 o -1 8 10 6.00 2.88 6.30 < 0 8 10 9.85 6.46 4.36 < 1 8 10 3.63 2.86 4.90 < 2 8 10 91.15 77.52 12.66 o 3 8 10 237.28 231.10 13.12 o 4 8 10 153.35 168.71 12.93 o 5 8 10 858.82 830.40 14.71 o 2 9 10 9.15 8.80 9.76 < -2 -5 11 5.25 4.11 6.19 < -1 -5 11 49.70 42.08 6.63 o 0 -5 11 30.57 21.29 7.59 o -3 -4 11 35.68 36.99 6.25 o -2 -4 11 843.83 834.18 9.47 o -1 -4 11 11.18 11.13 5.21 o 0 -4 11 179.48 175.56 6.23 o 1 -4 11 187.19 195.41 6.65 o 2 -4 11 13.70 10.90 6.15 < -4 -3 11 17.05 16.10 8.57 < -3 -3 11 194.69 193.89 6.30 o -2 -3 11 119.90 121.23 5.94 o -1 -3 11 134.85 144.38 5.94 o 0 -3 11 0.42 0.71 4.46 < 1 -3 11 24.49 24.44 5.36 o 2 -3 11 38.97 54.88 8.86 o 3 -3 11 432.67 446.17 9.28 o -5 -2 11 160.17 148.11 7.88 o -4 -2 11 13.51 13.57 5.21 o -3 -2 11 466.72 439.94 9.24 o -2 -2 11 5.14 7.32 4.88 < -1 -2 11 554.29 563.34 7.76 o 0 -2 11 17.36 19.87 4.32 o 1 -2 11 106.92 104.21 6.01 o 2 -2 11 188.96 198.06 6.51 o 3 -2 11 44.05 38.36 5.69 o 4 -2 11 150.12 143.61 8.90 o -5 -1 11 33.16 26.83 5.27 o -4 -1 11 0.74 -0.13 4.98 < -3 -1 11 0.06 -0.25 4.90 < -2 -1 11 286.51 288.94 6.69 o -1 -1 11 4.56 3.88 4.19 < 0 -1 11 257.48 263.03 6.01 o 1 -1 11 1.70 3.17 4.32 < 2 -1 11 16.47 14.34 4.46 o 3 -1 11 25.69 26.25 5.11 o 4 -1 11 314.99 326.18 8.11 o 5 -1 11 24.50 28.96 7.57 o -5 0 11 122.51 115.00 7.21 o -4 0 11 428.31 431.19 8.16 o -3 0 11 103.20 106.96 4.48 o -2 0 11 966.64 948.38 8.18 o -1 0 11 441.06 440.83 9.03 o 0 0 11 301.48 308.84 5.69 o 1 0 11 175.25 179.31 5.59 o 2 0 11 48.41 54.36 4.30 o 3 0 11 31.59 31.77 5.27 o 4 0 11 94.94 97.48 5.57 o 5 0 11 7.40 4.82 7.13 < -5 1 11 6.96 10.13 4.69 o -4 1 11 162.94 159.31 4.86 o -3 1 11 32.23 31.38 3.96 o -2 1 11 294.10 302.04 5.28 o -1 1 11 25.14 30.54 3.50 o 0 1 11 178.67 182.15 6.09 o 1 1 11 17.08 21.04 4.13 o 2 1 11 1.39 2.17 3.82 < 3 1 11 166.18 177.22 5.46 o 4 1 11 16.91 19.12 5.61 o 5 1 11 318.62 322.44 11.16 o 6 1 11 319.31 316.02 18.31 o -4 2 11 35.32 36.80 3.79 o -3 2 11 231.18 233.18 5.88 o -2 2 11 830.30 835.39 6.89 o -1 2 11 244.21 237.15 4.82 o 0 2 11 610.65 616.70 6.20 o 1 2 11 77.29 76.94 4.63 o 2 2 11 19.35 19.45 3.90 o 3 2 11 59.37 57.71 5.21 o 4 2 11 3.02 4.09 6.28 < 5 2 11 0.90 -2.54 7.13 < 6 2 11 130.94 125.09 15.33 o -4 3 11 127.58 127.11 4.80 o -3 3 11 32.72 31.80 4.15 o -2 3 11 44.94 46.97 4.57 o -1 3 11 353.19 365.54 5.46 o 0 3 11 15.42 18.95 4.21 o 1 3 11 428.58 435.75 7.99 o 2 3 11 121.66 130.68 7.92 o 3 3 11 45.53 45.58 5.75 o 4 3 11 185.92 191.28 7.51 o 5 3 11 292.55 299.49 15.20 o 6 3 11 19.15 16.72 17.62 < -4 4 11 355.62 308.00 9.95 o -3 4 11 252.32 248.10 6.30 o -2 4 11 34.39 36.59 3.90 o -1 4 11 1281.00 1276.96 10.40 o 0 4 11 23.99 26.42 3.82 o 1 4 11 1113.42 1124.77 9.93 o 2 4 11 2.37 1.15 5.36 < 3 4 11 19.46 20.29 5.63 o 4 4 11 143.39 140.81 7.36 o 5 4 11 18.40 21.83 13.36 < 6 4 11 23.37 14.66 17.03 < -3 5 11 236.00 239.90 7.22 o -2 5 11 113.77 107.90 5.55 o -1 5 11 74.00 74.33 4.84 o 0 5 11 62.73 62.72 4.61 o 1 5 11 170.67 163.02 7.17 o 2 5 11 108.47 112.16 5.78 o 3 5 11 209.35 202.42 8.65 o 4 5 11 71.28 76.29 8.69 o 5 5 11 224.78 219.52 15.18 o 6 5 11 647.63 631.02 22.82 o -2 6 11 731.15 733.32 13.08 o -1 6 11 411.03 411.78 8.34 o 0 6 11 660.59 626.76 9.12 o 1 6 11 296.44 292.14 9.09 o 2 6 11 208.07 210.03 8.61 o 3 6 11 24.18 21.91 9.24 o 4 6 11 0.79 0.02 9.19 < -1 7 11 59.80 49.08 7.74 o 0 7 11 276.29 256.07 7.53 o 1 7 11 12.38 12.26 7.53 < 2 7 11 367.54 347.15 14.14 o 3 7 11 192.59 187.76 12.41 o 4 7 11 25.65 21.68 11.90 < 5 7 11 337.16 308.35 14.35 o 3 8 11 120.04 118.50 12.55 o -3 -3 12 204.56 152.65 9.20 o -2 -3 12 168.17 155.98 6.26 o -1 -3 12 621.53 581.87 9.53 o 0 -3 12 343.89 330.48 8.36 o 1 -3 12 213.81 221.42 9.32 o -3 -2 12 9.65 5.32 5.78 < -2 -2 12 167.50 157.56 6.30 o -1 -2 12 123.85 119.81 6.13 o 0 -2 12 146.12 139.52 6.78 o 1 -2 12 232.84 221.70 7.67 o 2 -2 12 21.04 25.17 6.59 o 3 -2 12 159.64 157.54 14.62 o -4 -1 12 542.44 483.01 12.04 o -3 -1 12 56.34 55.90 4.90 o -2 -1 12 78.01 72.52 6.32 o -1 -1 12 1255.36 1286.25 11.81 o 0 -1 12 23.17 29.77 5.19 o 1 -1 12 701.53 748.67 9.93 o 2 -1 12 33.91 26.12 6.90 o 3 -1 12 155.74 155.99 10.76 o 4 -1 12 29.48 24.69 12.93 < -4 0 12 360.64 333.26 10.49 o -3 0 12 101.11 94.41 5.00 o -2 0 12 22.28 22.14 5.30 o -1 0 12 70.83 73.75 6.13 o 0 0 12 87.82 91.78 5.40 o 1 0 12 570.62 579.12 9.01 o 2 0 12 168.15 161.31 6.67 o 3 0 12 537.19 554.27 10.45 o 4 0 12 37.80 40.09 6.44 o -4 1 12 100.59 96.31 6.11 o -3 1 12 170.61 164.46 5.98 o -2 1 12 116.77 115.58 4.67 o -1 1 12 27.85 34.99 6.48 o 0 1 12 1033.75 1061.30 12.29 o 1 1 12 21.62 21.06 5.13 o 2 1 12 880.53 907.45 10.25 o 3 1 12 223.20 215.71 10.11 o 4 1 12 200.21 195.02 10.24 o 5 1 12 287.34 292.86 15.85 o -3 2 12 360.90 354.24 6.30 o -2 2 12 28.06 30.25 4.02 o -1 2 12 29.28 35.40 4.63 o 0 2 12 67.05 70.56 7.05 o 1 2 12 5.92 10.63 6.36 < 2 2 12 526.08 520.28 9.68 o 3 2 12 5.19 4.92 6.34 < 4 2 12 491.51 492.60 12.68 o 5 2 12 128.01 126.82 13.89 o -3 3 12 375.58 368.97 7.70 o -2 3 12 4.43 5.90 4.69 < -1 3 12 352.35 354.61 7.13 o 0 3 12 807.14 823.92 13.40 o 1 3 12 365.97 367.92 8.84 o 2 3 12 723.82 711.23 12.77 o 3 3 12 53.61 58.65 6.96 o 4 3 12 251.89 249.08 10.74 o -2 4 12 104.67 107.90 5.65 o -1 4 12 70.26 69.14 5.30 o 0 4 12 46.30 49.77 5.92 o 1 4 12 140.00 140.02 6.19 o 2 4 12 247.79 244.28 9.78 o 3 4 12 370.78 373.66 10.99 o 4 4 12 343.13 355.34 10.78 o -1 5 12 105.82 99.83 5.67 o 0 5 12 24.07 24.69 6.23 o 1 5 12 752.53 743.33 11.18 o 2 5 12 5.66 2.36 5.55 < 3 5 12 682.39 709.79 13.64 o 4 5 12 20.50 14.95 8.61 < 0 6 12 22.52 21.62 7.69 o 1 6 12 31.09 36.82 8.57 o 2 6 12 104.74 102.69 8.44 o 3 6 12 453.32 408.53 15.39 o -1 -1 13 198.20 209.07 8.59 o 0 -1 13 3.62 6.42 6.09 < 1 -1 13 16.51 9.28 7.30 < -2 0 13 261.37 255.32 17.14 o -1 0 13 58.03 50.83 7.71 o 0 0 13 218.76 226.43 7.80 o 1 0 13 137.78 149.92 7.24 o 2 0 13 127.60 123.32 7.24 o -2 1 13 35.29 31.57 11.65 o -1 1 13 10.87 8.21 6.94 < 0 1 13 3.77 5.92 6.03 < 1 1 13 3.22 3.86 6.15 < 2 1 13 5.53 2.63 7.51 < 3 1 13 111.80 130.72 14.32 o -1 2 13 432.56 413.42 12.14 o 0 2 13 88.46 97.64 7.55 o 1 2 13 35.29 30.75 7.19 o 2 2 13 190.44 200.92 10.41 o 3 2 13 57.98 65.57 7.96 o -1 3 13 47.36 43.97 5.94 o 0 3 13 105.80 99.67 8.01 o 1 3 13 29.04 33.09 6.90 o 2 3 13 3.70 5.09 6.88 < 3 3 13 16.56 16.93 9.32 < 0 4 13 255.17 240.74 8.15 o 1 4 13 116.15 117.75 8.03 o 2 4 13 85.20 100.67 9.55 o 3 4 13 152.14 144.52 9.97 o 2 5 13 20.74 23.73 10.36 o #======================================================================= data_alpha1 #======================================================================= # 5. CHEMICAL DATA _chemical_name_systematic ? _chemical_name_common ? _chemical_formula_moiety ? _chemical_formula_structural ? _chemical_formula_analytical ? _chemical_formula_iupac ? _chemical_formula_sum 'Fe2 O7 P2' _chemical_formula_weight 285.6 _chemical_melting_point ? _chemical_compound_source ? _chemical_absolute_configuration . #======================================================================= # 6. CRYSTAL DATA _space_group_crystal_system triclinic _space_group_name_H-M_alt 'X-1' _space_group_name_Hall '-X 1' _space_group_IT_number 2 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,-y,-z 3 x+3/4,y+1/4,z 4 -x+3/4,-y+1/4,-z 5 x+1/2,y+1/2,z 6 -x+1/2,-y+1/2,-z 7 x+1/4,y+3/4,z 8 -x+1/4,-y+3/4,-z _cell_length_a 13.3690(5) _cell_length_b 16.9853(4) _cell_length_c 6.3545(3) _cell_angle_alpha 50.200(3) _cell_angle_beta 72.409(4) _cell_angle_gamma 94.100(4) _cell_volume 985.17(11) _cell_formula_units_Z 8 _cell_measurement_reflns_used 25284 _cell_measurement_theta_min 2.80 _cell_measurement_theta_max 41.22 _cell_measurement_temperature 100 _cell_special_details ? _exptl_crystal_density_diffrn 3.8516 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_F_000 1104 _exptl_crystal_type_of_structure cryst _exptl_absorpt_coefficient_mu 6.519 _exptl_crystal_description 'plate' _exptl_crystal_colour 'light brown' _exptl_crystal_size_max 0.060 _exptl_crystal_size_mid 0.037 _exptl_crystal_size_min 0.010 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; STOE LANA, absorption correction by scaling of reflection intensities. J. Koziskova, F. Hahn, J. Richter, J. Kozisek, "Comparison of different absorption corrections on the model structure of tetrakis(\m~2~-acetato)- diaqua-di-copper(II)", Acta Chimica Slovaca, vol. 9, no. 2, 2016, pp. 136 - 140. Afterwards a spherical absorption correction was performed within STOE LANA. ; _exptl_absorpt_correction_T_min 0.4543 _exptl_absorpt_correction_T_max 0.5419 #======================================================================= # 7. EXPERIMENTAL DATA _diffrn_measurement_device 'Eulerian 4-circle diffractometer' _diffrn_measurement_device_type 'STOE STADIVARI' _diffrn_detector 'EIGER2 1M CDTE' _diffrn_detector_type ? _diffrn_detector_area_resol_mean 13.33 _diffrn_source 'Axo_Mo' _diffrn_source_type ? _diffrn_radiation_probe x-ray _diffrn_source_target ? _diffrn_source_voltage 60 _diffrn_source_current 0.830 _diffrn_source_power 0.050 _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_monochromator 'Graded multilayer mirror' _diffrn_radiation_polarisn_norm -90 _diffrn_radiation_collimation '1.2 0.6 mm diameter' _diffrn_ambient_temperature 100 _diffrn_measurement_method 'rotation method, \w scans' _diffrn_measurement_details ; 1935 frames, detector distance = 45 mm ; _diffrn_reflns_number 15018 _diffrn_reflns_theta_min 2.8 _diffrn_reflns_theta_max 41.06 _diffrn_reflns_theta_full 41.01 _diffrn_measured_fraction_theta_max 0.98 _diffrn_measured_fraction_theta_full 0.98 _diffrn_reflns_av_R_equivalents 0.0161 _diffrn_reflns_av_unetI/netI 0.0132 _diffrn_reflns_limit_h_min -23 _diffrn_reflns_limit_h_max 24 _diffrn_reflns_limit_k_min -18 _diffrn_reflns_limit_k_max 31 _diffrn_reflns_limit_l_min -9 _diffrn_reflns_limit_l_max 11 _diffrn_reflns_reduction_process ? #_diffrn_reflns_av_sigmaI/netI 0.0132 #======================================================================= # 8. REFINEMENT DATA _reflns_number_total 3198 _reflns_number_gt 2830 _reflns_threshold_expression 'I>2\s(I)' _refine_ls_structure_factor_coef Fsqd _refine_ls_R_factor_gt 0.0168 _refine_ls_wR_factor_gt 0.0405 _refine_ls_R_factor_all 0.0202 _refine_ls_wR_factor_ref 0.0408 _refine_ls_goodness_of_fit_ref 1.2769 _refine_ls_goodness_of_fit_gt 1.3507 _refine_ls_restrained_S_gt ? _refine_ls_restrained_S_all ? _refine_ls_number_reflns 3198 _refine_ls_number_parameters 101 _refine_ls_number_restraints 0 _refine_ls_number_constraints 0 _refine_ls_weighting_scheme sigma _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.02P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_hydrogen_treatment ? _refine_ls_shift/su_max 0.0444 _refine_ls_shift/su_mean 0.0047 _refine_diff_density_max 0.70 _refine_diff_density_min -1.02 _refine_ls_extinction_method 'B-C type 1 Gaussian isotropic (Becker & Coppens, 1974)' _refine_ls_extinction_coef 130(30) _refine_ls_extinction_expression ? _refine_ls_abs_structure_details ? _refine_ls_abs_structure_Flack ? _refine_ls_abs_structure_Rogers ? loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Fe 0.3463 0.8444 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' O 0.0106 0.0060 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' P 0.1023 0.0942 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' _computing_data_collection ; X-Area Pilatus3_SV 1.31.194.0 (STOE, 2023) ; _computing_cell_refinement ; X-Area Recipe 2.0.2 (STOE, 2024) ; _computing_data_reduction ; X-Area Integrate 2.5.18.0 (STOE, 2024) X-Area LANA 2.8.4 (STOE, 2024) ; _computing_publication_material ; STOE & Cie GmbH, X-Area, software package for collecting single-crystal or multi-domain crystal data on STOE area-detector diffractometers, for image processing, for the correction and scaling of reflection intensities and for outlier rejection, version 2.4, Darmstadt 2024 ; #======================================================================= # 9. ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_adp_type _atom_site_U_iso_or_equiv _atom_site_site_symmetry_multiplicity _atom_site_occupancy _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_disorder_assembly _atom_site_disorder_group Fe1a Fe 0.095495(11) 0.211439(10) 0.54104(3) Uani 0.00403(6) 8 1 d . . . Fe1b Fe 0.123799(10) 0.034640(10) 0.49497(3) Uani 0.00363(6) 8 1 d . . . P1a P 0.125929(19) 0.279521(18) -0.08701(5) Uani 0.00323(10) 8 1 d . . . P1b P -0.126281(19) 0.235257(18) 0.08900(5) Uani 0.00310(10) 8 1 d . . . O1a O 0.13231(6) 0.20387(5) 0.21694(14) Uani 0.0048(3) 8 1 d . . . O1b O -0.13217(6) 0.30665(5) -0.21457(14) Uani 0.0046(3) 8 1 d . . . O2a O 0.19830(5) 0.39910(5) -0.29371(15) Uani 0.0048(3) 8 1 d . . . O2b O -0.16545(6) 0.11402(5) 0.26405(15) Uani 0.0052(3) 8 1 d . . . O3a O 0.14705(6) 0.24080(5) -0.24729(15) Uani 0.0069(3) 8 1 d . . . O3b O -0.18775(5) 0.25471(5) 0.28734(15) Uani 0.0050(3) 8 1 d . . . O4 O 0.00104(5) 0.27928(5) 0.00426(15) Uani 0.0070(3) 8 1 d . . . loop_ _atom_site_aniso_label _atom_site_aniso_type_symbol _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Fe1a Fe 0.00552(5) 0.00392(5) 0.00401(5) 0.00206(4) -0.00257(4) -0.00310(4) Fe1b Fe 0.00391(5) 0.00405(5) 0.00414(5) 0.00161(4) -0.00206(4) -0.00320(4) P1a P 0.00335(8) 0.00298(8) 0.00295(8) 0.00093(6) -0.00135(6) -0.00196(7) P1b P 0.00310(8) 0.00336(8) 0.00281(8) 0.00121(6) -0.00125(6) -0.00217(7) O1a O 0.0063(2) 0.0046(2) 0.0035(2) 0.00252(18) -0.00261(19) -0.0027(2) O1b O 0.0062(2) 0.0046(2) 0.0035(2) 0.00244(18) -0.00266(19) -0.0027(2) O2a O 0.0044(2) 0.0033(2) 0.0052(2) 0.00089(18) -0.00161(19) -0.0026(2) O2b O 0.0057(2) 0.0037(2) 0.0055(2) 0.00172(18) -0.0023(2) -0.0030(2) O3a O 0.0102(3) 0.0069(2) 0.0064(3) 0.0034(2) -0.0044(2) -0.0055(2) O3b O 0.0051(2) 0.0064(2) 0.0051(2) 0.00215(18) -0.00185(19) -0.0048(2) O4 O 0.0035(2) 0.0084(3) 0.0090(3) 0.00219(19) -0.0029(2) -0.0059(2) #======================================================================= # 10. MOLECULAR GEOMETRY loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_1 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Fe1a O1a . . 2.0580(11) ? Fe1a O1b . 7_546 2.1397(8) ? Fe1a O2a . 8_555 2.1005(8) ? Fe1a O2b . 4_456 2.1668(8) ? Fe1a O3a . 1_556 1.9756(12) ? Fe1b O1a . . 2.1742(8) ? Fe1b O1b . 7_546 2.0860(12) ? Fe1b O2a . 6_555 2.1201(7) ? Fe1b O2b . 2_556 2.1903(8) ? Fe1b O3b . 7_545 2.0325(11) ? Fe1b O3b . 4_456 2.2463(7) ? P1a O1a . . 1.5254(9) ? P1a O2a . . 1.5238(8) ? P1a O3a . . 1.5033(12) ? P1a O4 . . 1.5921(8) ? P1b O1b . . 1.5194(9) ? P1b O2b . . 1.5209(9) ? P1b O3b . . 1.5228(11) ? P1b O4 . . 1.5795(8) ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_2 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag O1a Fe1a O1b . . 7_546 79.99(3) ? O1a Fe1a O2a . . 8_555 94.08(4) ? O1a Fe1a O2b . . 4_456 93.57(4) ? O1a Fe1a O3a . . 1_556 149.50(3) ? O1b Fe1a O2a 7_546 . 8_555 169.60(4) ? O1b Fe1a O2b 7_546 . 4_456 92.81(3) ? O1b Fe1a O3a 7_546 . 1_556 92.99(4) ? O2a Fe1a O2b 8_555 . 4_456 78.95(3) ? O2a Fe1a O3a 8_555 . 1_556 96.36(4) ? O2b Fe1a O3a 4_456 . 1_556 116.53(4) ? O1a Fe1b O1b . . 7_546 78.59(3) ? O1a Fe1b O2a . . 6_555 85.93(3) ? O1a Fe1b O2b . . 2_556 163.49(3) ? O1a Fe1b O3b . . 7_545 96.62(4) ? O1a Fe1b O3b . . 4_456 83.59(3) ? O1b Fe1b O2a 7_546 . 6_555 87.48(4) ? O1b Fe1b O2b 7_546 . 2_556 96.72(4) ? O1b Fe1b O3b 7_546 . 7_545 156.35(3) ? O1b Fe1b O3b 7_546 . 4_456 81.59(4) ? O2a Fe1b O2b 6_555 . 2_556 78.01(3) ? O2a Fe1b O3b 6_555 . 7_545 115.48(4) ? O2a Fe1b O3b 6_555 . 4_456 166.15(4) ? O2b Fe1b O3b 2_556 . 7_545 93.76(4) ? O2b Fe1b O3b 2_556 . 4_456 111.59(2) ? O3b Fe1b O3b 7_545 . 4_456 74.84(4) ? O1a P1a O2a . . . 111.85(5) ? O1a P1a O3a . . . 113.24(5) ? O1a P1a O4 . . . 104.60(4) ? O2a P1a O3a . . . 113.17(4) ? O2a P1a O4 . . . 103.17(4) ? O3a P1a O4 . . . 109.93(6) ? O1b P1b O2b . . . 112.46(6) ? O1b P1b O3b . . . 112.18(5) ? O1b P1b O4 . . . 105.78(4) ? O2b P1b O3b . . . 111.76(4) ? O2b P1b O4 . . . 110.77(5) ? O3b P1b O4 . . . 103.34(6) ? Fe1a O1a Fe1b . . . 99.68(3) ? Fe1a O1a P1a . . . 128.53(6) ? Fe1b O1a P1a . . . 128.74(7) ? Fe1a O1b Fe1b 3_454 . 3_454 99.92(3) ? Fe1a O1b P1b 3_454 . . 128.13(7) ? Fe1b O1b P1b 3_454 . . 131.93(6) ? Fe1a O2a Fe1b 8_555 . 6_555 103.60(2) ? Fe1a O2a P1a 8_555 . . 127.94(5) ? Fe1b O2a P1a 6_555 . . 126.38(5) ? Fe1a O2b Fe1b 4_456 . 2_556 99.15(3) ? Fe1a O2b P1b 4_456 . . 113.70(5) ? Fe1b O2b P1b 2_556 . . 144.96(5) ? Fe1a O3a P1a 1_554 . . 146.26(5) ? Fe1b O3b Fe1b 3_455 . 4_456 105.16(4) ? Fe1b O3b P1b 3_455 . . 126.48(5) ? Fe1b O3b P1b 4_456 . . 126.78(6) ? P1a O4 P1b . . . 151.91(8) ? #======================================================================= # 11. STRUCTURE-FACTOR LIST loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_include_status 0 0 1 21637.70 21919.50 41.70 o 0 0 2 29133.50 25797.20 60.37 o 0 0 3 33367.00 33392.00 81.72 o 0 0 4 31418.00 31316.70 115.06 o 0 0 5 30055.40 30757.20 131.37 o 0 0 6 940.03 906.06 70.39 o 0 0 7 5359.63 5771.83 171.52 o 0 0 8 324.94 365.28 210.83 < 0 4 -6 7146.13 7083.99 146.17 o 0 4 -5 2427.01 2435.84 72.73 o 0 4 -4 577.82 615.15 45.37 o 0 4 -3 7453.87 7908.13 129.84 o 0 4 -2 1556.15 1634.50 43.37 o 0 4 -1 4214.04 4158.28 32.05 o 0 4 0 184847.00 182321.00 128.73 o 0 4 1 617.92 628.28 7.67 o 0 4 2 231517.00 234417.00 128.43 o 0 4 3 39204.10 39355.70 65.46 o 0 4 4 29158.20 29072.70 73.63 o 0 4 5 35456.80 35313.60 107.39 o 0 4 6 5955.82 5912.46 85.43 o 0 4 7 26875.20 27435.70 130.98 o 0 4 8 48.63 85.06 96.74 < 0 8 -5 99.06 88.07 83.06 < 0 8 -4 15294.00 15808.00 142.24 o 0 8 -3 3068.18 3244.40 69.40 o 0 8 -2 25517.50 26074.10 167.45 o 0 8 -1 404.18 514.74 28.36 o 0 8 1 35993.30 36741.20 49.65 o 0 8 2 8225.56 7479.23 23.05 o 0 8 3 9116.61 9352.86 43.43 o 0 8 4 27954.20 29414.20 117.83 o 0 8 5 20428.80 20292.80 74.87 o 0 8 6 49.47 197.48 63.71 o 0 8 7 9715.26 9872.58 83.11 o 0 8 8 154.93 161.12 69.05 o 0 8 9 17122.20 17485.10 243.10 o 0 12 -4 12331.10 12915.70 205.64 o 0 12 -3 382.06 450.68 78.73 o 0 12 -2 33876.20 34719.90 164.13 o 0 12 -1 18156.40 18643.10 90.85 o 0 12 0 34131.40 33302.30 130.79 o 0 12 1 13567.30 13896.80 57.78 o 0 12 2 9879.84 9585.43 51.76 o 0 12 3 138715.00 139344.00 193.85 o 0 12 4 4590.51 4628.42 44.72 o 0 12 5 727.23 930.76 29.02 o 0 12 6 3541.32 3488.25 77.08 o 0 12 7 128.06 180.80 36.36 o 0 12 8 4990.44 5046.99 79.08 o 0 12 9 6577.64 6564.48 117.80 o 0 12 10 649.25 647.51 114.76 o 0 16 -2 13524.40 13820.20 195.64 o 0 16 -1 1776.40 1920.30 72.06 o 0 16 0 17837.60 17940.10 110.54 o 0 16 1 10985.50 11175.40 103.49 o 0 16 2 37093.80 35598.40 103.03 o 0 16 3 57221.60 56282.70 108.92 o 0 16 4 3729.88 4007.57 40.71 o 0 16 5 43956.20 44490.60 183.12 o 0 16 6 33518.40 33044.60 150.82 o 0 16 7 9209.52 9302.08 92.46 o 0 16 8 7561.40 7506.15 97.12 o 0 16 9 82.33 57.38 64.05 < 0 16 10 11151.60 10694.80 152.88 o 0 20 -1 392.09 463.36 121.09 o 0 20 0 250.52 250.86 81.06 o 0 20 1 817.47 806.97 62.38 o 0 20 2 8839.45 8884.13 85.44 o 0 20 3 13098.20 13111.50 100.16 o 0 20 4 2042.22 1990.76 58.05 o 0 20 5 13421.10 13460.20 117.53 o 0 20 6 5067.59 5060.81 72.08 o 0 20 7 20737.50 21450.80 102.55 o 0 20 8 18147.60 18088.30 101.19 o 0 20 9 1993.56 1997.40 83.07 o 0 20 10 4936.28 4792.33 110.45 o 0 20 11 573.56 669.52 146.11 o 0 24 1 5108.99 5056.36 292.98 o 0 24 2 1699.61 1722.80 201.50 o 0 24 3 2679.52 2624.38 133.45 o 0 24 4 462.40 450.02 88.07 o 0 24 5 387.12 368.28 71.05 o 0 24 6 1360.18 1430.52 66.72 o 0 24 7 1723.45 1693.11 67.72 o 0 24 8 1253.49 1212.33 66.39 o 0 24 9 1374.36 1350.12 65.39 o 0 24 10 2391.79 2350.43 106.43 o 0 24 11 766.32 757.27 118.43 o 0 28 4 7693.42 7424.04 330.40 o 0 28 5 12094.70 11923.00 226.34 o 0 28 6 9006.88 8449.22 222.29 o 0 28 7 49.45 82.06 92.40 < 0 28 8 2897.29 2750.53 110.10 o 0 28 9 3875.50 3776.37 85.42 o 0 28 10 1137.63 1096.23 97.75 o 1 -31 -8 7983.04 7521.65 299.70 o 1 -31 -7 22.07 -14.34 219.50 < 1 -27 -10 206.84 155.79 83.40 < 1 -27 -9 9632.18 9323.71 117.16 o 1 -27 -8 1859.31 1851.59 77.07 o 1 -27 -7 109.60 74.06 79.06 < 1 -27 -6 12727.70 12986.30 193.96 o 1 -27 -5 40.69 19.35 101.74 < 1 -27 -4 862.41 813.65 124.10 o 1 -27 -3 180.07 172.46 243.85 < 1 -23 -10 2026.43 2034.10 91.41 o 1 -23 -9 4248.89 4150.15 85.09 o 1 -23 -8 2945.75 3036.14 64.06 o 1 -23 -7 65.45 97.41 49.70 < 1 -23 -6 6153.40 6291.75 81.76 o 1 -23 -5 455.30 551.43 54.38 o 1 -23 -4 4218.28 4406.75 103.77 o 1 -23 -3 261.05 274.54 69.05 o 1 -23 -2 79.01 138.44 94.07 < 1 -23 -1 13.47 -16.35 103.41 < 1 -19 -10 8174.39 7809.01 143.18 o 1 -19 -9 215.63 225.17 78.39 o 1 -19 -8 22127.50 22381.10 155.66 o 1 -19 -7 197.63 171.46 43.37 o 1 -19 -6 226.04 243.18 40.03 o 1 -19 -5 5614.63 5615.41 59.40 o 1 -19 -4 1368.30 1400.85 40.37 o 1 -19 -3 2459.28 2575.68 61.39 o 1 -19 -2 2574.05 2669.43 59.39 o 1 -19 -1 556.16 497.39 51.37 o 1 -19 0 581.99 591.13 65.05 o 1 -19 1 704.85 704.22 83.40 o 1 -15 -10 6703.79 6430.75 162.52 o 1 -15 -9 3462.23 3328.84 97.09 o 1 -15 -8 23752.40 23808.40 138.31 o 1 -15 -7 2289.82 2287.06 47.38 o 1 -15 -6 13990.20 13851.60 146.26 o 1 -15 -5 7525.14 8042.06 155.88 o 1 -15 -4 14.87 18.01 20.68 < 1 -15 -3 17128.00 17398.70 63.48 o 1 -15 -2 832.56 869.71 25.35 o 1 -15 -1 1673.87 1764.20 49.71 o 1 -15 0 2676.53 2793.91 60.72 o 1 -15 1 193.42 175.13 54.04 o 1 -15 2 1175.92 1249.02 76.73 o 1 -15 3 1028.70 1084.54 97.41 o 1 -11 -10 12.35 21.68 140.10 < 1 -11 -9 28.15 -18.35 89.73 < 1 -11 -8 6383.73 6300.81 93.11 o 1 -11 -7 2617.07 2591.72 47.71 o 1 -11 -6 10444.30 10721.60 115.51 o 1 -11 -5 1318.49 1476.95 28.02 o 1 -11 -4 3069.41 2955.88 40.38 o 1 -11 -3 29013.90 29099.50 144.63 o 1 -11 -2 1891.28 1817.78 31.03 o 1 -11 -1 7267.21 7432.42 53.08 o 1 -11 0 2531.80 2545.15 39.37 o 1 -11 1 2.59 6.34 43.03 < 1 -11 2 3061.21 3161.99 62.06 o 1 -11 3 2263.41 2401.45 65.39 o 1 -11 4 31.90 70.39 78.06 < 1 -7 -9 2448.87 2314.07 150.80 o 1 -7 -8 1045.63 916.07 109.75 o 1 -7 -7 535.96 568.11 50.37 o 1 -7 -6 3.81 29.36 52.04 < 1 -7 -5 1298.21 1228.73 30.69 o 1 -7 -4 522.63 526.09 23.35 o 1 -7 -3 10005.90 10677.50 43.43 o 1 -7 -2 3627.81 3794.91 27.04 o 1 -7 -1 7410.41 7326.04 26.73 o 1 -7 0 4194.06 4276.90 37.38 o 1 -7 1 1481.64 1558.42 38.37 o 1 -7 2 3811.29 3661.93 71.74 o 1 -7 3 1288.86 1342.79 61.05 o 1 -7 4 2286.94 2292.37 73.06 o 1 -7 5 5526.08 5874.33 120.46 o 1 -7 6 2121.41 2186.92 115.10 o 1 -3 -8 3815.91 3704.29 167.50 o 1 -3 -7 3566.14 3658.51 83.41 o 1 -3 -6 8965.35 9142.42 95.13 o 1 -3 -5 13021.10 13010.60 90.16 o 1 -3 -4 2811.34 2739.81 34.70 o 1 -3 -3 210.61 142.78 16.35 o 1 -3 -2 5975.56 5939.83 22.05 o 1 -3 -1 61.68 62.05 10.67 o 1 -3 0 3685.96 3598.70 17.70 o 1 -3 1 522.37 442.71 18.02 o 1 -3 2 1563.96 1531.79 22.02 o 1 -3 3 500.52 480.38 25.02 o 1 -3 4 137.89 139.44 41.03 o 1 -3 5 2577.89 2669.43 69.06 o 1 -3 6 3123.54 3398.17 138.80 o 1 -3 7 1552.30 1611.02 123.10 o 1 1 -7 2398.52 2602.65 159.14 o 1 1 -6 3795.90 3749.99 100.76 o 1 1 -5 9467.47 9549.30 113.15 o 1 1 -4 11988.80 11665.50 122.20 o 1 1 -3 6696.03 6666.16 69.10 o 1 1 -2 3895.99 3755.29 35.71 o 1 1 -1 7363.66 7308.71 49.46 o 1 1 0 1215.48 1240.22 15.69 o 1 1 1 616.85 611.32 7.34 o 1 1 2 1364.89 1284.69 17.35 o 1 1 3 605.22 617.18 20.35 o 1 1 4 3244.47 3166.68 36.71 o 1 1 5 653.13 638.84 45.04 o 1 1 6 55.30 63.05 43.70 < 1 1 7 58.05 49.37 68.72 < 1 1 8 0.22 58.38 143.77 < 1 5 -6 608.01 567.44 102.75 o 1 5 -5 1629.93 1604.69 89.08 o 1 5 -4 949.37 995.47 58.38 o 1 5 -3 542.36 583.79 40.03 o 1 5 -2 6183.64 6014.33 54.74 o 1 5 -1 7587.01 7897.98 59.77 o 1 5 0 111.40 174.13 15.01 o 1 5 1 5484.04 5438.99 14.70 o 1 5 2 7442.16 7102.06 27.41 o 1 5 3 21.26 32.36 11.68 o 1 5 4 17846.30 17527.80 54.49 o 1 5 5 1050.02 1062.23 31.69 o 1 5 6 4240.07 4235.78 69.74 o 1 5 7 7196.99 7131.19 96.11 o 1 5 8 3905.87 4099.02 115.78 o 1 5 9 2363.36 2342.75 148.13 o 1 9 -5 59.74 85.73 90.40 < 1 9 -4 19.46 10.01 94.40 < 1 9 -3 1521.26 1587.67 65.39 o 1 9 -2 105.17 102.74 47.37 o 1 9 -1 322.25 307.24 59.05 o 1 9 0 2078.23 1980.90 26.36 o 1 9 1 3651.14 3856.71 21.36 o 1 9 2 10954.60 11345.60 24.06 o 1 9 3 2060.43 2046.15 19.35 o 1 9 4 13858.60 13786.20 60.48 o 1 9 5 10.45 24.69 23.68 < 1 9 6 8934.37 8689.66 110.49 o 1 9 7 4143.44 4150.92 61.06 o 1 9 8 5170.42 5136.12 81.42 o 1 9 9 12665.70 12591.60 162.58 o 1 9 10 2619.70 2518.28 157.48 o 1 13 -3 2785.50 2843.26 113.10 o 1 13 -2 516.01 549.43 64.05 o 1 13 -1 5771.96 5935.61 67.74 o 1 13 0 138.74 186.81 38.70 o 1 13 1 1493.23 1344.17 27.69 o 1 13 2 360.55 407.65 18.35 o 1 13 3 6428.46 6489.79 30.71 o 1 13 4 6580.55 6533.58 44.73 o 1 13 5 2911.78 3081.80 37.70 o 1 13 6 2519.71 2643.51 70.07 o 1 13 7 343.43 378.29 35.36 o 1 13 8 2181.77 2060.49 62.05 o 1 13 9 6526.01 6522.75 105.12 o 1 13 10 23.94 46.70 81.39 < 1 17 -2 2401.93 2297.72 142.46 o 1 17 -1 2657.72 2644.73 108.43 o 1 17 0 1283.31 1309.75 65.72 o 1 17 1 9546.51 9741.19 90.12 o 1 17 2 19.28 -3.34 44.70 < 1 17 3 661.36 720.91 31.69 o 1 17 4 509.61 566.11 25.35 o 1 17 5 8546.26 8477.90 103.48 o 1 17 6 17.25 33.36 37.36 < 1 17 7 9095.37 9546.66 79.11 o 1 17 8 56.40 18.01 51.37 < 1 17 9 37.61 61.71 56.04 < 1 17 10 5110.92 5127.07 99.10 o 1 17 11 667.89 796.96 202.83 o 1 21 0 118.37 77.06 114.09 < 1 21 1 3656.13 3827.69 111.11 o 1 21 2 4362.88 4480.85 92.43 o 1 21 3 2636.35 2606.03 71.06 o 1 21 4 208.01 204.15 60.71 o 1 21 5 5279.12 5317.11 91.43 o 1 21 6 303.54 326.25 41.70 o 1 21 7 11731.00 11865.30 85.79 o 1 21 8 99.54 114.75 42.70 o 1 21 9 6858.76 6899.32 115.13 o 1 21 10 8578.58 8307.48 140.84 o 1 21 11 772.28 735.58 94.41 o 1 25 2 2094.99 2001.42 245.21 o 1 25 3 2968.89 2985.43 172.49 o 1 25 4 2382.13 2358.43 138.79 o 1 25 5 42.53 -10.34 84.73 < 1 25 6 746.39 818.31 88.07 o 1 25 7 5536.73 5618.39 96.10 o 1 25 8 36.18 40.03 53.37 < 1 25 9 6503.89 6634.87 95.78 o 1 25 10 1715.64 1578.34 99.08 o 1 25 11 4536.61 4106.88 117.79 o 1 29 5 589.17 635.83 149.12 o 1 29 6 100.07 170.79 128.43 < 1 29 7 525.72 581.79 125.10 o 1 29 8 2465.72 2338.43 129.12 o 1 29 9 726.64 776.28 104.08 o 1 29 10 262.95 192.81 140.44 < 2 -30 -9 2141.26 2064.48 144.46 o 2 -30 -8 2353.64 2502.23 163.15 o 2 -30 -7 1198.98 1090.23 112.43 o 2 -30 -6 2253.72 2190.60 165.15 o 2 -30 -5 339.93 266.87 215.16 < 2 -26 -10 237.84 241.18 73.39 o 2 -26 -9 4521.72 4361.11 95.43 o 2 -26 -8 7086.10 7228.46 110.80 o 2 -26 -7 12120.80 12302.40 165.91 o 2 -26 -6 10191.90 10776.60 157.21 o 2 -26 -5 3857.77 3796.71 114.78 o 2 -26 -4 9271.39 9332.15 198.59 o 2 -26 -3 5321.44 5124.14 178.86 o 2 -26 -2 9753.80 9292.50 240.99 o 2 -22 -10 312.56 270.21 82.40 o 2 -22 -9 4295.86 4097.44 99.77 o 2 -22 -8 845.34 908.39 57.38 o 2 -22 -7 7240.99 7267.33 80.43 o 2 -22 -6 14423.40 14638.20 107.85 o 2 -22 -5 12771.80 13060.90 97.15 o 2 -22 -4 7365.14 7465.00 81.43 o 2 -22 -3 5187.68 5195.86 83.42 o 2 -22 -2 32276.10 31729.40 164.11 o 2 -22 -1 10540.60 10492.80 143.53 o 2 -22 0 4456.17 4175.25 186.52 o 2 -18 -10 972.64 947.10 113.43 o 2 -18 -9 12.50 11.34 67.38 < 2 -18 -8 7557.70 7519.42 93.11 o 2 -18 -7 3727.07 3960.58 70.40 o 2 -18 -6 2632.09 2721.19 50.05 o 2 -18 -5 41.97 -7.67 52.71 < 2 -18 -4 764.63 783.96 47.37 o 2 -18 -3 5207.21 5230.86 58.73 o 2 -18 -2 16970.90 16707.40 96.18 o 2 -18 -1 87.63 83.06 38.36 o 2 -18 0 9830.70 10180.70 86.45 o 2 -18 1 13283.20 13623.00 112.84 o 2 -18 2 3859.74 3953.88 134.46 o 2 -14 -10 106.60 140.10 111.08 < 2 -14 -9 5977.37 5979.60 128.14 o 2 -14 -8 20364.90 20220.90 130.93 o 2 -14 -7 581.98 634.83 44.03 o 2 -14 -6 23422.50 23798.20 125.98 o 2 -14 -5 5447.42 5611.77 128.15 o 2 -14 -4 43654.50 43154.50 113.88 o 2 -14 -3 10700.30 10700.30 54.76 o 2 -14 -2 193.77 179.47 26.35 o 2 -14 -1 6817.98 6658.34 63.42 o 2 -14 0 556.66 612.15 49.71 o 2 -14 1 4109.97 4229.60 65.73 o 2 -14 2 626.37 699.55 62.38 o 2 -14 3 9584.53 9747.56 121.83 o 2 -10 -9 2653.53 2796.53 146.13 o 2 -10 -8 1926.97 1882.29 72.40 o 2 -10 -7 1948.95 1894.98 57.05 o 2 -10 -6 53678.90 54122.80 211.99 o 2 -10 -5 606.76 652.52 27.69 o 2 -10 -4 60281.80 58784.60 128.28 o 2 -10 -3 65947.70 67183.20 218.03 o 2 -10 -2 71493.20 72479.50 124.31 o 2 -10 -1 58021.00 53812.20 120.29 o 2 -10 0 5856.16 5772.80 47.40 o 2 -10 1 71702.10 71194.10 290.29 o 2 -10 2 2314.03 2368.48 68.40 o 2 -10 3 2770.37 2869.30 63.06 o 2 -10 4 6988.58 7403.62 117.14 o 2 -10 5 44.76 51.71 80.39 < 2 -6 -9 1378.77 1217.34 211.84 o 2 -6 -8 805.00 801.97 101.75 o 2 -6 -7 201.15 221.17 53.71 o 2 -6 -6 3528.50 3500.11 105.10 o 2 -6 -5 1371.76 1323.80 35.36 o 2 -6 -4 89225.00 88059.60 125.62 o 2 -6 -3 17534.30 18166.30 53.51 o 2 -6 -1 64345.80 63182.60 92.74 o 2 -6 0 132295.00 138206.00 130.88 o 2 -6 1 214388.00 206807.00 250.44 o 2 -6 2 347.21 385.97 30.36 o 2 -6 3 38793.20 39187.60 151.56 o 2 -6 4 27020.30 28125.90 157.39 o 2 -6 5 8668.25 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158.64 o 2 22 5 21197.00 21513.10 139.96 o 2 22 6 21748.40 21982.30 110.90 o 2 22 7 8675.28 8896.42 107.14 o 2 22 8 1177.22 1107.24 49.71 o 2 22 9 17715.30 17926.10 135.91 o 2 22 10 3757.07 3690.59 82.08 o 2 22 11 66.83 50.70 79.06 < 2 26 3 306.35 267.54 281.88 < 2 26 4 2779.52 2869.29 279.26 o 2 26 5 6621.45 6413.33 215.25 o 2 26 6 16044.80 16430.00 196.34 o 2 26 7 10657.60 10397.40 201.28 o 2 26 8 3911.62 3992.91 104.44 o 2 26 9 11202.30 11080.40 158.23 o 2 26 10 5857.88 5837.76 146.16 o 2 26 11 9567.04 9196.95 197.60 o 2 30 6 13.15 29.36 153.78 < 2 30 7 391.23 461.36 125.10 o 2 30 8 808.19 750.26 152.12 o 2 30 9 3046.76 2956.09 171.16 o 3 -29 -9 3089.44 2986.13 91.42 o 3 -29 -8 357.06 396.30 83.73 o 3 -29 -7 4953.32 5047.61 125.13 o 3 -29 -6 583.06 595.47 108.08 o 3 -29 -5 1885.89 1807.56 133.78 o 3 -29 -4 837.69 645.52 145.45 o 3 -25 -10 1867.69 1752.51 82.40 o 3 -25 -9 13504.00 13187.20 110.17 o 3 -25 -8 1451.51 1391.16 79.40 o 3 -25 -7 20594.50 20382.70 207.41 o 3 -25 -6 82.94 120.09 64.72 < 3 -25 -5 3596.90 3565.76 103.77 o 3 -25 -4 3131.67 3301.75 105.43 o 3 -25 -3 1224.97 1177.96 117.76 o 3 -25 -2 1526.66 1436.87 129.77 o 3 -25 -1 353.87 280.88 148.11 < 3 -21 -10 3529.63 3477.34 116.78 o 3 -21 -9 9327.12 9219.36 130.50 o 3 -21 -8 1385.23 1365.47 69.72 o 3 -21 -7 26750.40 27413.40 174.42 o 3 -21 -6 564.90 586.79 48.04 o 3 -21 -5 15727.40 16106.80 108.19 o 3 -21 -4 1022.04 1067.20 57.38 o 3 -21 -3 1179.55 1160.62 54.38 o 3 -21 -2 9672.25 9628.87 121.50 o 3 -21 -1 1758.51 1680.10 96.75 o 3 -21 0 194.04 206.49 91.07 o 3 -21 1 221.19 204.49 128.76 < 3 -17 -10 77.70 64.05 124.76 < 3 -17 -9 1006.17 1006.48 82.40 o 3 -17 -8 129.34 131.10 62.71 o 3 -17 -7 10770.20 11334.60 127.85 o 3 -17 -6 32.85 28.35 44.03 < 3 -17 -5 8484.76 8589.51 104.14 o 3 -17 -4 129.09 91.40 45.37 o 3 -17 -3 7249.94 7090.23 55.74 o 3 -17 -2 6991.53 6669.68 91.45 o 3 -17 -1 1554.85 1641.73 55.38 o 3 -17 0 4681.54 4817.00 59.06 o 3 -17 1 1537.60 1536.29 65.05 o 3 -17 2 100.17 92.74 71.72 < 3 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618.15 59.38 o 3 3 -3 5559.69 5806.15 170.87 o 3 3 -2 10424.10 10247.00 65.12 o 3 3 -1 1681.86 1701.33 38.70 o 3 3 0 3227.59 3756.31 23.70 o 3 3 1 214.54 224.51 9.67 o 3 3 2 150.52 172.47 10.68 o 3 3 3 2400.79 2411.77 17.69 o 3 3 4 637.07 676.22 19.68 o 3 3 5 3208.40 3229.97 47.38 o 3 3 6 62.74 67.72 42.70 < 3 3 7 1884.68 1909.65 59.38 o 3 3 8 2105.28 2344.38 143.79 o 3 3 9 4823.05 4520.71 171.18 o 3 7 -5 12185.30 12681.90 196.63 o 3 7 -4 2471.84 2760.47 101.09 o 3 7 -3 7246.23 7416.59 108.13 o 3 7 -2 8012.55 8276.97 76.77 o 3 7 -1 9900.56 9911.80 63.77 o 3 7 0 7382.18 6943.06 61.10 o 3 7 1 1283.86 1356.27 12.34 o 3 7 2 814.86 734.65 10.01 o 3 7 3 730.14 711.61 18.02 o 3 7 4 3272.52 3302.20 38.38 o 3 7 5 3323.16 3201.46 31.03 o 3 7 6 4341.67 4494.23 59.40 o 3 7 7 344.01 353.94 40.70 o 3 7 8 250.33 264.87 60.05 o 3 7 9 1064.91 1139.59 102.08 o 3 11 -4 219.16 174.47 98.41 < 3 11 -3 8438.79 8591.09 162.54 o 3 11 -2 4302.17 4494.87 73.74 o 3 11 -1 1942.59 1914.34 50.04 o 3 11 0 2207.22 2346.48 43.04 o 3 11 1 1625.69 1598.76 26.02 o 3 11 2 13824.90 13293.80 39.75 o 3 11 3 216.67 213.50 12.34 o 3 11 4 1104.63 1029.23 21.69 o 3 11 5 837.82 785.32 25.69 o 3 11 6 12027.80 12281.80 111.19 o 3 11 7 23.78 18.68 33.02 < 3 11 8 6417.28 6519.50 76.42 o 3 11 9 26.58 7.01 60.38 < 3 11 10 2473.51 2501.91 108.10 o 3 15 -2 704.84 613.82 91.07 o 3 15 -1 1280.48 1314.75 90.41 o 3 15 0 729.31 800.63 66.72 o 3 15 1 1398.85 1399.17 44.04 o 3 15 2 2805.41 2976.84 38.37 o 3 15 3 816.00 783.30 21.02 o 3 15 4 6053.80 5947.82 35.38 o 3 15 5 724.94 799.98 25.02 o 3 15 6 8320.87 8007.47 109.15 o 3 15 7 72.28 63.05 33.69 < 3 15 8 10163.30 10122.80 94.47 o 3 15 9 373.89 388.96 53.37 o 3 15 10 7601.32 7477.99 140.17 o 3 15 11 4406.15 4310.72 116.79 o 3 19 -1 471.65 394.97 206.83 < 3 19 0 1519.06 1559.64 89.07 o 3 19 1 1419.38 1329.77 87.07 o 3 19 2 1103.75 1131.25 59.72 o 3 19 3 5035.46 5057.74 75.75 o 3 19 4 3484.89 3594.52 77.74 o 3 19 5 3388.86 3517.77 52.72 o 3 19 6 764.45 798.64 41.03 o 3 19 7 233.37 268.54 34.36 o 3 19 8 7336.43 7380.22 95.11 o 3 19 9 381.66 383.30 58.71 o 3 19 10 3821.54 3722.96 89.75 o 3 19 11 1759.13 1798.87 91.41 o 3 23 1 4597.38 4685.82 253.59 o 3 23 2 14.39 -40.70 114.08 < 3 23 3 1376.41 1337.11 118.10 o 3 23 4 2050.05 2202.58 96.08 o 3 23 5 8207.55 8494.23 117.81 o 3 23 6 4531.63 4779.22 96.43 o 3 23 7 1.98 0.67 47.37 < 3 23 8 38.03 31.02 52.37 < 3 23 9 4789.43 4829.32 82.75 o 3 23 10 581.71 651.51 66.05 o 3 23 11 220.81 239.18 89.07 o 3 27 4 373.88 234.51 272.54 < 3 27 5 1333.62 1267.38 138.45 o 3 27 6 5217.09 5190.17 192.54 o 3 27 7 3026.74 3296.39 152.14 o 3 27 8 1389.72 1297.74 133.78 o 3 27 9 6794.01 6794.52 119.14 o 3 27 10 201.96 201.82 130.43 < 3 27 11 4209.23 3369.05 204.21 o 4 -28 -9 143.84 171.13 78.39 o 4 -28 -8 84.44 62.71 82.40 < 4 -28 -7 7.59 -2.34 79.06 < 4 -28 -6 6106.94 6079.44 120.80 o 4 -28 -5 5507.78 5383.47 150.50 o 4 -28 -4 654.65 639.50 120.09 o 4 -28 -3 2901.56 2076.92 199.52 o 4 -24 -10 1646.57 1644.06 90.08 o 4 -24 -9 456.29 451.35 81.06 o 4 -24 -8 977.83 1016.48 66.72 o 4 -24 -7 4601.66 4398.83 86.42 o 4 -24 -6 9.49 29.36 55.37 < 4 -24 -5 3457.91 3414.93 107.44 o 4 -24 -4 23.77 39.36 60.04 < 4 -24 -3 217.69 255.53 74.06 o 4 -24 -2 76.49 55.04 88.07 < 4 -24 -1 1069.32 1032.50 114.43 o 4 -20 -10 806.74 752.93 116.43 o 4 -20 -9 2721.75 2565.67 94.75 o 4 -20 -8 7854.70 7931.33 134.16 o 4 -20 -7 6402.10 6407.32 90.10 o 4 -20 -6 103.39 160.12 52.04 o 4 -20 -5 31155.90 31509.40 141.06 o 4 -20 -4 7952.66 7998.20 91.78 o 4 -20 -3 18725.30 19103.20 152.63 o 4 -20 -2 3529.03 3438.99 69.73 o 4 -20 -1 962.90 853.35 64.05 o 4 -20 0 6618.88 6790.76 122.14 o 4 -20 1 1140.17 1168.62 111.09 o 4 -16 -10 1534.86 1470.24 120.77 o 4 -16 -9 212.43 256.86 88.73 o 4 -16 -8 1331.28 1327.76 89.07 o 4 -16 -7 4598.58 4588.76 82.42 o 4 -16 -6 4609.82 4547.84 104.11 o 4 -16 -5 23390.60 23635.90 123.31 o 4 -16 -3 74882.40 75538.40 184.58 o 4 -16 -2 24959.10 24001.20 114.31 o 4 -16 -1 15003.40 14597.50 91.83 o 4 -16 0 16137.50 15855.50 107.53 o 4 -16 1 11030.20 11212.30 107.49 o 4 -16 2 23244.90 23324.80 158.00 o 4 -16 3 1199.93 1329.42 104.08 o 4 -12 -9 1944.26 1740.84 148.46 o 4 -12 -8 289.53 233.18 97.74 o 4 -12 -7 1895.17 1937.01 60.72 o 4 -12 -6 39.41 52.04 41.70 < 4 -12 -5 1897.28 1992.79 66.39 o 4 -12 -4 414.64 514.74 37.36 o 4 -12 -3 56808.40 55867.60 140.94 o 4 -12 -2 3633.55 3509.65 48.05 o 4 -12 -1 15217.70 15284.70 69.49 o 4 -12 0 37821.20 36642.00 140.90 o 4 -12 1 21210.80 20724.40 111.93 o 4 -12 2 20366.80 20627.90 127.60 o 4 -12 3 603.57 624.82 64.38 o 4 -12 4 25294.40 26614.60 222.50 o 4 -8 -8 832.39 797.97 103.08 o 4 -8 -7 5132.70 4994.28 92.10 o 4 -8 -6 1754.06 1854.27 61.39 o 4 -8 -5 25324.30 25442.40 122.00 o 4 -8 -4 11608.10 12086.00 62.78 o 4 -8 -3 10018.90 10292.40 62.12 o 4 -8 -2 59834.40 60287.60 143.03 o 4 -8 -1 1912.54 2164.58 29.03 o 4 -8 0 6704.22 6266.58 36.39 o 4 -8 1 1352.63 1327.85 48.38 o 4 -8 2 15113.90 15063.10 227.12 o 4 -8 3 895.97 932.09 47.04 o 4 -8 4 11301.50 12098.90 108.16 o 4 -8 5 29.44 30.69 70.39 < 4 -8 6 10762.40 11183.40 192.27 o 4 -4 -8 780.28 734.58 147.12 o 4 -4 -7 13062.90 13193.80 214.66 o 4 -4 -6 42.81 77.06 60.38 < 4 -4 -5 18062.90 18102.60 118.24 o 4 -4 -4 7213.15 7190.48 49.73 o 4 -4 -3 40770.90 40089.00 79.09 o 4 -4 -2 126630.00 124295.00 128.95 o 4 -4 -1 1996.78 1908.24 19.36 o 4 -4 0 128389.00 127686.00 125.67 o 4 -4 1 60148.00 61610.60 80.57 o 4 -4 2 15193.20 13855.80 46.79 o 4 -4 3 30639.50 30993.80 91.33 o 4 -4 4 237.56 389.96 54.37 o 4 -4 5 14940.90 15639.50 122.54 o 4 -4 6 3813.72 3854.42 107.77 o 4 -4 7 1141.01 1074.21 92.41 o 4 0 -7 4009.80 4096.06 173.84 o 4 0 -6 1870.67 1856.59 128.78 o 4 0 -5 13368.00 13562.00 138.89 o 4 0 -4 53.35 105.08 65.38 < 4 0 -3 12494.40 12561.30 65.12 o 4 0 -2 19953.30 18839.60 62.53 o 4 0 -1 55378.00 56396.30 107.43 o 4 0 0 329727.00 355077.00 264.16 o 4 0 1 2526.11 2070.67 21.70 o 4 0 2 28067.90 23565.20 43.27 o 4 0 3 172572.00 178809.00 144.38 o 4 0 4 49079.70 46949.80 102.56 o 4 0 5 41273.40 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1448.88 59.38 o 5 21 5 2479.10 2383.81 65.73 o 5 21 6 4304.43 4344.74 71.41 o 5 21 7 2609.29 2647.40 55.05 o 5 21 8 2449.26 2505.24 61.72 o 5 21 9 7006.45 7153.68 109.79 o 5 21 10 3374.60 3201.37 86.08 o 5 21 11 54.37 87.07 77.39 < 5 25 4 294.35 349.27 213.83 < 5 25 5 26.89 32.02 114.42 < 5 25 6 2370.70 2353.42 98.09 o 5 25 7 4456.76 4559.28 111.45 o 5 25 8 2194.13 2228.62 80.74 o 5 25 9 3548.57 3420.61 143.80 o 5 25 10 196.05 224.50 85.06 o 5 25 11 1455.54 1482.91 96.08 o 5 29 7 715.17 700.89 160.46 o 5 29 8 1136.09 1233.01 260.88 o 5 29 9 2382.23 2387.13 237.54 o 6 -30 -8 521.20 491.72 129.43 o 6 -30 -7 3270.48 3031.20 115.44 o 6 -30 -6 2336.92 2264.68 135.79 o 6 -30 -5 1208.90 1094.56 152.79 o 6 -26 -9 3333.38 3365.86 98.76 o 6 -26 -8 2311.07 2368.76 96.75 o 6 -26 -7 2126.07 2048.46 76.07 o 6 -26 -6 1638.01 1554.65 100.75 o 6 -26 -5 4704.27 4745.21 107.44 o 6 -26 -4 14712.10 14202.10 188.97 o 6 -26 -3 4803.49 4605.77 129.47 o 6 -26 -2 5770.48 5718.61 152.84 o 6 -22 -9 479.96 516.73 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111.43 o 8 -28 -5 3.27 16.01 84.73 < 8 -28 -4 7.99 68.72 99.41 < 8 -28 -3 1990.99 1873.63 119.10 o 8 -24 -9 388.86 278.88 116.42 o 8 -24 -8 397.83 419.99 82.40 o 8 -24 -7 3905.74 3809.40 83.08 o 8 -24 -6 12.62 54.71 62.38 < 8 -24 -5 1936.01 1911.65 67.72 o 8 -24 -4 813.42 801.64 63.05 o 8 -24 -3 584.91 562.77 71.06 o 8 -24 -2 926.11 888.71 83.40 o 8 -24 -1 161.45 165.79 84.40 < 8 -24 0 154.36 175.80 214.83 < 8 -20 -9 48.20 32.69 94.74 < 8 -20 -8 575.81 599.80 88.40 o 8 -20 -7 33.77 61.38 64.71 < 8 -20 -6 299.80 285.22 65.05 o 8 -20 -5 19465.80 19210.70 140.94 o 8 -20 -4 2846.13 2885.01 64.39 o 8 -20 -3 2822.39 2962.40 67.40 o 8 -20 -2 6739.26 6468.86 94.44 o 8 -20 -1 6082.39 6071.10 98.44 o 8 -20 0 16867.20 16006.40 184.66 o 8 -20 1 86.66 82.40 73.72 < 8 -20 2 3305.16 3200.04 139.80 o 8 -16 -9 929.57 725.58 147.12 o 8 -16 -8 1082.71 976.79 89.41 o 8 -16 -7 90.51 62.71 90.40 < 8 -16 -6 327.17 349.93 54.04 o 8 -16 -5 4351.33 4385.87 74.08 o 8 -16 -4 24.97 49.70 53.37 < 8 -16 -3 24686.00 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497.23 455.36 34.36 o 8 -8 3 10885.60 10731.60 90.47 o 8 -8 4 10695.00 10872.80 109.15 o 8 -8 5 4.96 3.34 65.05 < 8 -8 6 3724.97 3695.92 150.15 o 8 -4 -7 2110.14 2081.16 125.78 o 8 -4 -6 635.89 721.90 122.76 o 8 -4 -5 3702.30 3760.32 99.43 o 8 -4 -4 1512.15 1623.71 51.04 o 8 -4 -3 3308.63 3367.40 46.05 o 8 -4 -2 56248.70 55398.30 122.08 o 8 -4 -1 1574.74 1931.79 43.04 o 8 -4 0 110710.00 114815.00 154.98 o 8 -4 1 30091.80 29819.90 82.04 o 8 -4 2 30677.90 28127.80 73.97 o 8 -4 3 23376.20 23198.20 72.87 o 8 -4 4 3275.97 2975.95 55.05 o 8 -4 5 29462.00 29422.40 138.37 o 8 -4 6 46.12 45.70 58.38 < 8 -4 7 1989.89 1904.98 85.07 o 8 0 -6 1567.83 1362.48 124.44 o 8 0 -5 834.77 796.30 96.41 o 8 0 -4 666.42 637.50 70.06 o 8 0 -3 2827.17 2891.05 77.07 o 8 0 -2 13082.80 13131.40 83.48 o 8 0 -1 1458.95 1405.92 34.70 o 8 0 0 83920.60 87087.00 348.44 o 8 0 1 457.75 677.88 23.69 o 8 0 2 86242.10 84941.40 125.52 o 8 0 3 74578.30 73131.10 115.06 o 8 0 4 26488.70 24889.20 80.93 o 8 0 5 26582.90 27393.70 128.02 o 8 0 6 2851.78 2791.60 51.05 o 8 0 7 50294.10 51638.20 175.33 o 8 0 8 8640.18 8672.31 116.48 o 8 4 -5 795.20 673.20 106.08 o 8 4 -4 2084.73 2078.81 89.74 o 8 4 -3 28.10 57.71 58.38 < 8 4 -2 2929.14 2811.31 73.40 o 8 4 -1 1161.59 1198.34 72.39 o 8 4 0 19208.50 19353.50 81.54 o 8 4 1 38132.80 39247.00 121.61 o 8 4 2 18266.10 18497.30 74.22 o 8 4 3 6392.78 5986.73 75.45 o 8 4 4 19549.70 18857.80 62.84 o 8 4 5 13696.10 13965.50 54.77 o 8 4 6 1344.52 1296.09 44.37 o 8 4 7 42743.60 43741.50 152.87 o 8 4 8 2779.27 2874.63 78.07 o 8 4 9 11282.70 11430.00 145.21 o 8 8 -3 6.76 11.34 71.39 < 8 8 -2 6517.60 6810.42 81.43 o 8 8 -1 1118.06 1170.29 48.71 o 8 8 0 6247.90 6235.11 64.41 o 8 8 1 44616.50 45658.00 154.68 o 8 8 2 3693.32 3627.30 33.70 o 8 8 3 22628.40 21786.70 84.92 o 8 8 4 8106.23 8078.53 40.40 o 8 8 5 6521.72 6425.24 52.40 o 8 8 6 982.83 1069.55 56.71 o 8 8 7 11019.90 11496.90 113.84 o 8 8 8 4209.24 4246.61 82.08 o 8 8 9 5034.93 5161.07 101.44 o 8 8 10 551.04 502.06 117.76 o 8 12 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1135.93 43.70 o 8 20 7 925.18 923.07 46.04 o 8 20 8 1642.23 1670.08 57.72 o 8 20 9 5860.33 6028.28 72.08 o 8 20 10 21360.60 22446.10 180.70 o 8 20 11 1520.96 1565.31 84.40 o 8 24 4 5490.06 5685.48 172.52 o 8 24 5 1140.43 1220.66 139.11 o 8 24 6 6463.55 6378.23 167.86 o 8 24 7 1201.73 1118.25 125.77 o 8 24 8 2671.38 2680.43 105.43 o 8 24 9 753.43 756.60 74.73 o 8 24 10 4.25 -2.34 76.39 < 8 24 11 0.24 -36.36 102.08 < 8 28 7 5394.57 4933.65 229.58 o 8 28 8 13741.20 13286.50 235.37 o 8 28 9 6508.26 6356.28 199.90 o 9 -27 -8 1227.14 1175.97 86.07 o 9 -27 -7 629.02 587.79 82.06 o 9 -27 -6 8810.84 8679.10 146.52 o 9 -27 -5 337.86 296.89 76.73 o 9 -27 -4 8672.04 8664.69 127.50 o 9 -27 -3 3302.05 3218.05 128.12 o 9 -27 -2 2778.84 2551.67 158.15 o 9 -23 -9 218.84 244.85 212.49 < 9 -23 -8 6153.92 6295.04 199.89 o 9 -23 -7 1280.88 1351.45 88.74 o 9 -23 -6 75.31 134.10 61.38 o 9 -23 -5 6461.86 6626.85 92.44 o 9 -23 -4 1531.36 1613.02 64.05 o 9 -23 -3 3.39 42.70 61.38 < 9 -23 -2 2228.84 2102.85 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72.06 o 9 -11 -5 3188.10 3074.59 82.08 o 9 -11 -4 2890.98 2902.43 64.06 o 9 -11 -3 7424.64 7551.43 100.80 o 9 -11 -2 111.25 83.06 36.03 o 9 -11 -1 37589.60 38656.90 149.27 o 9 -11 0 7110.16 7338.15 70.09 o 9 -11 1 13518.70 12325.80 86.49 o 9 -11 2 1337.51 1179.32 66.39 o 9 -11 3 807.13 611.49 73.73 o 9 -11 4 4828.88 4881.06 133.80 o 9 -11 5 6.85 16.68 82.39 < 9 -7 -7 6987.79 6652.46 178.88 o 9 -7 -6 7036.27 6724.18 152.51 o 9 -7 -5 10380.50 10418.50 99.81 o 9 -7 -4 2521.03 2403.88 74.74 o 9 -7 -3 1058.91 1081.56 56.38 o 9 -7 -2 13669.80 13252.20 72.48 o 9 -7 -1 514.20 501.40 33.03 o 9 -7 0 813.28 881.07 37.70 o 9 -7 1 6214.80 6184.37 50.07 o 9 -7 2 288.10 266.87 30.69 o 9 -7 3 1385.81 1327.13 40.03 o 9 -7 4 1927.97 1809.58 88.41 o 9 -7 5 22.06 -10.01 78.73 < 9 -7 6 165.11 103.41 91.40 < 9 -7 7 3.05 68.05 146.44 < 9 -3 -6 8213.82 8183.84 198.25 o 9 -3 -5 7600.90 7626.17 134.49 o 9 -3 -4 11638.90 11217.00 135.53 o 9 -3 -3 32420.10 32035.80 135.41 o 9 -3 -2 37786.80 37355.30 138.54 o 9 -3 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151.78 18.68 o 9 5 5 10787.20 10551.00 63.77 o 9 5 6 2222.97 2233.03 36.70 o 9 5 7 51.83 35.36 48.04 < 9 5 8 52.42 61.05 49.04 < 9 5 9 162.05 210.16 64.05 o 9 5 10 257.83 256.86 118.09 o 9 9 -3 5502.22 5287.73 133.81 o 9 9 -2 277.84 317.91 69.05 o 9 9 -1 5358.50 5411.80 79.75 o 9 9 0 9337.94 9486.85 87.45 o 9 9 1 2600.39 2629.79 54.05 o 9 9 2 908.17 893.40 33.36 o 9 9 3 7807.10 7243.01 57.42 o 9 9 4 6115.95 5999.07 52.07 o 9 9 5 798.85 765.62 47.37 o 9 9 6 236.52 297.23 38.36 o 9 9 7 2006.25 2075.50 48.38 o 9 9 8 935.69 1017.15 63.38 o 9 9 9 1412.58 1493.24 68.06 o 9 9 10 19.92 63.05 111.08 < 9 13 -1 11224.60 11978.70 158.89 o 9 13 0 2804.10 2868.96 89.42 o 9 13 1 13487.80 13958.30 120.86 o 9 13 2 14249.40 14078.30 97.16 o 9 13 3 1503.61 1560.66 38.03 o 9 13 4 12091.10 12076.10 74.79 o 9 13 5 67.84 37.03 40.36 < 9 13 6 8206.22 8060.10 80.11 o 9 13 7 241.07 199.15 33.69 o 9 13 8 0.97 32.36 44.37 < 9 13 9 777.52 846.67 64.05 o 9 13 10 1521.59 1700.09 78.73 o 9 13 11 846.29 882.70 84.07 o 9 17 0 2041.63 1973.05 115.77 o 9 17 1 14088.40 14519.10 163.93 o 9 17 2 309.65 311.24 62.38 o 9 17 3 2068.66 2157.55 78.07 o 9 17 4 19612.60 19859.30 168.67 o 9 17 5 3190.41 3203.71 57.05 o 9 17 6 6553.58 6435.53 70.08 o 9 17 7 1711.06 1654.41 41.70 o 9 17 8 3574.30 3678.89 67.73 o 9 17 9 1538.48 1637.37 53.04 o 9 17 10 2629.20 2770.17 64.73 o 9 17 11 533.66 506.73 78.39 o 9 21 2 927.68 1049.18 127.44 o 9 21 3 857.69 938.41 111.42 o 9 21 4 311.44 324.58 90.07 o 9 21 5 354.46 359.94 88.73 o 9 21 6 7332.41 7472.21 117.14 o 9 21 7 149.43 178.80 55.38 o 9 21 8 2540.13 2529.94 74.07 o 9 21 9 371.98 358.61 57.04 o 9 21 10 85.99 116.75 57.38 o 9 21 11 2200.97 2265.66 91.08 o 9 25 5 327.93 239.18 137.77 < 9 25 6 12.63 0.33 147.11 < 9 25 7 1528.93 1725.11 175.48 o 9 25 8 2549.88 2494.91 111.10 o 9 25 9 638.55 672.86 82.06 o 9 25 10 217.69 244.18 76.06 o 9 25 11 13.13 -10.34 115.09 < 10 -26 -8 130.85 78.73 94.40 < 10 -26 -7 45.43 49.70 76.06 < 10 -26 -6 598.86 562.11 77.73 o 10 -26 -5 2527.16 2441.86 79.07 o 10 -26 -4 5341.80 5127.14 122.80 o 10 -26 -3 137.85 195.81 80.73 o 10 -26 -2 3605.59 3408.63 130.13 o 10 -22 -8 656.47 698.88 121.76 o 10 -22 -7 409.30 346.27 106.75 o 10 -22 -6 108.18 150.11 79.06 < 10 -22 -5 42.81 18.35 67.05 < 10 -22 -4 1146.16 1170.29 64.72 o 10 -22 -3 625.47 710.89 93.07 o 10 -22 -2 7013.80 7005.50 116.14 o 10 -22 -1 252.87 280.88 61.05 o 10 -22 0 2253.35 2205.28 101.76 o 10 -22 1 13342.40 14004.00 254.07 o 10 -18 -8 3622.23 3606.48 129.79 o 10 -18 -7 1449.66 1527.94 89.07 o 10 -18 -6 508.35 453.35 63.72 o 10 -18 -5 146.60 100.08 71.05 < 10 -18 -4 2459.18 2405.17 68.06 o 10 -18 -3 1943.83 1959.04 108.76 o 10 -18 -2 1517.35 1535.29 60.38 o 10 -18 -1 2146.10 2192.60 64.72 o 10 -18 0 1136.94 1181.96 62.72 o 10 -18 1 1079.31 1051.52 72.39 o 10 -18 2 26.50 43.70 72.39 < 10 -18 3 4446.44 4148.90 254.93 o 10 -14 -8 603.47 548.10 127.10 o 10 -14 -7 3583.41 3772.29 146.81 o 10 -14 -6 6884.21 6797.90 146.84 o 10 -14 -5 98.32 160.79 75.06 o 10 -14 -4 2663.19 2641.11 69.40 o 10 -14 -3 989.95 1043.18 49.71 o 10 -14 -2 6375.60 6588.32 90.44 o 10 -14 -1 34062.00 35982.80 205.32 o 10 -14 0 371.49 358.28 53.04 o 10 -14 1 3733.91 3543.16 78.08 o 10 -14 2 5412.50 5071.46 106.45 o 10 -14 3 1431.37 1333.44 96.75 o 10 -14 4 3122.94 2946.42 122.78 o 10 -10 -7 1194.52 1011.49 179.48 o 10 -10 -6 4890.12 4717.24 134.47 o 10 -10 -5 3323.44 3350.53 109.44 o 10 -10 -4 7137.91 7024.97 121.48 o 10 -10 -3 1055.70 1018.17 66.39 o 10 -10 -2 5122.82 5392.96 66.41 o 10 -10 -1 19251.10 19902.00 118.62 o 10 -10 0 1684.55 1955.73 47.04 o 10 -10 1 61588.30 59623.60 158.88 o 10 -10 2 3529.33 3102.42 63.40 o 10 -10 3 8779.40 7952.06 99.13 o 10 -10 4 20568.80 19229.90 174.01 o 10 -10 5 4192.95 3951.94 112.11 o 10 -10 6 8876.57 8350.79 142.85 o 10 -6 -7 835.60 569.79 228.85 o 10 -6 -6 1609.98 1487.92 107.09 o 10 -6 -5 7847.47 7591.26 118.14 o 10 -6 -4 3603.67 3586.18 67.07 o 10 -6 -3 619.88 673.20 53.04 o 10 -6 -2 2946.98 3059.03 59.73 o 10 -6 -1 2298.76 2299.88 43.38 o 10 -6 0 550.94 475.05 29.69 o 10 -6 1 39692.40 40668.60 95.10 o 10 -6 2 493.07 392.98 34.03 o 10 -6 3 48231.10 44577.20 137.60 o 10 -6 4 14503.00 14082.50 124.55 o 10 -6 5 2621.59 2514.61 90.75 o 10 -6 6 14262.20 13984.40 145.57 o 10 -6 7 7581.02 7471.03 152.85 o 10 -2 -6 153.22 166.12 101.41 < 10 -2 -5 1944.27 1664.44 105.42 o 10 -2 -4 3733.50 3774.01 87.42 o 10 -2 -3 10424.70 10493.70 155.56 o 10 -2 -2 453.86 468.03 39.36 o 10 -2 -1 1872.89 1985.14 65.06 o 10 -2 0 783.77 634.52 36.36 o 10 -2 1 235.60 218.50 26.35 o 10 -2 2 56162.20 54080.00 124.48 o 10 -2 3 30636.70 28298.20 115.75 o 10 -2 4 86.21 69.05 32.69 o 10 -2 5 1734.89 1552.01 62.39 o 10 -2 6 2011.78 1929.68 50.71 o 10 -2 7 849.55 948.42 74.39 o 10 -2 8 14137.30 14339.40 203.66 o 10 2 -5 84.07 65.38 99.07 < 10 2 -4 469.41 462.36 85.73 o 10 2 -3 9448.30 9432.45 111.81 o 10 2 -2 526.28 515.74 54.71 o 10 2 -1 11716.50 11738.30 118.86 o 10 2 0 9656.74 9402.86 112.18 o 10 2 1 15524.50 16092.90 61.81 o 10 2 2 41757.00 40454.00 125.31 o 10 2 3 1736.37 1735.27 58.05 o 10 2 4 80682.30 78425.70 131.72 o 10 2 5 1764.38 1900.68 47.04 o 10 2 6 4121.82 4037.14 56.72 o 10 2 7 2269.93 2305.38 54.38 o 10 2 8 69.09 132.43 78.39 < 10 2 9 2908.38 2937.38 113.10 o 10 6 -3 2157.53 2310.02 95.08 o 10 6 -2 3092.73 3105.90 85.08 o 10 6 -1 9075.54 9071.34 87.12 o 10 6 0 331.63 304.23 45.03 o 10 6 1 17756.90 17999.30 238.52 o 10 6 2 20401.40 20360.70 91.57 o 10 6 3 4679.28 4859.08 58.74 o 10 6 4 65799.30 64522.90 174.84 o 10 6 5 2274.75 2462.30 64.73 o 10 6 6 64246.30 63606.00 131.38 o 10 6 7 20842.50 20962.90 117.25 o 10 6 8 2236.86 2311.04 66.73 o 10 6 9 10575.50 10527.20 115.49 o 10 6 10 3571.10 3783.32 196.86 o 10 10 -2 2337.85 2232.31 108.43 o 10 10 -1 4119.67 4208.51 96.10 o 10 10 0 4325.25 4449.17 62.73 o 10 10 1 2360.00 2468.89 59.05 o 10 10 2 2.88 -2.34 39.03 < 10 10 3 5206.48 5013.08 59.74 o 10 10 4 10956.90 11000.50 85.14 o 10 10 6 46628.80 46350.70 140.25 o 10 10 7 8310.23 8583.53 69.09 o 10 10 8 9321.14 9493.27 84.45 o 10 10 9 17700.30 18258.00 148.27 o 10 10 10 6399.07 6380.89 102.12 o 10 14 -1 264.24 148.45 116.76 < 10 14 0 9129.88 9266.00 144.19 o 10 14 1 273.33 336.59 66.05 o 10 14 2 6127.38 6313.76 74.75 o 10 14 3 484.99 551.76 50.71 o 10 14 4 6723.21 6646.96 67.75 o 10 14 5 2050.97 2020.12 43.37 o 10 14 6 8045.89 8067.75 65.42 o 10 14 7 4332.96 4341.47 59.39 o 10 14 8 121.07 143.11 43.03 o 10 14 9 2806.02 2911.66 82.08 o 10 14 10 3275.04 3312.79 85.75 o 10 14 11 8265.35 8122.50 106.13 o 10 18 1 88.54 42.03 120.09 < 10 18 2 8417.22 8324.42 154.86 o 10 18 3 1946.53 2090.80 126.78 o 10 18 4 15585.70 15243.40 159.94 o 10 18 5 7100.51 6977.58 82.76 o 10 18 6 4401.27 4332.75 61.73 o 10 18 7 16007.00 16167.70 97.17 o 10 18 8 1849.11 1887.29 48.04 o 10 18 9 9317.22 9811.47 89.45 o 10 18 10 3373.19 3378.54 79.41 o 10 18 11 51.57 55.37 66.05 < 10 22 3 265.02 270.87 149.11 < 10 22 4 5932.50 5978.61 175.86 o 10 22 5 3349.66 3238.73 138.46 o 10 22 6 7965.06 7882.64 155.52 o 10 22 7 11898.30 11508.40 144.21 o 10 22 8 6807.29 6852.90 108.12 o 10 22 9 21508.10 21519.80 162.33 o 10 22 10 6311.78 6249.04 115.80 o 10 22 11 5677.83 5612.47 110.45 o 10 26 7 410.37 346.93 190.48 < 10 26 8 2453.69 2699.42 206.85 o 10 26 9 11796.00 11853.70 207.30 o 10 26 10 1890.34 1726.82 98.75 o 11 -29 -5 1157.96 923.42 214.84 o 11 -25 -7 15927.10 15382.10 201.68 o 11 -25 -6 700.26 644.84 74.73 o 11 -25 -5 19934.30 19567.00 156.64 o 11 -25 -4 20246.70 19941.50 174.34 o 11 -25 -3 895.56 941.42 79.06 o 11 -25 -2 7115.63 6779.32 140.50 o 11 -25 -1 1360.97 1222.35 92.41 o 11 -21 -8 73.44 177.80 139.10 < 11 -21 -7 8246.60 8127.43 198.58 o 11 -21 -6 34.44 67.38 84.06 < 11 -21 -5 17987.00 18045.60 168.31 o 11 -21 -4 6159.87 6424.85 103.11 o 11 -21 -3 4829.09 4927.45 88.09 o 11 -21 -2 17895.60 17709.30 130.57 o 11 -21 -1 1902.29 1830.24 64.39 o 11 -21 0 12001.60 11924.20 127.52 o 11 -21 1 2085.64 2092.83 89.41 o 11 -17 -8 3874.54 3469.41 171.84 o 11 -17 -7 1737.90 1607.37 107.76 o 11 -17 -6 7676.69 7864.15 166.53 o 11 -17 -5 3356.06 3394.90 106.10 o 11 -17 -4 474.86 626.15 83.73 o 11 -17 -3 259.03 339.26 75.39 o 11 -17 -2 1191.58 1171.96 68.39 o 11 -17 -1 68.48 138.77 58.71 o 11 -17 0 16428.40 16407.80 123.22 o 11 -17 1 553.77 567.44 62.05 o 11 -17 2 2792.35 2619.06 98.76 o 11 -17 3 542.97 593.80 81.73 o 11 -13 -7 6153.66 5999.71 165.52 o 11 -13 -6 21976.20 22893.90 243.84 o 11 -13 -5 9763.17 9696.39 132.51 o 11 -13 -4 14896.40 15065.20 120.87 o 11 -13 -3 1589.60 1669.43 62.39 o 11 -13 -2 12436.90 12746.90 91.15 o 11 -13 -1 18051.00 19332.30 125.93 o 11 -13 0 1200.27 1167.64 58.72 o 11 -13 1 2675.39 2615.41 78.74 o 11 -13 2 723.07 731.58 66.72 o 11 -13 3 1190.06 1210.99 84.40 o 11 -13 4 773.88 740.25 101.75 o 11 -9 -7 7951.16 7584.69 272.67 o 11 -9 -6 8560.02 8244.05 251.65 o 11 -9 -5 7201.85 7162.14 149.18 o 11 -9 -4 17393.40 17262.20 188.35 o 11 -9 -3 19317.90 19755.30 138.62 o 11 -9 -2 42167.20 45499.90 237.95 o 11 -9 -1 24088.70 24061.90 103.62 o 11 -9 0 4439.79 4915.14 57.06 o 11 -9 1 30373.60 30745.10 138.43 o 11 -9 2 4286.70 3868.07 59.06 o 11 -9 3 10350.30 9493.83 110.49 o 11 -9 4 25.33 36.69 73.05 < 11 -9 5 693.80 644.51 94.07 o 11 -9 6 295.67 274.88 103.41 o 11 -5 -6 1020.97 880.71 136.78 o 11 -5 -5 1404.08 1403.50 120.10 o 11 -5 -4 90.50 41.36 66.05 < 11 -5 -3 1130.58 1136.93 72.39 o 11 -5 -2 22743.40 22390.80 121.97 o 11 -5 -1 26782.40 26779.40 120.36 o 11 -5 0 8573.29 9017.14 64.77 o 11 -5 1 12299.00 13154.70 64.45 o 11 -5 2 10692.10 10538.90 76.13 o 11 -5 3 31265.20 29286.60 137.43 o 11 -5 4 3092.89 2945.49 50.72 o 11 -5 5 2290.17 2249.00 61.72 o 11 -5 6 488.50 416.32 89.07 o 11 -5 7 757.90 716.57 98.74 o 11 -1 -5 2658.27 2557.32 152.14 o 11 -1 -4 2638.61 2666.41 95.42 o 11 -1 -3 2918.50 2941.39 81.41 o 11 -1 -2 1323.28 1319.10 60.05 o 11 -1 -1 337.87 366.28 53.37 o 11 -1 0 69.46 85.06 35.69 o 11 -1 1 721.91 711.91 26.02 o 11 -1 2 2316.72 2354.95 33.37 o 11 -1 3 4261.62 4182.71 55.40 o 11 -1 4 2313.18 2254.76 44.37 o 11 -1 5 2340.31 2283.07 71.73 o 11 -1 6 1788.20 1803.21 44.37 o 11 -1 7 719.21 713.90 69.39 o 11 -1 8 152.25 83.40 111.42 < 11 3 -4 13501.20 13346.90 151.57 o 11 3 -3 13332.60 13709.20 172.27 o 11 3 -2 5150.47 5049.37 86.09 o 11 3 -1 7400.00 7270.70 104.46 o 11 3 0 25260.80 25302.40 169.12 o 11 3 1 24675.40 24547.00 136.39 o 11 3 2 2022.77 2281.12 48.71 o 11 3 3 515.80 564.78 35.03 o 11 3 4 330.69 363.95 35.36 o 11 3 5 7015.28 6907.88 66.08 o 11 3 6 217.15 220.50 28.69 o 11 3 7 195.14 224.17 44.03 o 11 3 8 562.04 523.07 59.71 o 11 3 9 56.36 88.73 79.39 < 11 7 -3 9944.46 9309.95 152.54 o 11 7 -2 8868.54 9013.51 124.16 o 11 7 -1 6427.82 6525.41 88.43 o 11 7 0 11496.80 11515.80 106.83 o 11 7 1 18886.80 18674.80 116.24 o 11 7 2 31413.80 29987.50 301.96 o 11 7 3 16304.90 15690.70 117.58 o 11 7 5 18727.10 18644.60 175.72 o 11 7 6 1356.90 1384.50 38.70 o 11 7 7 5095.41 5106.84 64.07 o 11 7 8 291.81 303.90 54.37 o 11 7 9 273.60 310.24 61.38 o 11 7 10 17.43 -7.01 84.40 < 11 11 -1 370.73 476.37 83.06 o 11 11 0 4823.73 4941.45 91.09 o 11 11 1 2940.15 2968.42 54.05 o 11 11 2 6870.15 6628.24 73.42 o 11 11 3 888.46 849.02 37.36 o 11 11 4 10957.00 10879.00 81.12 o 11 11 5 26089.00 26096.60 131.68 o 11 11 6 198.16 206.82 34.69 o 11 11 7 5207.54 5131.25 72.41 o 11 11 8 9.71 16.35 41.70 < 11 11 9 4777.39 4950.45 94.43 o 11 11 10 25.18 -6.67 66.05 < 11 15 0 2204.42 2398.78 115.77 o 11 15 1 345.87 336.92 82.06 o 11 15 2 1236.63 1231.01 74.06 o 11 15 3 6748.11 6723.12 89.77 o 11 15 4 200.85 241.18 46.03 o 11 15 5 755.49 736.25 39.70 o 11 15 6 762.30 773.28 32.36 o 11 15 7 5476.46 5422.59 52.39 o 11 15 8 1696.86 1713.46 47.37 o 11 15 9 2127.33 2133.20 58.38 o 11 15 10 13.52 9.01 53.04 < 11 15 11 362.98 327.58 74.39 o 11 19 2 3047.01 3214.66 166.49 o 11 19 3 11581.20 11379.80 204.29 o 11 19 4 37.94 18.35 85.73 < 11 19 5 9801.65 9681.26 142.19 o 11 19 6 996.12 970.45 52.71 o 11 19 7 16.80 6.67 42.70 < 11 19 8 2134.14 2194.92 56.38 o 11 19 9 1414.35 1428.85 60.38 o 11 19 10 1092.55 1159.94 57.71 o 11 19 11 298.70 326.58 61.05 o 11 23 4 2434.25 2312.40 159.48 o 11 23 5 10918.20 11356.70 218.31 o 11 23 6 386.88 350.60 147.78 o 11 23 7 6791.21 6718.09 229.60 o 11 23 8 9207.78 9219.65 145.52 o 11 23 9 83.06 70.72 96.41 < 11 23 10 401.50 442.67 69.05 o 11 23 11 462.28 392.30 82.40 o 12 -28 -6 4.59 18.35 162.46 < 12 -28 -5 11.01 31.36 98.74 < 12 -28 -4 0.14 -18.01 131.10 < 12 -24 -7 601.49 588.46 97.08 o 12 -24 -6 2024.22 1979.39 89.41 o 12 -24 -5 490.63 518.07 79.73 o 12 -24 -4 800.75 852.68 74.06 o 12 -24 -3 1149.97 1108.24 70.39 o 12 -24 -2 284.03 259.20 80.06 o 12 -24 -1 6.05 31.02 73.39 < 12 -20 -7 70.02 27.69 108.42 < 12 -20 -6 859.09 794.30 129.44 o 12 -20 -5 4468.25 4452.51 108.78 o 12 -20 -4 1295.08 1394.15 88.74 o 12 -20 -3 1830.30 1940.66 80.07 o 12 -20 -2 3953.27 3989.26 89.75 o 12 -20 -1 5969.52 5990.95 122.80 o 12 -20 0 4417.32 4244.29 97.77 o 12 -20 1 52.29 53.37 75.72 < 12 -16 -7 8.06 22.35 89.73 < 12 -16 -6 259.86 297.56 80.73 o 12 -16 -5 3452.24 3580.75 112.44 o 12 -16 -4 4119.84 4264.60 105.77 o 12 -16 -3 7483.65 7456.78 121.48 o 12 -16 -2 10.76 -11.68 65.38 < 12 -16 -1 2386.87 2529.27 63.39 o 12 -16 0 7369.29 7462.98 113.14 o 12 -16 1 3658.67 3563.78 83.75 o 12 -16 2 11518.40 11244.80 132.52 o 12 -16 3 756.69 749.93 85.73 o 12 -12 -7 185.07 202.15 180.80 < 12 -12 -6 1247.26 1195.65 126.77 o 12 -12 -5 14.73 -28.69 84.06 < 12 -12 -4 8269.44 8378.61 105.47 o 12 -12 -3 10616.50 10724.30 105.82 o 12 -12 -2 3661.73 3724.07 71.74 o 12 -12 -1 530.39 617.15 59.71 o 12 -12 0 27.25 77.06 42.70 < 12 -12 1 6.64 15.68 51.04 < 12 -12 2 7309.64 6836.25 105.79 o 12 -12 3 19.56 3.67 71.72 < 12 -12 4 12773.00 11628.90 157.57 o 12 -12 5 1545.66 1560.31 107.42 o 12 -8 -6 2524.45 2550.96 205.18 o 12 -8 -5 599.69 531.41 174.80 o 12 -8 -4 421.63 380.96 63.05 o 12 -8 -3 2593.99 2774.55 68.73 o 12 -8 -2 25061.70 26297.30 199.18 o 12 -8 -1 946.34 1054.20 67.72 o 12 -8 0 2440.66 2692.87 54.38 o 12 -8 1 6056.27 6290.32 69.75 o 12 -8 2 3955.63 3935.73 62.73 o 12 -8 3 10480.90 9670.62 123.51 o 12 -8 4 9701.60 9187.04 101.14 o 12 -8 5 4283.34 4111.79 107.44 o 12 -8 6 8.58 26.35 90.07 < 12 -4 -5 1583.21 1522.61 137.45 o 12 -4 -4 777.20 894.04 105.42 o 12 -4 -3 5.92 70.72 65.72 < 12 -4 -2 10550.80 10648.70 117.84 o 12 -4 -1 2296.23 2421.90 64.06 o 12 -4 0 25679.20 26386.00 115.67 o 12 -4 1 8739.39 8828.26 66.43 o 12 -4 2 7239.49 7535.19 60.08 o 12 -4 3 24833.50 24391.30 162.43 o 12 -4 4 1714.38 1480.95 62.05 o 12 -4 5 40567.30 39378.70 155.51 o 12 -4 6 74.61 39.03 70.05 < 12 -4 7 6739.13 6484.47 151.51 o 12 0 -4 1116.17 1158.61 106.42 o 12 0 -3 2064.49 2176.89 100.09 o 12 0 -2 37.48 38.36 58.38 < 12 0 -1 4692.39 4867.89 93.77 o 12 0 0 20031.70 20207.20 125.29 o 12 0 1 71.76 90.73 28.02 o 12 0 2 11359.10 12271.10 84.15 o 12 0 3 14042.80 14176.80 121.24 o 12 0 4 2051.80 2026.84 65.73 o 12 0 5 39383.00 38480.40 142.83 o 12 0 6 1655.19 1566.00 52.04 o 12 0 7 42386.70 42594.60 159.19 o 12 0 8 2888.46 2726.51 142.80 o 12 4 -3 1918.41 1939.67 95.08 o 12 4 -2 2632.40 2637.05 90.42 o 12 4 -1 515.47 595.13 61.38 o 12 4 0 3765.08 3768.44 64.40 o 12 4 1 18346.10 18054.60 131.95 o 12 4 2 3566.07 3837.97 82.08 o 12 4 4 65.27 131.10 40.70 o 12 4 5 2280.13 2384.52 45.04 o 12 4 6 342.99 370.95 39.70 o 12 4 7 35551.40 35847.60 156.80 o 12 4 8 78.84 26.69 67.72 < 12 4 9 6201.78 6502.95 115.46 o 12 8 -2 1981.65 1916.99 98.08 o 12 8 -1 73.00 62.05 67.05 < 12 8 0 349.20 394.30 45.37 o 12 8 1 16616.90 16689.00 104.86 o 12 8 2 1897.16 1929.36 50.04 o 12 8 3 22230.60 21726.40 113.94 o 12 8 4 5154.39 4798.77 74.08 o 12 8 5 5464.04 5550.37 55.06 o 12 8 6 2856.67 2973.14 47.38 o 12 8 7 502.76 541.09 41.37 o 12 8 8 15323.30 15144.10 150.25 o 12 8 9 1962.04 2067.45 80.74 o 12 8 10 412.48 395.64 73.72 o 12 12 -1 57.92 102.74 97.41 < 12 12 0 1405.17 1468.55 86.41 o 12 12 1 2858.65 2914.34 97.42 o 12 12 2 601.50 567.78 41.37 o 12 12 3 26509.20 26128.80 107.26 o 12 12 4 1560.48 1625.38 59.05 o 12 12 5 23650.10 23643.20 96.22 o 12 12 6 9646.61 9660.05 69.76 o 12 12 7 7097.52 7269.72 62.41 o 12 12 8 20227.50 20329.10 107.88 o 12 12 9 3021.91 3104.88 68.40 o 12 12 10 16449.60 16851.30 184.65 o 12 12 11 1374.74 1386.82 95.41 o 12 16 1 51.48 61.71 98.41 < 12 16 2 94.64 170.13 101.74 < 12 16 3 6857.23 6972.07 127.82 o 12 16 4 1031.63 1156.27 56.05 o 12 16 5 12678.10 12635.30 112.17 o 12 16 6 2580.42 2602.02 44.04 o 12 16 7 9468.79 9459.22 74.77 o 12 16 8 9918.17 10020.50 82.78 o 12 16 9 7348.27 7423.14 80.43 o 12 16 10 22026.70 22163.50 138.29 o 12 16 11 3422.21 3284.47 78.41 o 12 20 3 59.15 81.39 110.08 < 12 20 4 3964.60 3908.52 156.49 o 12 20 5 1735.45 1794.53 92.41 o 12 20 6 1531.84 1469.56 111.09 o 12 20 7 17.91 37.36 46.70 < 12 20 8 123.22 153.78 59.04 o 12 20 9 3528.53 3643.15 76.07 o 12 20 10 5273.09 5335.01 89.43 o 12 20 11 33.41 21.02 67.05 < 12 24 6 7253.18 6536.45 246.29 o 12 24 7 3081.37 3004.14 198.52 o 12 24 8 3796.56 3697.61 209.87 o 12 24 9 1263.37 1296.07 108.42 o 12 24 10 908.90 851.35 90.41 o 13 -27 -6 3138.12 2697.20 199.19 o 13 -27 -5 293.37 259.86 84.73 o 13 -27 -4 9654.07 9328.16 153.87 o 13 -27 -3 1152.16 1056.86 197.49 o 13 -23 -7 9247.52 9009.17 158.88 o 13 -23 -6 960.20 906.06 85.40 o 13 -23 -5 8539.73 8694.95 198.58 o 13 -23 -4 768.73 750.26 71.06 o 13 -23 -3 5081.59 4919.50 102.44 o 13 -23 -2 116.25 98.74 62.05 < 13 -23 -1 21.05 36.36 67.38 < 13 -23 0 14.67 25.02 77.72 < 13 -19 -7 2836.44 2506.30 171.49 o 13 -19 -6 12082.40 12312.80 236.01 o 13 -19 -5 31646.90 30595.40 300.79 o 13 -19 -4 2417.45 2440.17 82.07 o 13 -19 -3 14417.60 15291.70 150.24 o 13 -19 -2 3201.82 3326.12 78.74 o 13 -19 -1 20631.90 20722.10 171.01 o 13 -19 0 4109.48 4129.76 96.76 o 13 -19 1 304.43 332.59 77.06 o 13 -19 2 4484.43 4274.36 106.11 o 13 -15 -7 21.97 0.00 101.74 < 13 -15 -6 7053.22 6993.18 125.81 o 13 -15 -5 7347.50 7441.17 121.14 o 13 -15 -4 4351.12 4303.02 97.43 o 13 -15 -3 22338.40 22485.60 180.05 o 13 -15 -2 8346.86 8727.83 119.15 o 13 -15 -1 27377.10 29138.90 175.77 o 13 -15 0 7041.52 7271.96 104.46 o 13 -15 1 6599.73 6542.51 101.45 o 13 -15 2 16498.50 15992.70 160.28 o 13 -15 3 727.49 623.49 78.40 o 13 -15 4 5338.16 5083.79 125.47 o 13 -11 -6 1781.75 1741.82 192.83 o 13 -11 -5 453.60 579.45 90.07 o 13 -11 -4 659.83 715.23 62.05 o 13 -11 -3 4.70 1.67 55.04 < 13 -11 -2 1653.05 1671.43 55.38 o 13 -11 -1 17779.40 18529.70 125.92 o 13 -11 0 1973.48 2142.89 77.40 o 13 -11 1 2456.70 2698.79 62.06 o 13 -11 2 8509.56 8483.26 82.44 o 13 -11 3 4006.11 3766.73 100.43 o 13 -11 4 13281.10 12687.90 214.33 o 13 -11 5 46.07 57.04 94.74 < 13 -7 -6 3908.23 3782.40 238.57 o 13 -7 -5 11004.60 10938.70 282.73 o 13 -7 -4 2692.77 2784.20 174.49 o 13 -7 -3 12210.30 12093.30 138.54 o 13 -7 -2 12740.10 12705.80 157.25 o 13 -7 -1 2432.30 2414.23 53.38 o 13 -7 0 1477.14 1617.72 51.04 o 13 -7 1 512.29 528.41 50.37 o 13 -7 2 786.21 828.33 55.04 o 13 -7 3 11.89 27.69 40.70 < 13 -7 4 4008.42 3816.80 70.40 o 13 -7 5 40.28 8.67 82.73 < 13 -7 6 1578.36 1528.62 91.08 o 13 -7 7 96.23 89.73 121.76 < 13 -3 -5 8593.73 8670.02 214.27 o 13 -3 -4 10727.70 10527.00 161.22 o 13 -3 -3 21089.40 20735.40 184.37 o 13 -3 -2 11504.70 11283.50 122.18 o 13 -3 -1 12282.40 11981.90 100.83 o 13 -3 0 29648.80 29478.50 135.07 o 13 -3 1 33869.00 34817.80 135.13 o 13 -3 2 15132.50 16154.20 98.86 o 13 -3 4 2619.76 2454.94 68.40 o 13 -3 5 6802.33 6607.46 74.42 o 13 -3 6 547.88 578.78 53.37 o 13 -3 7 5.29 -57.38 77.06 < 13 -3 8 174.99 191.48 125.43 < 13 1 -4 570.84 591.79 100.08 o 13 1 -3 5837.59 5622.16 141.15 o 13 1 -2 10539.80 10433.50 115.16 o 13 1 -1 4469.41 4401.88 84.09 o 13 1 0 6349.39 6337.88 103.12 o 13 1 1 24044.00 23902.20 131.67 o 13 1 2 39768.30 40342.90 229.57 o 13 1 3 17416.80 17985.60 215.46 o 13 1 4 6369.27 6070.43 98.45 o 13 1 5 7458.50 7254.15 66.75 o 13 1 6 12092.70 11964.50 83.46 o 13 1 7 2380.68 2313.39 67.06 o 13 1 8 637.17 765.27 127.43 o 13 1 9 22.47 14.68 113.75 < 13 5 -3 2690.76 2495.61 100.09 o 13 5 -2 82.25 117.09 78.06 < 13 5 -1 912.18 974.78 70.06 o 13 5 0 417.58 415.99 60.05 o 13 5 1 1248.36 1185.65 50.71 o 13 5 2 1396.65 1318.78 52.38 o 13 5 3 2431.83 2353.85 71.40 o 13 5 4 4700.65 4521.30 68.07 o 13 5 5 9145.75 9342.75 78.78 o 13 5 6 7797.31 8062.87 91.45 o 13 5 7 196.45 172.13 39.70 o 13 5 8 4321.55 4464.82 76.08 o 13 5 9 440.11 416.65 73.72 o 13 5 10 1179.11 1086.89 194.16 o 13 9 -1 20085.80 20580.00 189.04 o 13 9 0 7056.93 7053.24 144.50 o 13 9 1 2858.90 2905.01 67.73 o 13 9 2 1087.46 1085.22 51.71 o 13 9 3 3809.22 3963.97 60.39 o 13 9 4 11077.30 11182.20 74.11 o 13 9 5 81.40 57.71 34.69 < 13 9 6 1254.80 1251.04 47.04 o 13 9 7 0.57 -8.34 44.70 < 13 9 8 530.16 549.76 58.38 o 13 9 9 1144.96 1064.20 73.39 o 13 9 10 2750.93 2751.85 89.08 o 13 13 0 3500.22 3622.81 124.79 o 13 13 1 16539.90 16980.90 196.68 o 13 13 2 9770.37 9866.81 99.13 o 13 13 3 5359.79 5166.21 70.74 o 13 13 4 16156.90 15751.00 81.14 o 13 13 5 4609.72 4674.19 63.07 o 13 13 6 12730.50 12789.20 75.12 o 13 13 7 675.90 687.88 40.70 o 13 13 8 367.77 392.30 43.37 o 13 13 9 3856.67 4008.92 80.41 o 13 13 10 602.77 696.88 79.73 o 13 13 11 775.53 867.35 96.08 o 13 17 2 564.64 492.05 115.09 o 13 17 3 5855.50 5886.80 141.49 o 13 17 4 17814.70 17996.30 158.96 o 13 17 5 1172.18 1178.63 58.71 o 13 17 6 8158.62 8304.95 113.47 o 13 17 7 724.54 738.58 47.37 o 13 17 8 16087.50 16063.80 110.52 o 13 17 9 3682.58 3741.95 89.42 o 13 17 10 788.73 750.26 58.05 o 13 17 11 2000.36 1899.32 80.40 o 13 21 4 1363.13 1610.67 152.79 o 13 21 5 90.53 37.69 88.73 < 13 21 6 3329.03 3360.51 137.80 o 13 21 7 1609.42 1349.14 184.82 o 13 21 8 8196.64 8314.97 133.16 o 13 21 9 388.82 418.99 65.38 o 13 21 10 1118.26 1067.54 76.06 o 13 21 11 1897.11 1961.36 133.45 o 13 25 8 1920.72 1895.97 200.84 o 14 -26 -5 20.49 -46.70 80.06 < 14 -26 -4 74.89 90.73 74.39 < 14 -26 -3 186.56 140.77 85.40 < 14 -22 -6 62.86 75.39 93.40 < 14 -22 -5 12.91 -16.01 94.07 < 14 -22 -4 398.73 351.94 77.06 o 14 -22 -3 1240.85 1202.99 84.74 o 14 -22 -2 2130.04 2338.71 103.42 o 14 -22 -1 82.43 127.10 68.38 < 14 -22 0 1519.81 1558.64 78.07 o 14 -18 -7 3647.73 3349.92 178.17 o 14 -18 -6 987.95 1201.63 144.45 o 14 -18 -5 19.72 37.03 106.75 < 14 -18 -4 160.69 200.49 91.07 o 14 -18 -3 867.25 905.39 83.07 o 14 -18 -2 4945.23 5048.94 93.10 o 14 -18 -1 6921.92 7037.85 118.47 o 14 -18 0 72.67 110.75 77.72 < 14 -18 1 84.59 115.42 75.39 < 14 -18 2 10.64 57.71 87.73 < 14 -14 -6 21.23 20.01 104.08 < 14 -14 -5 1094.38 1141.26 84.74 o 14 -14 -4 38.19 56.04 84.73 < 14 -14 -3 330.68 388.63 81.06 o 14 -14 -2 158.57 269.87 65.38 o 14 -14 -1 12056.80 12592.70 118.18 o 14 -14 0 3364.93 3314.50 95.42 o 14 -14 1 9184.76 9320.87 102.80 o 14 -14 2 5610.09 5684.16 128.81 o 14 -14 3 1629.19 1582.67 120.77 o 14 -14 4 997.35 828.34 104.42 o 14 -10 -6 1301.42 1127.26 199.16 o 14 -10 -5 2480.86 2796.17 197.18 o 14 -10 -4 1068.62 1055.52 77.40 o 14 -10 -3 271.40 268.20 63.72 o 14 -10 -2 64.82 75.39 49.70 < 14 -10 -1 5381.11 5530.46 88.10 o 14 -10 0 1610.51 1822.56 74.73 o 14 -10 1 22510.70 23535.20 149.00 o 14 -10 2 278.30 278.55 52.71 o 14 -10 3 5981.43 5807.46 111.79 o 14 -10 4 13261.40 12248.20 209.66 o 14 -10 5 2639.48 2312.76 100.09 o 14 -10 6 9043.85 8170.99 317.75 o 14 -6 -5 2471.58 2274.70 211.52 o 14 -6 -4 6202.35 6473.57 232.59 o 14 -6 -3 719.36 630.83 101.41 o 14 -6 -2 652.36 661.19 67.39 o 14 -6 -1 772.25 753.93 53.38 o 14 -6 0 883.91 979.13 39.70 o 14 -6 1 17526.90 18604.50 103.21 o 14 -6 2 3083.17 3021.58 99.76 o 14 -6 3 6603.24 6291.47 95.11 o 14 -6 4 3385.51 3221.42 55.72 o 14 -6 5 1021.60 938.09 77.40 o 14 -6 6 14811.80 13548.80 230.04 o 14 -6 7 1906.59 1796.22 104.42 o 14 -2 -4 10325.70 10472.40 295.74 o 14 -2 -3 2244.17 1970.40 124.44 o 14 -2 -2 1797.80 1837.57 77.73 o 14 -2 -1 3369.08 3247.80 77.07 o 14 -2 0 10.65 -26.35 73.05 < 14 -2 1 26.82 30.36 39.70 < 14 -2 2 18576.90 19888.20 135.29 o 14 -2 3 7980.06 8064.03 118.16 o 14 -2 4 2244.28 2187.63 55.72 o 14 -2 5 2280.42 2272.02 52.05 o 14 -2 6 958.21 945.76 54.04 o 14 -2 7 6.31 -79.39 75.72 < 14 -2 8 9375.79 9061.95 218.29 o 14 2 -3 3114.97 3102.23 100.76 o 14 2 -2 4066.94 4245.87 94.09 o 14 2 -1 4157.22 4241.58 85.09 o 14 2 0 329.69 339.26 59.71 o 14 2 1 3909.85 3861.59 59.06 o 14 2 2 10207.00 10225.90 107.49 o 14 2 3 329.13 377.96 55.04 o 14 2 4 36082.40 34696.20 121.07 o 14 2 5 2210.36 2286.38 53.05 o 14 2 6 2707.75 2714.82 58.72 o 14 2 7 8587.69 8595.54 127.16 o 14 2 8 539.47 609.14 92.07 o 14 2 9 8015.93 7749.58 186.23 o 14 6 -2 2680.00 2520.96 100.76 o 14 6 -1 4584.14 4623.05 107.11 o 14 6 0 896.71 911.73 67.05 o 14 6 1 2633.13 2596.70 63.06 o 14 6 2 465.26 494.72 47.37 o 14 6 3 98.65 146.78 38.03 o 14 6 4 33616.40 32402.40 139.10 o 14 6 5 192.30 190.48 43.37 o 14 6 6 21130.70 21306.20 134.95 o 14 6 7 8428.26 8543.16 76.43 o 14 6 8 4569.12 4462.22 104.77 o 14 6 9 18936.80 19582.20 187.02 o 14 6 10 3635.05 3547.11 123.12 o 14 10 -1 3171.25 3345.15 137.46 o 14 10 0 1133.22 1179.96 98.08 o 14 10 1 402.28 488.71 56.04 o 14 10 2 715.88 687.54 53.04 o 14 10 3 61.08 81.06 36.69 o 14 10 4 3636.35 3759.35 49.05 o 14 10 5 4370.72 4266.39 56.06 o 14 10 6 20177.40 20362.80 110.56 o 14 10 7 322.96 375.62 55.71 o 14 10 8 3718.36 3705.60 85.42 o 14 10 9 7737.97 8054.74 103.12 o 14 10 10 5626.42 5883.40 142.82 o 14 14 1 60.25 94.74 96.41 < 14 14 2 1072.85 1128.91 112.76 o 14 14 3 246.71 303.23 67.38 o 14 14 4 1353.34 1374.80 61.38 o 14 14 5 6003.74 5880.54 65.07 o 14 14 6 2521.65 2692.76 65.39 o 14 14 7 13086.60 13012.70 82.79 o 14 14 8 151.89 161.79 44.70 o 14 14 9 102.14 65.05 54.37 < 14 14 10 473.20 523.74 67.05 o 14 14 11 318.17 236.18 112.75 o 14 18 3 464.60 529.41 110.42 o 14 18 4 2240.08 2240.31 99.09 o 14 18 5 2730.78 2608.37 114.77 o 14 18 6 1050.62 999.47 75.73 o 14 18 7 19837.40 19746.50 120.23 o 14 18 8 1022.51 1050.85 55.71 o 14 18 9 9007.75 9039.30 107.47 o 14 18 10 2473.12 2637.36 108.10 o 14 18 11 2628.11 2591.02 90.75 o 14 22 5 331.84 379.62 165.79 o 14 22 6 1675.94 1643.06 135.12 o 14 22 7 5880.56 5554.46 226.25 o 14 22 8 1458.36 1240.37 202.50 o 14 22 9 11879.80 11792.00 196.96 o 14 22 10 4246.05 4100.13 127.79 o 15 -25 -5 14666.10 14603.70 155.59 o 15 -25 -4 15819.90 15476.90 158.27 o 15 -25 -3 229.61 223.84 76.39 o 15 -25 -2 16224.90 13850.50 238.42 o 15 -21 -6 552.59 555.43 109.42 o 15 -21 -5 6235.78 6063.48 129.81 o 15 -21 -4 3595.55 3748.94 100.76 o 15 -21 -3 988.33 1098.55 86.40 o 15 -21 -2 14660.90 14895.90 145.57 o 15 -21 -1 1558.59 1475.24 88.74 o 15 -21 0 14963.90 14760.10 152.59 o 15 -21 1 2343.98 2330.74 111.10 o 15 -17 -6 4007.16 4088.38 140.47 o 15 -17 -5 235.73 282.55 91.40 o 15 -17 -4 8573.56 8383.56 128.83 o 15 -17 -3 1736.43 1799.20 103.75 o 15 -17 -2 523.15 544.42 82.40 o 15 -17 -1 42.13 47.37 76.72 < 15 -17 0 4795.43 5020.19 160.83 o 15 -17 1 380.86 335.59 63.72 o 15 -17 2 2394.03 2385.12 108.76 o 15 -17 3 2649.39 2530.63 111.77 o 15 -13 -6 15034.30 14214.70 225.71 o 15 -13 -5 2398.66 2314.39 104.43 o 15 -13 -4 15436.20 15815.40 178.30 o 15 -13 -3 5366.38 5393.11 117.46 o 15 -13 -2 24571.80 25361.50 168.05 o 15 -13 -1 12219.50 13261.40 99.48 o 15 -13 0 268.21 309.90 53.37 o 15 -13 1 7006.56 7312.26 103.12 o 15 -13 2 2170.02 2101.84 105.09 o 15 -13 3 1973.36 2081.47 97.75 o 15 -13 4 73.34 149.45 78.06 < 15 -9 -5 1814.26 1689.45 200.84 o 15 -9 -4 15994.10 15886.10 208.02 o 15 -9 -3 4862.35 4791.99 123.46 o 15 -9 -2 24032.40 23661.60 134.64 o 15 -9 -1 9353.67 9585.30 122.83 o 15 -9 0 17638.60 18978.90 130.58 o 15 -9 1 29366.20 31311.30 161.10 o 15 -9 2 11907.70 12528.50 123.85 o 15 -9 3 8379.22 8512.41 96.12 o 15 -9 4 3457.69 3424.60 84.41 o 15 -9 5 4047.17 3943.23 136.47 o 15 -9 6 4477.48 4315.74 158.16 o 15 -5 -3 353.86 447.68 155.12 o 15 -5 -2 10718.70 10764.80 119.50 o 15 -5 -1 248.32 155.79 65.05 o 15 -5 0 1997.56 2032.46 61.72 o 15 -5 1 10297.80 11107.90 96.47 o 15 -5 2 22183.90 23057.60 117.93 o 15 -5 3 15550.30 16094.90 94.50 o 15 -5 4 2993.16 2894.04 61.06 o 15 -5 5 4933.22 4854.07 117.12 o 15 -5 6 9021.91 8364.43 116.48 o 15 -5 7 3616.70 3191.42 120.45 o 15 -1 -3 6253.28 5864.58 139.82 o 15 -1 -2 3029.31 2978.43 91.42 o 15 -1 -1 2671.21 2703.13 71.40 o 15 -1 0 1456.52 1411.85 63.39 o 15 -1 1 1318.75 1372.15 67.39 o 15 -1 2 54.21 103.41 49.04 o 15 -1 3 556.53 594.13 51.04 o 15 -1 4 696.11 699.22 59.38 o 15 -1 5 1662.99 1591.35 45.71 o 15 -1 6 1887.50 1915.31 68.06 o 15 -1 7 1777.34 1800.53 72.73 o 15 -1 8 1158.12 1093.23 231.52 o 15 3 -3 3273.04 2442.32 147.14 o 15 3 -2 7467.48 7039.09 147.84 o 15 3 -1 13309.70 13336.90 144.22 o 15 3 0 26988.70 26711.50 157.04 o 15 3 1 7058.60 6847.21 95.45 o 15 3 2 5966.40 6015.56 76.42 o 15 3 3 9709.94 9981.11 142.54 o 15 3 4 16053.20 15640.40 103.52 o 15 3 5 4826.51 4713.35 76.75 o 15 3 6 14.78 -10.67 44.70 < 15 3 7 3.33 4.00 46.70 < 15 3 8 910.18 875.70 66.72 o 15 3 9 19.87 34.36 100.41 < 15 7 -1 1248.16 1160.29 101.08 o 15 7 0 15466.20 15174.00 130.88 o 15 7 1 9061.51 8830.09 91.79 o 15 7 2 20578.10 20352.60 104.88 o 15 7 3 5621.27 5384.30 64.40 o 15 7 4 14588.90 14319.00 94.83 o 15 7 5 23905.30 23518.70 128.63 o 15 7 6 9431.15 9360.24 92.46 o 15 7 7 4281.31 4219.92 73.74 o 15 7 8 1625.54 1658.40 68.39 o 15 7 9 2261.30 2188.26 107.76 o 15 7 10 2465.66 2517.26 111.77 o 15 11 0 928.43 813.32 123.43 o 15 11 1 445.62 559.77 103.75 o 15 11 2 3907.29 3794.38 77.08 o 15 11 3 423.64 426.66 49.71 o 15 11 4 11148.80 11232.10 100.14 o 15 11 5 7809.39 7794.59 77.09 o 15 11 6 922.01 941.09 44.37 o 15 11 7 8146.06 8024.30 101.46 o 15 11 8 5280.25 5302.97 116.12 o 15 11 9 7328.41 7596.00 101.45 o 15 11 10 638.76 647.17 81.73 o 15 15 2 1415.33 1562.30 120.77 o 15 15 3 12914.30 13182.80 214.33 o 15 15 4 383.84 422.66 61.05 o 15 15 5 282.36 241.18 59.71 o 15 15 6 547.44 601.47 45.04 o 15 15 7 107.43 116.09 45.70 o 15 15 8 449.40 479.70 47.70 o 15 15 9 6897.75 6924.36 98.78 o 15 15 10 230.97 258.86 66.38 o 15 19 4 1858.46 1883.95 128.44 o 15 19 5 12040.50 11893.20 178.93 o 15 19 6 4743.10 4674.16 145.48 o 15 19 7 576.05 557.77 68.39 o 15 19 8 6535.85 6451.35 146.50 o 15 19 9 57.15 52.37 60.04 < 15 19 10 3524.39 3536.07 78.74 o 15 23 9 146.37 140.77 156.12 < 16 -24 -5 75.48 168.79 142.11 < 16 -24 -4 40.99 46.37 74.06 < 16 -24 -3 41.15 59.71 85.73 < 16 -24 -2 40.57 86.40 75.72 < 16 -20 -6 2977.90 2789.26 171.49 o 16 -20 -5 4.62 77.39 137.77 < 16 -20 -4 766.41 778.62 97.08 o 16 -20 -3 20.47 65.38 89.73 < 16 -20 -2 403.32 384.63 71.39 o 16 -20 -1 37.98 34.36 76.39 < 16 -20 0 1689.36 1603.69 99.08 o 16 -20 1 57.84 72.05 87.07 < 16 -16 -6 28.02 62.71 119.42 < 16 -16 -5 685.64 539.42 107.75 o 16 -16 -4 1637.06 1572.66 95.41 o 16 -16 -3 930.41 775.29 108.75 o 16 -16 -2 3.12 25.02 78.73 < 16 -16 -1 10.74 4.00 67.72 < 16 -16 0 1730.89 1781.85 90.08 o 16 -16 1 285.98 285.22 78.73 o 16 -16 2 7413.95 7550.34 159.19 o 16 -16 3 18.70 101.07 82.73 < 16 -12 -5 428.45 489.38 207.83 o 16 -12 -4 291.39 262.87 80.39 o 16 -12 -3 8845.79 8846.30 173.22 o 16 -12 -2 1445.43 1416.18 78.40 o 16 -12 -1 120.91 127.76 51.04 o 16 -12 0 0.25 42.70 43.37 < 16 -12 1 20.93 -1.00 51.37 < 16 -12 2 3344.88 3371.20 82.08 o 16 -12 3 4566.03 4488.58 112.45 o 16 -12 4 4386.58 4569.95 108.11 o 16 -12 5 288.33 276.88 97.74 o 16 -8 -5 23.26 71.39 138.10 < 16 -8 -4 629.56 730.91 126.10 o 16 -8 -3 9861.74 9810.45 177.57 o 16 -8 -2 5181.31 4968.27 133.81 o 16 -8 -1 2583.61 2539.97 68.06 o 16 -8 0 1405.55 1424.52 60.38 o 16 -8 1 683.53 780.62 60.05 o 16 -8 2 538.09 547.09 45.70 o 16 -8 3 5243.52 5521.23 79.75 o 16 -8 4 2585.79 2740.14 95.09 o 16 -8 5 9832.27 9478.33 146.20 o 16 -8 6 686.15 622.49 100.08 o 16 -4 -4 794.04 737.25 142.78 o 16 -4 -3 1790.28 1698.12 143.12 o 16 -4 -2 4028.23 4059.01 113.44 o 16 -4 -1 8507.53 8379.32 106.14 o 16 -4 0 7363.69 7406.69 109.47 o 16 -4 1 262.30 379.29 50.04 o 16 -4 2 2959.93 3234.71 79.74 o 16 -4 3 4899.59 5248.92 65.74 o 16 -4 4 373.46 370.95 45.03 o 16 -4 5 19848.70 18816.30 150.63 o 16 -4 6 147.98 111.08 66.38 < 16 -4 7 5448.87 4895.27 184.87 o 16 0 -3 272.77 257.53 137.10 < 16 0 -2 895.52 927.07 86.40 o 16 0 -1 4385.84 4165.87 134.13 o 16 0 0 12891.10 12733.70 142.89 o 16 0 1 5326.17 5478.63 86.43 o 16 0 2 2193.38 2325.74 67.06 o 16 0 3 77.43 0.00 75.72 < 16 0 4 1860.41 1864.95 65.06 o 16 0 5 13708.20 13176.80 105.17 o 16 0 6 83.48 134.77 54.37 o 16 0 7 13764.60 13534.60 135.88 o 16 0 8 3743.73 3519.09 106.10 o 16 4 -2 154.37 85.06 92.40 < 16 4 -1 0.97 -4.00 78.39 < 16 4 0 8357.39 8613.74 108.47 o 16 4 1 10400.60 10203.10 97.80 o 16 4 2 2507.84 2470.57 67.73 o 16 4 3 1587.56 1621.04 67.39 o 16 4 4 14.57 37.03 40.03 < 16 4 5 14.27 63.71 45.70 < 16 4 6 1331.52 1397.16 70.39 o 16 4 7 11576.40 11694.20 108.82 o 16 4 8 1182.91 1216.66 71.73 o 16 4 9 1388.88 1469.89 100.08 o 16 8 0 356.52 354.27 84.73 o 16 8 1 4705.69 4832.63 84.42 o 16 8 2 3324.04 3412.56 66.73 o 16 8 3 5917.33 5893.20 78.75 o 16 8 4 494.55 510.73 47.37 o 16 8 5 2800.28 2821.93 67.40 o 16 8 6 4309.91 4312.70 98.10 o 16 8 7 14.38 15.68 47.04 < 16 8 8 15985.50 15753.80 129.22 o 16 8 9 891.37 919.40 81.73 o 16 8 10 357.47 376.29 88.07 o 16 12 1 173.92 131.43 111.08 < 16 12 2 468.47 566.44 74.06 o 16 12 3 5651.04 5848.68 87.43 o 16 12 4 23.77 -6.00 47.70 < 16 12 5 2919.58 2883.99 52.38 o 16 12 6 3833.79 3993.90 67.73 o 16 12 7 3037.28 3100.21 55.72 o 16 12 8 19570.50 19876.80 110.21 o 16 12 9 268.80 251.19 64.72 o 16 12 10 13313.00 13183.90 203.65 o 16 16 3 1692.78 1594.69 128.11 o 16 16 4 740.78 796.30 94.74 o 16 16 5 1003.70 1003.48 73.73 o 16 16 6 399.20 435.67 63.38 o 16 16 7 1214.74 1338.43 68.72 o 16 16 8 4933.07 5065.28 114.79 o 16 16 9 586.47 612.15 55.04 o 16 16 10 15249.30 15535.40 118.87 o 16 20 6 497.43 589.12 137.11 o 16 20 7 198.12 196.15 120.43 < 16 20 8 58.16 45.70 78.39 < 16 20 9 4.30 -22.02 80.73 < 16 20 10 1051.03 1104.90 105.75 o 17 -23 -4 1537.18 1705.43 102.42 o 17 -23 -3 9170.95 9127.28 144.86 o 17 -23 -2 447.08 531.74 83.40 o 17 -19 -5 9910.50 9810.28 216.63 o 17 -19 -4 1405.06 1546.62 106.75 o 17 -19 -3 17256.10 18582.20 209.04 o 17 -19 -2 8997.00 9577.33 137.84 o 17 -19 -1 16729.00 17154.40 198.68 o 17 -19 0 4412.33 4333.06 136.47 o 17 -19 1 460.58 442.34 88.40 o 17 -15 -5 2809.21 2593.38 151.47 o 17 -15 -4 860.53 724.24 124.10 o 17 -15 -3 9838.88 9691.61 183.58 o 17 -15 -2 1665.18 1942.64 78.40 o 17 -15 -1 19100.10 20389.60 190.03 o 17 -15 0 5249.53 5594.93 110.12 o 17 -15 1 10217.30 10626.80 161.22 o 17 -15 2 15920.90 16407.90 195.33 o 17 -15 3 2894.56 3028.13 115.44 o 17 -11 -5 3424.09 2936.81 167.16 o 17 -11 -4 4401.05 4179.56 159.49 o 17 -11 -3 540.82 507.39 98.08 o 17 -11 -2 66.30 146.44 87.07 < 17 -11 -1 2466.43 2516.59 74.07 o 17 -11 0 3006.03 3047.17 82.08 o 17 -11 1 4063.09 4205.84 86.75 o 17 -11 2 7132.27 7654.00 108.13 o 17 -11 3 4142.51 4166.81 104.10 o 17 -11 4 3800.79 3973.21 137.80 o 17 -11 5 844.83 841.00 102.75 o 17 -7 -4 6732.52 6267.92 198.23 o 17 -7 -3 8248.74 8059.67 179.22 o 17 -7 -2 12775.20 12085.60 187.62 o 17 -7 -1 1242.08 1221.34 75.40 o 17 -7 0 12029.00 12445.30 103.82 o 17 -7 1 3096.50 3406.54 92.09 o 17 -7 2 6770.12 7360.60 92.11 o 17 -7 3 31.32 38.70 43.03 < 17 -7 4 52.99 141.44 68.72 o 17 -7 5 400.52 308.90 70.72 o 17 -7 6 119.02 136.77 99.41 < 17 -3 -3 4041.46 4042.01 165.83 o 17 -3 -2 7645.39 7540.08 170.21 o 17 -3 -1 11925.70 11571.60 141.87 o 17 -3 0 26212.20 26609.80 168.40 o 17 -3 1 12404.20 12986.50 106.83 o 17 -3 2 12478.10 13607.70 114.84 o 17 -3 3 9426.71 9831.20 115.82 o 17 -3 4 16637.30 17044.30 108.53 o 17 -3 5 10129.40 10350.70 103.81 o 17 -3 6 1262.31 1174.63 86.40 o 17 -3 7 595.11 493.72 85.40 o 17 1 -2 216.20 217.16 83.40 o 17 1 -1 449.43 499.72 72.72 o 17 1 0 4656.90 4581.04 111.45 o 17 1 1 16330.30 16429.10 136.57 o 17 1 2 9416.23 9778.09 126.50 o 17 1 3 6201.57 6463.71 108.46 o 17 1 4 8292.82 8528.16 114.81 o 17 1 5 21526.50 21135.80 145.63 o 17 1 6 13898.50 13710.40 132.21 o 17 1 7 3745.99 3596.82 71.74 o 17 1 8 2016.28 1778.54 96.75 o 17 5 -1 901.41 894.38 78.40 o 17 5 0 1651.17 1711.45 71.73 o 17 5 1 23.02 37.36 66.72 < 17 5 2 749.42 778.28 55.04 o 17 5 3 1846.84 1929.99 65.39 o 17 5 4 116.65 138.44 49.70 o 17 5 5 5064.82 4988.62 101.11 o 17 5 6 1549.87 1485.25 63.39 o 17 5 7 2114.64 2113.84 66.06 o 17 5 8 5040.65 4814.38 101.44 o 17 5 9 3379.23 3469.97 116.44 o 17 9 0 4181.98 4085.10 274.27 o 17 9 1 1868.31 1849.26 74.73 o 17 9 2 13284.70 13366.30 110.17 o 17 9 3 7735.00 7696.98 110.80 o 17 9 4 11450.50 11478.20 89.13 o 17 9 5 764.78 810.64 58.71 o 17 9 6 2597.14 2662.07 64.73 o 17 9 7 2773.06 2961.04 74.07 o 17 9 8 191.60 199.48 55.04 o 17 9 9 122.53 168.79 78.39 o 17 9 10 1880.05 1925.66 96.75 o 17 13 2 6921.09 6614.74 194.23 o 17 13 3 5637.65 5673.83 114.12 o 17 13 4 20496.00 20431.30 166.33 o 17 13 5 4565.25 4509.93 86.09 o 17 13 6 15217.20 15012.50 110.52 o 17 13 7 2836.03 2836.60 63.39 o 17 13 8 5748.99 5695.54 74.08 o 17 13 9 7672.02 7640.57 104.13 o 17 13 10 77.67 101.74 77.39 < 17 17 4 4082.75 3851.84 130.46 o 17 17 5 385.19 394.97 99.74 o 17 17 6 10569.50 10028.20 145.87 o 17 17 7 4452.26 4357.76 112.45 o 17 17 8 11991.80 12080.10 138.20 o 17 17 9 3612.23 3497.71 81.75 o 17 17 10 134.95 86.40 66.72 < 18 -22 -3 252.86 248.19 82.73 o 18 -22 -2 1015.28 996.80 87.74 o 18 -22 -1 33.81 65.72 174.80 < 18 -18 -5 2214.47 1622.77 219.53 o 18 -18 -4 191.33 210.16 97.41 o 18 -18 -3 1167.11 1267.37 119.43 o 18 -18 -2 3181.85 3248.05 111.44 o 18 -18 -1 2336.32 2265.68 118.11 o 18 -18 0 0.85 13.68 94.74 < 18 -18 1 459.85 427.33 80.06 o 18 -14 -4 35.71 -3.67 110.75 < 18 -14 -3 3335.24 3408.56 146.47 o 18 -14 -2 2118.22 2300.01 87.74 o 18 -14 -1 1988.81 1899.98 79.74 o 18 -14 0 2031.76 2224.60 101.42 o 18 -14 1 1268.81 1305.74 103.08 o 18 -14 2 1109.41 1162.94 100.08 o 18 -14 3 7.94 10.67 87.40 < 18 -10 -4 1155.41 912.74 142.12 o 18 -10 -3 1314.41 1278.39 135.45 o 18 -10 -2 73.13 72.05 106.08 < 18 -10 -1 782.69 727.24 87.40 o 18 -10 0 4264.51 4364.05 89.42 o 18 -10 1 5727.94 5939.49 98.44 o 18 -10 2 308.54 328.25 58.04 o 18 -10 3 868.36 971.78 64.05 o 18 -10 4 3341.21 3424.91 108.77 o 18 -10 5 425.47 426.66 88.40 o 18 -6 -3 8.49 11.68 131.43 < 18 -6 -2 809.24 699.56 94.74 o 18 -6 -1 175.41 157.12 72.05 o 18 -6 0 649.59 631.50 58.38 o 18 -6 1 9044.87 9060.45 96.12 o 18 -6 2 9816.26 10566.90 112.15 o 18 -6 3 2130.18 2120.19 61.72 o 18 -6 4 400.26 419.32 50.04 o 18 -6 5 494.00 471.70 68.72 o 18 -6 6 2500.88 2395.15 129.45 o 18 -2 -2 1089.87 1156.27 134.78 o 18 -2 -1 161.27 195.48 81.39 o 18 -2 0 1017.64 1073.20 90.74 o 18 -2 1 3464.65 3538.39 70.40 o 18 -2 2 14097.90 14303.50 103.17 o 18 -2 3 7295.47 7585.08 109.46 o 18 -2 4 4439.62 4631.71 85.09 o 18 -2 5 248.22 218.83 58.71 o 18 -2 6 12.26 3.00 63.71 < 18 -2 7 153.23 124.76 70.05 < 18 2 -1 11.92 -2.00 79.73 < 18 2 0 1444.79 1424.85 71.73 o 18 2 1 101.15 156.12 62.71 o 18 2 2 3762.36 3947.85 102.10 o 18 2 3 6259.78 6431.27 114.46 o 18 2 4 15256.20 15122.10 116.20 o 18 2 5 49.74 79.06 57.04 < 18 2 6 3162.57 2918.06 85.41 o 18 2 7 3872.77 3773.02 74.41 o 18 2 8 1245.01 1180.97 84.07 o 18 6 0 1617.68 1510.61 80.07 o 18 6 1 515.70 502.06 63.38 o 18 6 2 126.54 116.09 58.04 < 18 6 3 759.27 781.95 55.71 o 18 6 4 9505.70 9456.17 93.46 o 18 6 5 2830.45 2864.63 97.42 o 18 6 6 5959.98 5595.18 90.77 o 18 6 7 3046.66 2979.10 88.08 o 18 6 8 3300.97 3155.98 97.76 o 18 6 9 8904.24 8677.86 132.17 o 18 10 1 564.72 505.06 186.48 o 18 10 2 449.02 484.04 64.38 o 18 10 3 719.01 751.59 73.06 o 18 10 4 953.25 939.09 62.72 o 18 10 5 4880.09 4823.01 87.42 o 18 10 6 4192.98 3986.64 106.77 o 18 10 7 27.72 40.70 55.71 < 18 10 8 301.33 328.92 58.38 o 18 10 9 2734.43 2603.37 86.41 o 18 14 3 757.68 703.56 95.08 o 18 14 4 1124.20 1106.23 84.74 o 18 14 5 1184.08 1189.31 77.40 o 18 14 6 946.39 980.79 57.38 o 18 14 7 4682.11 4758.89 76.08 o 18 14 8 285.28 307.57 59.04 o 18 14 9 56.30 60.71 59.71 < 18 14 10 812.29 760.60 78.73 o 18 18 6 360.31 345.93 123.10 o 18 18 7 4420.59 4097.17 120.46 o 18 18 8 157.66 103.41 69.72 < 18 18 9 3236.24 3181.67 97.43 o 19 -21 -3 9.25 178.47 138.10 < 19 -21 -2 4403.39 4692.77 183.85 o 19 -21 -1 1232.17 1174.63 222.18 o 19 -17 -4 9929.63 10073.00 219.96 o 19 -17 -3 1081.85 1253.68 134.78 o 19 -17 -2 79.52 34.03 107.41 < 19 -17 -1 3561.36 3797.65 130.79 o 19 -17 0 8.02 15.01 92.74 < 19 -17 1 1561.88 1564.98 91.74 o 19 -17 2 2884.79 2838.96 133.46 o 19 -13 -4 10582.90 9481.58 207.96 o 19 -13 -3 7504.62 7219.00 182.22 o 19 -13 -2 9490.72 9870.33 158.88 o 19 -13 -1 9405.07 9857.91 145.52 o 19 -13 0 1607.80 1637.05 83.40 o 19 -13 1 20367.70 21235.40 194.05 o 19 -13 2 3280.95 3365.17 115.11 o 19 -13 3 4258.02 4453.47 123.12 o 19 -13 4 60.68 27.35 119.42 < 19 -9 -3 913.04 795.64 140.11 o 19 -9 -2 6227.49 6017.07 177.53 o 19 -9 -1 10265.80 10583.10 154.88 o 19 -9 0 7215.40 7640.67 153.18 o 19 -9 1 20521.30 21443.80 186.70 o 19 -9 2 4393.75 4736.78 96.43 o 19 -9 3 16504.20 17671.00 140.58 o 19 -9 4 6516.82 6751.35 116.80 o 19 -9 5 11190.60 11486.40 162.57 o 19 -5 -3 11.86 -74.06 128.43 < 19 -5 -2 3.12 14.34 128.76 < 19 -5 -1 589.36 598.47 74.06 o 19 -5 0 376.06 428.33 80.06 o 19 -5 1 9444.51 9836.28 118.49 o 19 -5 2 2774.52 2892.98 94.42 o 19 -5 3 3501.93 3751.59 96.76 o 19 -5 4 1335.74 1517.92 55.71 o 19 -5 5 13980.30 14249.60 145.90 o 19 -5 6 9523.63 9534.62 137.51 o 19 -1 -2 2562.79 2369.81 126.11 o 19 -1 -1 3958.21 3725.00 106.77 o 19 -1 0 4884.66 5018.21 159.83 o 19 -1 1 3823.49 4024.93 95.09 o 19 -1 2 1298.73 1282.06 73.73 o 19 -1 3 324.89 330.92 64.38 o 19 -1 4 423.36 394.64 77.73 o 19 -1 5 0.39 9.34 54.71 < 19 -1 6 491.20 542.42 70.05 o 19 -1 7 893.44 846.68 80.06 o 19 -1 8 1093.67 930.42 126.44 o 19 3 -1 8678.97 7728.24 192.58 o 19 3 0 6853.02 6899.01 130.49 o 19 3 1 5544.66 5362.78 100.78 o 19 3 2 9665.53 9846.05 127.50 o 19 3 3 22165.20 22642.80 167.35 o 19 3 4 8926.44 9001.23 91.45 o 19 3 5 5052.01 5040.29 86.42 o 19 3 6 1005.68 1082.87 76.06 o 19 3 7 7610.68 7385.88 104.46 o 19 3 8 2568.29 2282.73 120.44 o 19 7 1 2729.82 2631.40 95.75 o 19 7 2 3698.81 3730.95 94.09 o 19 7 3 8766.57 8834.23 123.82 o 19 7 4 10874.60 10608.50 123.84 o 19 7 5 21496.40 21550.50 163.67 o 19 7 6 3174.19 3318.44 109.10 o 19 7 7 10999.10 10808.20 132.19 o 19 7 8 5618.13 5333.12 103.11 o 19 7 9 10204.70 10018.70 163.89 o 19 11 3 70.93 94.40 75.06 < 19 11 4 550.30 585.46 62.38 o 19 11 5 2627.82 2661.74 63.39 o 19 11 6 313.67 304.23 54.04 o 19 11 7 11180.60 11135.40 127.85 o 19 11 8 2545.76 2635.70 100.42 o 19 11 9 6756.08 6747.82 136.82 o 19 15 5 1693.11 1597.36 90.74 o 19 15 6 6576.38 6588.55 133.49 o 19 15 7 50.03 71.72 61.71 < 19 15 8 22.71 32.36 57.38 < 19 15 9 2955.96 3014.13 87.75 o 20 -20 -1 199.49 319.24 225.84 < 20 -16 -3 1806.18 1463.92 117.77 o 20 -16 -2 759.24 845.34 221.84 o 20 -16 -1 40.06 47.37 99.41 < 20 -16 0 0.01 11.68 96.74 < 20 -16 1 317.77 354.61 90.74 o 20 -16 2 1596.09 1489.59 165.81 o 20 -12 -3 10261.20 9586.18 205.62 o 20 -12 -2 253.82 233.18 99.41 o 20 -12 -1 1200.46 1215.33 99.41 o 20 -12 0 284.90 317.24 70.72 o 20 -12 1 163.81 111.75 87.07 < 20 -12 2 546.34 572.78 73.72 o 20 -12 3 4263.58 4269.29 119.12 o 20 -12 4 2291.50 2325.06 110.76 o 20 -8 -2 1276.09 1103.91 114.09 o 20 -8 -1 4287.76 4495.18 164.16 o 20 -8 0 826.10 1022.48 77.73 o 20 -8 1 812.63 931.07 73.73 o 20 -8 2 104.54 105.41 75.06 < 20 -8 3 3465.81 3574.07 83.08 o 20 -8 4 3225.72 3316.45 93.75 o 20 -8 5 5498.61 5630.42 121.80 o 20 -4 -2 1109.86 919.75 186.15 o 20 -4 -1 3674.69 3567.12 106.10 o 20 -4 0 184.43 105.41 75.72 < 20 -4 1 1102.25 1163.61 69.72 o 20 -4 2 36.70 142.11 74.06 < 20 -4 3 1092.78 1126.91 67.39 o 20 -4 4 2026.97 2112.16 73.40 o 20 -4 5 10703.20 10939.90 131.85 o 20 -4 6 620.17 690.88 93.07 o 20 -4 7 3612.32 2998.24 153.15 o 20 0 -1 530.61 429.33 84.40 o 20 0 0 2797.88 2655.10 104.76 o 20 0 1 1197.90 1075.88 88.74 o 20 0 2 382.01 406.98 72.06 o 20 0 3 233.35 184.14 71.72 o 20 0 4 314.02 325.92 60.38 o 20 0 5 4558.47 4501.25 99.10 o 20 0 6 4430.02 4473.19 102.10 o 20 0 7 8766.87 8468.49 127.50 o 20 4 0 5770.19 5332.21 167.85 o 20 4 1 2606.96 2548.97 77.74 o 20 4 2 2081.57 2024.10 73.40 o 20 4 3 126.46 140.77 60.05 o 20 4 4 104.96 101.74 59.04 < 20 4 5 14.04 41.36 63.38 < 20 4 6 4041.97 3918.20 98.43 o 20 4 7 5983.50 5939.24 110.46 o 20 4 8 2781.01 2756.19 84.08 o 20 8 2 5774.42 5667.90 100.78 o 20 8 3 523.46 508.73 66.38 o 20 8 4 290.54 305.57 53.04 o 20 8 5 584.33 585.79 59.71 o 20 8 6 654.30 646.84 72.39 o 20 8 7 284.11 297.56 58.71 o 20 8 8 9023.69 8585.11 153.53 o 20 8 9 116.87 91.40 89.73 < 20 12 4 1674.75 1726.46 90.41 o 20 12 5 1820.38 1726.48 88.74 o 20 12 6 55.27 27.35 56.38 < 20 12 7 450.88 424.66 65.38 o 20 12 8 3786.13 3622.54 94.09 o 20 12 9 21.11 30.02 65.72 < 20 16 7 956.75 785.30 123.77 o 20 16 8 96.03 46.03 100.74 < 21 -15 -2 334.76 301.23 126.76 o 21 -15 -1 8097.89 8424.45 282.35 o 21 -15 0 2515.42 2594.33 125.45 o 21 -15 1 3314.37 3608.42 140.47 o 21 -15 2 12012.70 12233.80 229.01 o 21 -11 -2 1797.22 1854.25 146.79 o 21 -11 -1 960.25 841.68 119.10 o 21 -11 0 1167.85 1255.02 87.40 o 21 -11 1 1198.64 1219.33 100.42 o 21 -11 2 2315.49 2247.32 92.42 o 21 -11 3 449.60 472.36 74.39 o 21 -11 4 2240.23 2371.10 108.43 o 21 -7 -2 3382.71 3149.00 157.48 o 21 -7 -1 4150.75 4343.67 156.49 o 21 -7 0 10263.80 10276.30 133.51 o 21 -7 1 6605.23 6871.52 130.48 o 21 -7 2 3342.13 3506.32 104.77 o 21 -7 3 2909.77 3164.91 72.73 o 21 -7 4 938.52 986.79 89.74 o 21 -7 5 4741.80 4938.78 137.14 o 21 -3 -1 5833.03 5360.25 145.49 o 21 -3 0 6015.50 5721.02 132.48 o 21 -3 1 5325.03 5448.81 107.78 o 21 -3 2 10731.20 10935.20 152.88 o 21 -3 3 14822.20 15222.50 144.24 o 21 -3 4 11842.40 12061.60 153.22 o 21 -3 5 7921.91 8147.30 107.80 o 21 -3 6 3232.03 3344.49 105.43 o 21 1 0 1960.14 1839.93 115.43 o 21 1 1 1431.31 1384.82 84.40 o 21 1 2 832.80 874.70 99.41 o 21 1 3 2516.84 2453.20 77.74 o 21 1 4 10834.30 10978.00 149.88 o 21 1 5 10840.40 11040.10 130.85 o 21 1 6 6262.53 6317.43 113.46 o 21 1 7 2793.40 2765.87 82.74 o 21 5 1 1609.39 1540.97 97.75 o 21 5 2 565.20 588.79 60.71 o 21 5 3 314.82 324.58 63.72 o 21 5 4 244.73 278.55 59.71 o 21 5 5 7.89 31.36 65.72 < 21 5 6 1043.09 1053.52 74.06 o 21 5 7 205.28 219.50 69.39 o 21 5 8 4092.69 4106.43 98.10 o 21 9 3 6009.25 5903.58 123.14 o 21 9 4 4037.07 3969.60 100.77 o 21 9 5 2130.89 2019.43 69.39 o 21 9 6 8599.99 8414.66 113.48 o 21 9 7 7749.73 7806.16 115.14 o 21 9 8 65.74 59.04 63.38 < 21 13 6 11698.30 11733.20 209.31 o 21 13 7 7630.07 7487.09 125.49 o 21 13 8 7338.37 7222.99 144.84 o 22 -14 -1 978.96 742.27 105.75 o 22 -14 0 7990.47 8259.88 194.91 o 22 -14 1 100.84 175.13 126.10 < 22 -14 2 279.39 282.88 123.43 o 22 -10 -1 1341.98 1120.59 90.74 o 22 -10 0 4014.30 4023.32 103.77 o 22 -10 1 1089.33 955.78 84.40 o 22 -10 2 1449.92 1511.26 88.07 o 22 -10 3 1.42 28.69 72.72 < 22 -10 4 203.41 222.84 130.43 < 22 -6 -1 702.74 595.47 104.75 o 22 -6 0 10.11 -21.35 93.40 < 22 -6 1 4586.17 4392.16 119.46 o 22 -6 2 2279.09 2304.37 103.76 o 22 -6 3 1124.73 1097.89 80.07 o 22 -6 4 277.77 273.54 84.73 o 22 -6 5 293.62 324.92 104.08 o 22 -2 0 5087.75 4831.11 117.79 o 22 -2 1 1465.34 1432.20 128.44 o 22 -2 2 1833.10 1579.69 126.11 o 22 -2 3 7358.93 7325.37 134.83 o 22 -2 4 7.78 55.37 66.05 < 22 -2 5 320.75 349.27 67.05 o 22 -2 6 12.59 14.68 76.06 < 22 2 1 111.32 162.12 75.06 o 22 2 2 37.30 89.73 74.72 < 22 2 3 6032.50 6067.07 101.45 o 22 2 4 1425.36 1420.85 70.39 o 22 2 5 364.52 355.27 78.06 o 22 2 6 36.79 79.39 72.05 < 22 2 7 1103.39 1130.92 84.74 o 22 6 3 2041.35 2033.77 76.73 o 22 6 4 2172.33 2077.82 85.74 o 22 6 5 1986.48 2004.74 82.40 o 22 6 6 1529.62 1479.91 74.06 o 22 6 7 132.72 97.41 62.38 < 22 10 5 3775.97 3838.42 115.45 o 22 10 6 4266.76 4122.15 81.42 o 22 10 7 166.01 164.46 70.39 o 23 -9 0 2244.43 2049.14 113.10 o 23 -9 1 4573.02 4280.06 118.46 o 23 -9 2 5402.56 5467.55 113.79 o 23 -9 3 10014.60 10175.50 204.61 o 23 -5 1 167.85 157.45 95.07 < 23 -5 2 46.26 14.01 105.75 < 23 -5 3 244.54 239.51 75.72 o 23 -5 4 2901.49 2846.63 98.42 o 23 -5 5 6293.57 6597.48 179.20 o 23 -1 1 2819.39 2772.22 123.11 o 23 -1 2 2222.11 2213.28 116.44 o 23 -1 3 2493.79 2567.97 101.76 o 23 -1 4 2931.86 2769.23 108.10 o 23 -1 5 567.84 548.43 68.72 o 23 -1 6 42.56 33.36 84.40 < 23 3 3 7410.80 7129.89 122.81 o 23 3 4 5425.19 5287.36 101.78 o 23 3 5 5077.34 5190.81 112.45 o 23 3 6 9217.25 8995.79 132.51 o 23 7 4 5689.89 4928.07 159.18 o 23 7 5 4036.15 3816.13 98.76 o 23 7 6 4060.23 3910.23 100.43 o 23 7 7 10108.60 9096.12 268.70 o 24 -8 1 1832.78 1729.15 175.15 o 24 -8 2 462.26 412.32 117.76 o 24 -4 2 89.36 79.06 99.74 < 24 -4 3 188.04 244.18 80.06 o 24 -4 4 3053.12 2698.19 114.44 o 24 0 3 303.65 289.22 70.05 o 24 0 4 30.39 53.37 83.73 < 24 0 5 1189.33 990.81 105.75 o 24 4 5 7.28 -27.02 149.11 < #======================================================================= data_alpha2 #======================================================================= # 5. CHEMICAL DATA _chemical_name_systematic ? _chemical_name_common ? _chemical_formula_moiety ? _chemical_formula_structural ? _chemical_formula_analytical ? _chemical_formula_iupac ? _chemical_formula_sum 'Fe2 O7 P2' _chemical_formula_weight 285.6 _chemical_melting_point ? _chemical_compound_source ? _chemical_absolute_configuration . #======================================================================= # 6. CRYSTAL DATA _space_group_crystal_system triclinic _space_group_ssg_name 'C-1(\a\b\g)0' loop_ _space_group_symop_ssg_id _space_group_symop_ssg_operation_algebraic 1 x1,x2,x3,x4 2 -x1,-x2,-x3,-x4 3 x1+1/2,x2+1/2,x3,x4 4 -x1+1/2,-x2+1/2,-x3,-x4 _cell_length_a 6.6393(6) _cell_length_b 8.4748(6) _cell_length_c 4.4839(3) _cell_angle_alpha 90.036(5) _cell_angle_beta 103.962(7) _cell_angle_gamma 92.929(6) _cell_volume 244.50(3) _cell_modulation_dimension 1 loop_ _cell_wave_vector_seq_id _cell_wave_vector_x _cell_wave_vector_y _cell_wave_vector_z 1 0.4489(3) 0.2517(3) 0.3646(3) _cell_formula_units_Z 2 _cell_measurement_temperature 300 _cell_measurement_reflns_used 10653 _cell_measurement_theta_min 3.88 _cell_measurement_theta_max 37.02 _cell_special_details ? _exptl_crystal_density_diffrn 3.8798 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_F_000 276 _exptl_crystal_type_of_structure mod _exptl_absorpt_coefficient_mu 6.566 _exptl_crystal_description 'plate' _exptl_crystal_colour 'light brown' _exptl_crystal_size_max 0.06 _exptl_crystal_size_mid 0.04 _exptl_crystal_size_min 0.01 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; STOE LANA, absorption correction by scaling of reflection intensities. J. Koziskova, F. Hahn, J. Richter, J. Kozisek, "Comparison of different absorption corrections on the model structure of tetrakis(\m~2~-acetato)- diaqua-di-copper(II)", Acta Chimica Slovaca, vol. 9, no. 2, 2016, pp. 136 - 140. Afterwards a spherical absorption correction was performed within STOE LANA. ; _exptl_absorpt_correction_T_min 0.3596 _exptl_absorpt_correction_T_max 0.5540 #======================================================================= # 7. EXPERIMENTAL DATA _diffrn_measurement_device 'Eulerian 4-circle diffractometer' _diffrn_measurement_device_type 'STOE STADIVARI' _diffrn_detector 'EIGER2 1M CDTE' _diffrn_detector_type ? _diffrn_detector_area_resol_mean 13.33 _diffrn_source 'Axo_Mo' _diffrn_source_type ? _diffrn_radiation_probe x-ray _diffrn_source_target ? _diffrn_source_voltage 60 _diffrn_source_current 0.830 _diffrn_source_power 0.050 _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_monochromator 'Graded multilayer mirror' _diffrn_radiation_polarisn_norm -90 _diffrn_radiation_collimation '1.2 0.6 mm diameter' _diffrn_ambient_temperature 300 _diffrn_measurement_method 'rotation method, \w scans' _diffrn_measurement_details ; 2098 frames, detector distance = 40 mm ; _diffrn_reflns_number 21588 _diffrn_reflns_theta_min 2.84 _diffrn_reflns_theta_max 37.04 _diffrn_reflns_theta_full 36.13 _diffrn_measured_fraction_theta_max 0.94 _diffrn_measured_fraction_theta_full 0.98 _diffrn_reflns_av_R_equivalents 0.0363 _diffrn_reflns_av_unetI/netI ? _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_l_min -6 _diffrn_reflns_limit_l_max 8 _diffrn_reflns_limit_index_m_1_min -2 _diffrn_reflns_limit_index_m_1_max 2 _diffrn_reflns_reduction_process ? _diffrn_standards_number ? _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% ? loop_ _diffrn_standard_refln_index_h _diffrn_standard_refln_index_k _diffrn_standard_refln_index_l ? ? ? #======================================================================= # 8. REFINEMENT DATA _refine_special_details ? _reflns_number_total 5785 _reflns_number_gt 3402 _reflns_threshold_expression 'I>3\s(I)' _refine_ls_structure_factor_coef Fsqd _refine_ls_R_factor_gt 0.0265 _refine_ls_wR_factor_gt 0.0765 _refine_ls_R_factor_all 0.0448 _refine_ls_wR_factor_ref 0.0805 _refine_ls_goodness_of_fit_ref 1.1018 _refine_ls_goodness_of_fit_gt 1.3855 _refine_ls_restrained_S_gt ? _refine_ls_restrained_S_all ? _refine_ls_number_reflns 5785 _refine_ls_number_parameters 251 _refine_ls_number_restraints 0 _refine_ls_number_constraints 4 _refine_ls_weighting_scheme sigma _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.04P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_hydrogen_treatment ? _refine_ls_shift/su_max 0.0378 _refine_ls_shift/su_mean 0.0070 _refine_diff_density_max 1.13 _refine_diff_density_min -1.15 _refine_ls_extinction_method 'B-C type 1 Gaussian isotropic (Becker & Coppens, 1974)' _refine_ls_extinction_coef 690(50) _refine_ls_extinction_expression ? _refine_ls_abs_structure_details ? _refine_ls_abs_structure_Flack ? _refine_ls_abs_structure_Rogers ? loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Fe 0.3492 0.8593 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' O 0.0115 0.0063 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' P 0.1048 0.0969 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' _computing_data_collection ; X-Area Pilatus3_SV 1.31.175.0 (STOE, 2021) ; _computing_cell_refinement ; X-Area Recipe 1.37.0.0 (STOE, 2021) ; _computing_data_reduction ; X-Area Integrate 2.5.1.0 (STOE, 2021) X-Area X-Red 2.3.0.0 (STOE, 2021) ; _computing_publication_material ; STOE & Cie GmbH, X-Area, software package for collecting single-crystal or multi-domain crystal data on STOE area-detector diffractometers, for image processing, for the correction and scaling of reflection intensities and for outlier rejection, version 2.0, Darmstadt 2021 ; _computing_structure_solution SUPERFLIP _computing_structure_refinement Jana2020 #======================================================================= # 9. ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_adp_type _atom_site_U_iso_or_equiv _atom_site_site_symmetry_multiplicity _atom_site_occupancy _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_disorder_assembly _atom_site_disorder_group Fe1 Fe 0.489014(18) 0.189884(13) 0.51774(3) Uani 0.01065(4) 4 1 d . . . P1 P 0.21133(3) 0.00069(3) -0.08996(5) Uani 0.00791(5) 4 1 d . . . O1 O 0.37351(9) 0.00434(8) 0.21420(14) Uani 0.00976(14) 4 1 d . . . O2 O 0.22535(10) 0.14714(7) -0.27860(15) Uani 0.01152(15) 4 1 d . . . O3 O 0.20953(11) -0.14842(8) -0.27222(16) Uani 0.01532(17) 4 1 d . . . O4 O 0 0 0 Uani 0.0260(3) 2 1 d . . . loop_ _atom_site_aniso_label _atom_site_aniso_type_symbol _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Fe1 Fe 0.01073(6) 0.00775(6) 0.01171(7) -0.00107(4) -0.00038(4) -0.00073(4) P1 P 0.00647(9) 0.00886(9) 0.00787(9) -0.00084(6) 0.00095(7) 0.00025(6) O1 O 0.0097(2) 0.0107(2) 0.0078(2) 0.00078(18) 0.00006(18) -0.00088(18) O2 O 0.0129(2) 0.0095(2) 0.0125(3) 0.00168(19) 0.0035(2) 0.0020(2) O3 O 0.0201(3) 0.0104(3) 0.0127(3) -0.0036(2) -0.0006(2) -0.0029(2) O4 O 0.0076(4) 0.0447(7) 0.0279(5) 0.0007(4) 0.0086(4) 0.0069(5) loop_ _atom_site_Fourier_wave_vector_seq_id _atom_site_Fourier_wave_vector_q1_coeff 1 1 2 2 loop_ _atom_site_occ_special_func_atom_site_label _atom_site_occ_special_func_crenel_c _atom_site_occ_special_func_crenel_w P1 0.06224(2) 1 O1 0.24683(7) 1 O2 0.03661(7) 1 O3 -0.04254(8) 1 O4 0 1 loop_ _atom_site_displace_Fourier_id _atom_site_displace_Fourier_atom_site_label _atom_site_displace_Fourier_axis _atom_site_displace_Fourier_wave_vector_seq_id Fe1x1 Fe1 x 1 Fe1y1 Fe1 y 1 Fe1z1 Fe1 z 1 Fe1x2 Fe1 x 2 Fe1y2 Fe1 y 2 Fe1z2 Fe1 z 2 loop_ _atom_site_displace_Fourier_param_id _atom_site_displace_Fourier_param_cos _atom_site_displace_Fourier_param_sin Fe1x1 0.01116(2) -0.01437(2) Fe1y1 -0.001895(15) 0.002900(16) Fe1z1 -0.00777(3) 0.01180(3) Fe1x2 0.00034(3) 0.00330(3) Fe1y2 0.00020(3) 0.00060(2) Fe1z2 -0.00193(5) -0.00102(5) loop_ _jana_atom_site_displace_XHarm_site_label _jana_atom_site_displace_XHarm_axis _jana_atom_site_displace_XHarm_param_order _jana_atom_site_displace_XHarm_param_coeff P1 x 1 0.00132(6) P1 y 1 -0.01279(5) P1 z 1 -0.00369(9) P1 x 2 0.00211(4) P1 y 2 0.00191(3) P1 z 2 0.00225(5) P1 x 3 -0.00231(7) P1 y 3 -0.00628(6) P1 z 3 0.00231(11) P1 x 4 0.00079(5) P1 y 4 0.00016(5) P1 z 4 -0.00138(9) O1 x 1 -0.00092(15) O1 y 1 -0.00528(12) O1 z 1 -0.0017(2) O1 x 2 0.00172(10) O1 y 2 0.00550(7) O1 z 2 0.00390(13) O1 x 3 -0.00103(18) O1 y 3 -0.00545(15) O1 z 3 0.0005(3) O1 x 4 0.00110(13) O1 y 4 0.00101(10) O1 z 4 -0.0009(2) O2 x 1 -0.02127(16) O2 y 1 -0.00618(12) O2 z 1 0.0067(2) O2 x 2 0.00015(11) O2 y 2 0.00135(8) O2 z 2 -0.00116(15) O2 x 3 -0.01243(18) O2 y 3 -0.00304(14) O2 z 3 0.0073(3) O2 x 4 -0.00025(15) O2 y 4 0.00022(11) O2 z 4 -0.0033(2) O3 x 1 0.03038(16) O3 y 1 -0.00676(12) O3 z 1 -0.0159(2) O3 x 2 0.00873(13) O3 y 2 0.00121(8) O3 z 2 0.00565(16) O3 x 3 0.00734(16) O3 y 3 -0.00246(14) O3 z 3 -0.0051(3) O3 x 4 0.00222(17) O3 y 4 -0.00072(11) O3 z 4 -0.0002(2) O4 x 1 -0.0046(2) O4 y 1 -0.0578(2) O4 z 1 -0.0162(4) O4 x 2 0 O4 y 2 0 O4 z 2 0 O4 x 3 -0.0013(2) O4 y 3 -0.0219(2) O4 z 3 0.0057(4) O4 x 4 0 O4 y 4 0 O4 z 4 0 loop_ _atom_site_U_Fourier_id _atom_site_U_Fourier_atom_site_label _atom_site_U_Fourier_tens_elem _atom_site_U_Fourier_wave_vector_seq_id Fe1U111 Fe1 U11 1 Fe1U221 Fe1 U22 1 Fe1U331 Fe1 U33 1 Fe1U121 Fe1 U12 1 Fe1U131 Fe1 U13 1 Fe1U231 Fe1 U23 1 Fe1U112 Fe1 U11 2 Fe1U222 Fe1 U22 2 Fe1U332 Fe1 U33 2 Fe1U122 Fe1 U12 2 Fe1U132 Fe1 U13 2 Fe1U232 Fe1 U23 2 loop_ _atom_site_U_Fourier_param_id _atom_site_U_Fourier_param_cos _atom_site_U_Fourier_param_sin Fe1U111 -0.00149(6) 0.00278(6) Fe1U221 0.00029(5) -0.00009(5) Fe1U331 0.00032(6) 0.00060(6) Fe1U121 -0.00025(4) -0.00010(4) Fe1U131 0.00056(5) -0.00182(5) Fe1U231 0.00032(4) 0.00038(4) Fe1U112 -0.00019(9) -0.00108(9) Fe1U222 -0.00013(10) -0.00005(10) Fe1U332 0.00025(12) 0.00011(11) Fe1U122 -0.00007(7) -0.00002(7) Fe1U132 -0.00059(8) 0.00030(8) Fe1U232 0.00002(8) 0.00004(8) loop_ _jana_atom_site_U_XHarm_atom_site_label _jana_atom_site_U_XHarm_tens_elem _jana_atom_site_U_XHarm_param_order _jana_atom_site_U_XHarm_param_coeff P1 U11 1 -0.00070(14) P1 U22 1 0.00009(15) P1 U33 1 -0.00017(18) P1 U12 1 0.00062(11) P1 U13 1 0.00026(13) P1 U23 1 -0.00052(12) P1 U11 2 -0.00001(9) P1 U22 2 -0.00115(11) P1 U33 2 -0.00043(9) P1 U12 2 0.00034(7) P1 U13 2 0.00014(7) P1 U23 2 -0.00066(8) P1 U11 3 -0.00014(16) P1 U22 3 0.00026(19) P1 U33 3 0.0000(2) P1 U12 3 0.00009(13) P1 U13 3 0.00001(16) P1 U23 3 -0.00023(15) P1 U11 4 -0.00027(14) P1 U22 4 0.00158(17) P1 U33 4 -0.00020(18) P1 U12 4 0.00004(12) P1 U13 4 0.00008(13) P1 U23 4 0.00039(13) O1 U11 1 0.0005(5) O1 U22 1 -0.0001(5) O1 U33 1 -0.0001(6) O1 U12 1 0.0000(4) O1 U13 1 0.0003(4) O1 U23 1 -0.0003(4) O1 U11 2 0.0002(3) O1 U22 2 -0.0001(3) O1 U33 2 -0.0001(3) O1 U12 2 0.0000(2) O1 U13 2 0.0001(2) O1 U23 2 -0.0004(2) O1 U11 3 -0.0005(5) O1 U22 3 0.0003(6) O1 U33 3 -0.0001(7) O1 U12 3 0.0000(5) O1 U13 3 -0.0002(5) O1 U23 3 -0.0001(5) O1 U11 4 0.0004(4) O1 U22 4 0.0007(5) O1 U33 4 0.0000(5) O1 U12 4 0.0004(3) O1 U13 4 0.0002(4) O1 U23 4 -0.0003(4) O2 U11 1 0.0012(4) O2 U22 1 0.0007(5) O2 U33 1 0.0000(5) O2 U12 1 0.0008(3) O2 U13 1 -0.0007(4) O2 U23 1 0.0001(4) O2 U11 2 0.0004(3) O2 U22 2 -0.0001(3) O2 U33 2 -0.0002(3) O2 U12 2 -0.0002(2) O2 U13 2 -0.0005(3) O2 U23 2 0.0000(2) O2 U11 3 0.0000(5) O2 U22 3 -0.0004(6) O2 U33 3 0.0007(6) O2 U12 3 0.0002(4) O2 U13 3 -0.0004(5) O2 U23 3 0.0001(5) O2 U11 4 -0.0015(5) O2 U22 4 -0.0001(5) O2 U33 4 -0.0001(5) O2 U12 4 -0.0002(4) O2 U13 4 0.0004(4) O2 U23 4 0.0004(4) O3 U11 1 -0.0077(4) O3 U22 1 -0.0007(4) O3 U33 1 -0.0015(5) O3 U12 1 0.0014(3) O3 U13 1 0.0025(4) O3 U23 1 -0.0003(3) O3 U11 2 -0.0028(5) O3 U22 2 -0.0011(3) O3 U33 2 -0.0009(3) O3 U12 2 0.0010(3) O3 U13 2 0.0013(3) O3 U23 2 -0.0008(3) O3 U11 3 -0.0029(5) O3 U22 3 0.0000(5) O3 U33 3 -0.0002(5) O3 U12 3 0.0004(4) O3 U13 3 0.0002(4) O3 U23 3 0.0000(4) O3 U11 4 -0.0013(6) O3 U22 4 0.0001(5) O3 U33 4 0.0004(6) O3 U12 4 -0.0001(5) O3 U13 4 -0.0006(5) O3 U23 4 0.0007(4) O4 U11 1 0 O4 U22 1 0 O4 U33 1 0 O4 U12 1 0 O4 U13 1 0 O4 U23 1 0 O4 U11 2 -0.0001(5) O4 U22 2 0.0030(12) O4 U33 2 -0.0013(7) O4 U12 2 -0.0003(7) O4 U13 2 0.0005(5) O4 U23 2 -0.0034(8) O4 U11 3 0 O4 U22 3 0 O4 U33 3 0 O4 U12 3 0 O4 U13 3 0 O4 U23 3 0 O4 U11 4 -0.0007(7) O4 U22 4 0.0145(13) O4 U33 4 0.0035(10) O4 U12 4 0.0007(8) O4 U13 4 0.0013(7) O4 U23 4 0.0030(9) #======================================================================= # 10. MOLECULAR GEOMETRY loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_ssg_symmetry_1 _geom_bond_site_ssg_symmetry_2 _geom_bond_distance_av _geom_bond_distance_min _geom_bond_distance_max _geom_bond_publ_flag Fe1 O1 . . 2.0724(19) 2.039(2) 2.112(2) ? Fe1 O1 . 2_6565 2.151(2) 2.119(2) 2.174(2) ? Fe1 O2 . 1_5565 2.178(2) 2.130(3) 2.226(3) ? Fe1 O2 . 4_5555 2.134(2) 2.104(2) 2.168(2) ? Fe1 O3 . 3_5565 2.013(2) 1.930(2) 2.066(2) ? Fe1 O3 . 2_6555 2.550(3) 2.245(3) 2.962(3) ? P1 O1 . . 1.5201(19) 1.504(2) 1.526(2) ? P1 O2 . . 1.520(2) 1.481(2) 1.525(2) ? P1 O3 . . 1.512(2) 1.493(2) 1.529(2) ? P1 O4 . . 1.5760(19) 1.494(3) 1.592(3) ? #------------------------------------------------------------------------------- # STOE DATA #------------------------------------------------------------------------------- #_STOE_detector_size_x '8.0 cm' #_STOE_detector_size_y '7.7 cm' #_STOE_detector_pixelsize_x '0.075 mm' #_STOE_detector_pixelsize_y '0.075 mm' #_STOE_detector_distance '40.0 mm' #_STOE_measurement_tube_power '49.8 W' #_STOE_measurement_total_run_number 22 #_STOE_measurement_total_frame_number 2098 #_STOE_measurement_min_exposure_per_frame '30.0 s' #_STOE_measurement_max_exposure_per_frame '30.0 s' #_STOE_measurement_mean_exposure_per_frame '30.0 s' #_STOE_measurement_total_exposure_time '17.5 h' #_STOE_evaluation_integration_A 12.7 #_STOE_evaluation_integration_B -0.6 #_STOE_evaluation_integration_EMS 0.020 #_STOE_evaluation_LANA_point_group '-1' #_STOE_evaluation_LANA_FS_max_order 3 #_STOE_evaluation_LANA_DXS_max_order - #_STOE_evaluation_LANA_DYS_max_order - #_STOE_evaluation_LANA_BIS_l_even_max 4 #_STOE_evaluation_LANA_BIS_l_odd_max 1 #_STOE_evaluation_LANA_BOS_l_even_max 4 #_STOE_evaluation_LANA_BOS_l_odd_max 1 #_STOE_evaluation_LANA_OR_c1 - #_STOE_evaluation_LANA_OR_c2 - #_STOE_evaluation_LANA_OR_c3 - #_STOE_evaluation_LANA_OR_c4 - #_STOE_evaluation_LANA_max_2theta_available 85.6 #_STOE_evaluation_LANA_max_2theta_desired 85.6 #_STOE_evaluation_LANA_number_refls_total 4315 #_STOE_evaluation_LANA_number_refls_outliers 0 #_STOE_evaluation_LANA_number_refls_after_OR 4315 #_STOE_evaluation_LANA_number_refls_unique 1167 #_STOE_evaluation_LANA_number_refls_written 21589 #_STOE_evaluation_LANA_completeness 64.9 #_STOE_evaluation_LANA_mean_redundancy 3.7 #_STOE_evaluation_LANA_table #; #--------------------------------------------------------------------- #2Theta 11.5 20.3 29.1 37.9 46.7 55.5 64.3 73.1 #--------------------------------------------------------------------- #<Resolution> 3.36 2.01 1.40 1.08 0.89 0.76 0.67 0.62 #N(total) 130 281 249 568 794 975 971 347 #<Redundancy> 9.3 6.7 3.2 4.2 4.2 3.8 3.2 2.4 #Complet. [%%] 100.0 100.0 98.8 100.0 100.0 100.0 99.7 39.2 #<I/sigma> 441.3 260.3 246.0 117.3 67.8 51.8 30.9 23.8 #R(int) 0.038 0.040 0.029 0.031 0.028 0.030 0.030 0.030 #--------------------------------------------------------------------- #; #======================================================================= # 11. STRUCTURE-FACTOR LIST loop_ _refln_index_h _refln_index_k _refln_index_l _refln_index_m_1 _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_include_status 2 0 0 -2 1.61 1.68 0.20 o 2 0 0 -1 74.49 71.34 0.39 o 2 0 0 0 152.65 127.03 0.59 o 2 0 0 1 41.60 41.79 0.56 o 2 0 0 2 8.21 9.06 0.84 o 4 0 0 -2 5.55 5.57 0.42 o 4 0 0 -1 28.44 27.94 0.64 o 4 0 0 0 7171.68 7311.19 7.23 o 4 0 0 1 348.96 358.98 2.14 o 4 0 0 2 1.09 2.24 1.34 < 6 0 0 -2 0.02 0.03 1.07 < 6 0 0 -1 44.39 47.44 2.02 o 6 0 0 0 991.09 1080.94 4.51 o 6 0 0 1 51.37 54.30 1.70 o 6 0 0 2 0.27 0.61 1.48 < 8 0 0 -2 4.11 4.11 1.09 o 8 0 0 -1 9.07 10.24 1.24 o 8 0 0 0 536.55 575.92 3.26 o 8 0 0 1 214.43 216.16 2.80 o 8 0 0 2 0.96 1.17 3.10 < 10 0 0 -2 2.59 4.29 2.92 < 10 0 0 -1 0.08 1.42 3.08 < 10 0 0 0 560.88 554.68 10.30 o -11 1 0 1 97.16 86.00 5.98 o -11 1 0 2 8.18 9.37 5.13 < -9 1 0 -2 1.43 1.43 5.82 < -9 1 0 -1 1.71 2.82 4.50 < -9 1 0 0 308.03 303.07 4.94 o -9 1 0 1 59.36 57.16 2.30 o -9 1 0 2 18.38 17.66 1.43 o -7 1 0 -2 17.54 17.74 1.88 o -7 1 0 -1 22.49 23.95 1.35 o -7 1 0 0 756.33 832.48 3.83 o -7 1 0 1 129.68 143.82 2.15 o -7 1 0 2 12.47 14.30 1.70 o -5 1 0 -2 0.90 1.35 1.26 < -5 1 0 -1 63.31 66.32 1.63 o -5 1 0 0 2309.44 2405.28 5.38 o -5 1 0 1 118.10 116.59 1.25 o -5 1 0 2 0.73 1.09 0.56 < -3 1 0 -2 2.11 1.26 0.51 < -3 1 0 -1 90.87 91.96 0.87 o -3 1 0 0 795.73 806.64 1.98 o -3 1 0 1 0.36 0.59 0.31 < -3 1 0 2 0.11 0.17 0.28 < -1 1 0 -2 0.01 -0.36 0.36 < -1 1 0 -1 25.80 24.80 0.40 o -1 1 0 0 202.12 193.79 0.47 o -1 1 0 1 3.16 2.74 0.17 o -1 1 0 2 2.18 1.26 0.25 o 1 1 0 -2 0.18 0.75 0.09 o 1 1 0 -1 2.55 2.12 0.23 o 1 1 0 0 848.14 932.25 1.25 o 1 1 0 1 3.22 4.12 0.40 o 1 1 0 2 1.29 0.87 0.54 < 3 1 0 -2 0.67 2.71 0.31 o 3 1 0 -1 29.94 27.61 0.53 o 3 1 0 0 2499.88 2576.01 3.92 o 3 1 0 1 47.65 49.98 1.01 o 3 1 0 2 2.16 2.88 0.98 < 5 1 0 -2 16.35 16.63 1.18 o 5 1 0 -1 298.72 309.79 2.50 o 5 1 0 0 195.84 243.12 2.79 o 5 1 0 1 3.75 5.38 1.45 o 5 1 0 2 2.80 2.91 1.40 < 7 1 0 -2 22.28 26.58 1.45 o 7 1 0 -1 134.85 146.62 1.93 o 7 1 0 0 2235.02 2335.67 7.24 o 7 1 0 1 13.12 15.95 1.71 o 7 1 0 2 5.18 6.69 2.10 o 9 1 0 -2 2.04 4.09 1.38 < 9 1 0 -1 84.28 87.69 2.13 o 9 1 0 0 1.33 5.29 2.10 < 9 1 0 1 1.62 -0.40 3.50 < 9 1 0 2 2.99 6.19 3.86 < 11 1 0 -2 20.95 22.70 3.70 o 11 1 0 -1 81.89 82.94 6.44 o -10 2 0 0 2.32 0.33 3.27 < -10 2 0 1 33.45 32.72 4.59 o -10 2 0 2 7.24 9.57 2.32 o -8 2 0 -2 1.30 3.25 2.63 < -8 2 0 -1 116.97 128.91 4.78 o -8 2 0 0 448.21 463.19 4.07 o -8 2 0 1 257.86 271.33 2.60 o -8 2 0 2 7.36 8.40 1.45 o -6 2 0 -2 0.75 0.92 1.51 < -6 2 0 -1 19.96 20.37 1.45 o -6 2 0 0 803.23 856.69 3.38 o -6 2 0 1 85.71 85.14 1.49 o -6 2 0 2 8.57 8.59 1.29 o -4 2 0 -2 15.02 14.70 0.81 o -4 2 0 -1 216.23 219.34 1.57 o -4 2 0 0 1849.86 1866.15 3.68 o -4 2 0 1 590.48 585.86 2.08 o -4 2 0 2 15.94 14.02 0.45 o -2 2 0 -2 0.20 1.34 0.73 < -2 2 0 -1 0.07 -0.48 0.33 < -2 2 0 0 7155.63 6849.61 5.04 o -2 2 0 1 124.82 111.03 0.56 o -2 2 0 2 1.27 0.75 0.25 < 0 2 0 -2 0.73 0.30 0.20 < 0 2 0 -1 54.54 46.50 0.28 o 0 2 0 0 37.01 39.33 0.45 o 0 2 0 1 77.70 70.81 0.51 o 0 2 0 2 0.00 -0.14 0.33 < 2 2 0 -2 1.88 1.54 0.34 o 2 2 0 -1 1.25 1.98 0.34 o 2 2 0 0 3774.97 3902.66 4.42 o 2 2 0 1 55.90 65.44 0.98 o 2 2 0 2 1.16 1.14 0.79 < 4 2 0 -2 5.88 5.29 0.61 o 4 2 0 -1 138.05 148.32 1.37 o 4 2 0 0 683.27 736.98 2.91 o 4 2 0 1 0.28 -0.58 1.10 < 4 2 0 2 0.61 0.12 1.43 < 6 2 0 -2 1.24 1.07 1.20 < 6 2 0 -1 4.04 4.90 1.79 < 6 2 0 0 176.16 200.78 2.68 o 6 2 0 1 152.40 156.89 2.63 o 6 2 0 2 2.65 1.66 1.79 < 8 2 0 -2 20.39 20.91 1.43 o 8 2 0 -1 104.25 112.58 2.07 o 8 2 0 0 39.60 48.74 2.04 o 8 2 0 1 8.26 8.37 1.91 o 8 2 0 2 1.13 0.96 2.10 < 10 2 0 -2 3.67 3.22 1.87 < 10 2 0 -1 28.31 28.19 2.46 o 10 2 0 0 50.25 50.58 3.36 o -11 3 0 2 5.15 3.87 2.69 < -9 3 0 -2 9.33 6.85 3.53 < -9 3 0 -1 24.04 22.70 4.85 o -9 3 0 0 291.19 285.60 5.10 o -9 3 0 1 38.81 39.00 2.32 o -9 3 0 2 9.95 9.34 1.59 o -7 3 0 -2 1.70 1.42 2.50 < -7 3 0 -1 149.72 153.16 3.46 o -7 3 0 0 1.14 2.36 1.49 < -7 3 0 1 3.60 2.83 1.37 < -7 3 0 2 0.03 -0.20 1.31 < -5 3 0 -2 0.49 -0.14 0.84 < -5 3 0 -1 100.48 103.77 1.43 o -5 3 0 0 3068.29 3097.86 6.33 o -5 3 0 1 5.23 3.49 0.93 o -5 3 0 2 0.67 0.61 1.03 < -3 3 0 -2 3.26 2.30 0.47 o -3 3 0 -1 68.54 65.72 1.09 o -3 3 0 0 3472.77 3566.37 5.79 o -3 3 0 1 0.06 0.76 0.42 < -3 3 0 2 0.36 0.39 0.47 < -1 3 0 -2 1.62 1.77 0.40 o -1 3 0 -1 65.66 62.13 0.56 o -1 3 0 0 4360.15 4143.35 3.64 o -1 3 0 1 63.95 54.92 0.55 o -1 3 0 2 0.54 0.12 0.33 < 1 3 0 -2 4.17 3.63 0.26 o 1 3 0 -1 77.07 75.49 0.56 o 1 3 0 0 4284.49 4275.48 4.63 o 1 3 0 1 24.33 23.11 0.56 o 1 3 0 2 2.11 1.07 0.65 < 3 3 0 -2 17.09 16.14 0.56 o 3 3 0 -1 138.37 161.67 1.29 o 3 3 0 0 4945.24 5642.87 9.26 o 3 3 0 1 50.36 55.91 1.56 o 3 3 0 2 0.38 0.76 1.28 < 5 3 0 -2 12.62 14.49 1.29 o 5 3 0 -1 151.18 153.60 2.46 o 5 3 0 0 4250.01 4409.80 8.58 o 5 3 0 1 152.52 157.69 2.62 o 5 3 0 2 10.64 10.67 1.73 o 7 3 0 -2 10.31 10.91 1.60 o 7 3 0 -1 50.69 52.93 2.02 o 7 3 0 0 156.74 164.41 2.83 o 7 3 0 1 108.68 103.02 2.66 o 7 3 0 2 0.18 0.65 2.10 < 9 3 0 -2 2.62 4.25 1.88 < 9 3 0 -1 65.39 68.70 2.47 o 9 3 0 0 603.73 616.95 4.90 o 9 3 0 1 107.82 106.07 3.49 o 9 3 0 2 0.00 0.12 6.18 < 11 3 0 -2 2.01 1.73 2.74 < 11 3 0 -1 20.93 20.41 5.96 o -10 4 0 0 247.94 250.05 4.36 o -10 4 0 1 26.23 24.94 2.75 o -10 4 0 2 5.53 6.72 2.33 < -8 4 0 -2 1.53 0.75 2.47 < -8 4 0 -1 0.12 0.12 2.02 < -8 4 0 0 104.26 95.38 3.18 o -8 4 0 1 226.02 222.62 2.63 o -8 4 0 2 28.59 30.44 1.59 o -6 4 0 -2 8.12 8.03 1.70 o -6 4 0 -1 0.01 -0.28 1.23 < -6 4 0 0 312.93 309.81 5.32 o -6 4 0 1 26.46 29.35 1.56 o -6 4 0 2 5.71 7.31 1.06 o -4 4 0 -2 0.50 0.98 1.20 < -4 4 0 -1 68.65 67.47 1.99 o -4 4 0 0 112.32 113.28 1.35 o -4 4 0 1 128.52 119.43 0.98 o -4 4 0 2 13.45 11.93 0.82 o -2 4 0 -2 0.00 0.34 0.78 < -2 4 0 -1 34.31 30.12 0.89 o -2 4 0 0 115.54 130.04 1.50 o -2 4 0 1 16.66 15.98 0.45 o -2 4 0 2 0.79 1.23 0.62 < 0 4 0 -2 4.05 3.52 0.33 o 0 4 0 -1 53.10 48.94 0.67 o 0 4 0 0 958.58 930.20 3.05 o 0 4 0 1 34.66 32.53 0.78 o 0 4 0 2 0.03 -0.22 0.58 < 2 4 0 -2 2.70 2.99 0.50 o 2 4 0 -1 5.82 6.13 0.58 o 2 4 0 0 71.14 66.75 1.04 o 2 4 0 1 39.02 39.64 1.43 o 2 4 0 2 0.46 0.28 1.17 < 4 4 0 -2 0.66 1.12 0.92 < 4 4 0 -1 52.96 59.91 1.46 o 4 4 0 0 135.90 157.18 2.18 o 4 4 0 1 41.57 44.60 1.29 o 4 4 0 2 5.40 5.66 1.09 o 6 4 0 -2 0.03 2.88 2.64 < 6 4 0 -1 5.71 5.38 2.01 < 6 4 0 0 109.73 111.88 2.46 o 6 4 0 1 22.45 23.62 1.98 o 6 4 0 2 3.36 2.07 2.10 < 8 4 0 -2 11.07 13.13 1.62 o 8 4 0 -1 261.48 264.35 3.07 o 8 4 0 0 96.79 95.45 2.41 o 8 4 0 1 1.28 2.83 2.49 < 8 4 0 2 8.45 8.46 2.63 o 10 4 0 -2 8.02 11.81 2.05 o 10 4 0 -1 13.65 13.52 2.15 o 10 4 0 0 5.97 5.90 2.52 < -9 5 0 -1 126.51 130.04 4.39 o -9 5 0 0 36.81 34.72 3.25 o -9 5 0 1 60.17 55.61 2.46 o -9 5 0 2 0.17 -1.56 1.93 < -7 5 0 -2 0.09 0.23 1.96 < -7 5 0 -1 70.90 72.09 2.32 o -7 5 0 0 1804.95 1673.87 7.43 o -7 5 0 1 21.26 20.99 1.73 o -7 5 0 2 1.07 1.51 1.51 < -5 5 0 -2 1.24 1.87 1.18 < -5 5 0 -1 273.01 263.17 2.32 o -5 5 0 0 170.72 192.07 2.23 o -5 5 0 1 458.68 462.90 3.06 o -5 5 0 2 5.18 3.44 0.84 o -3 5 0 -2 3.96 3.05 0.72 o -3 5 0 -1 35.39 30.52 1.09 o -3 5 0 0 2968.85 2653.02 3.79 o -3 5 0 1 5.33 6.15 0.92 o -3 5 0 2 0.53 0.22 0.50 < -1 5 0 -2 2.71 2.16 0.37 o -1 5 0 -1 58.09 51.36 0.83 o -1 5 0 0 3902.48 3824.55 6.68 o -1 5 0 2 0.01 0.30 0.51 < 1 5 0 -2 2.61 3.33 0.47 o 1 5 0 -1 131.56 136.07 1.34 o 1 5 0 0 3997.68 4200.30 7.27 o 1 5 0 1 12.36 13.23 0.78 o 1 5 0 2 3.68 2.71 1.15 < 3 5 0 -2 3.36 3.52 0.73 o 3 5 0 -1 86.51 95.92 1.99 o 3 5 0 0 3137.09 3455.53 8.52 o 3 5 0 1 66.25 69.70 1.93 o 3 5 0 2 6.54 7.05 1.37 o 5 5 0 -2 0.10 -0.33 1.12 < 5 5 0 -1 63.64 66.98 1.70 o 5 5 0 0 7.21 10.80 1.14 o 5 5 0 1 4.43 3.89 1.14 o 5 5 0 2 0.96 1.01 1.45 < 7 5 0 -2 0.36 -1.12 1.62 < 7 5 0 -1 6.01 2.91 2.38 < 7 5 0 0 1659.68 1679.58 13.89 o 7 5 0 1 84.04 82.70 3.52 o 7 5 0 2 1.41 -0.58 2.36 < 9 5 0 -2 0.12 1.29 2.16 < 9 5 0 -1 11.67 11.14 2.61 o 9 5 0 0 8.80 10.39 2.72 o 9 5 0 1 12.84 12.31 3.00 o 11 5 0 -2 8.93 9.01 2.58 o -10 6 0 1 174.26 165.68 3.66 o -10 6 0 2 16.40 16.69 2.57 o -8 6 0 -2 10.55 12.26 2.60 o -8 6 0 -1 73.38 68.93 3.46 o -8 6 0 0 34.12 34.96 2.23 o -8 6 0 1 0.38 -0.45 1.90 < -8 6 0 2 0.95 0.93 1.88 < -6 6 0 -2 4.80 3.78 1.66 < -6 6 0 -1 32.52 33.14 2.44 o -6 6 0 0 12.30 14.11 1.73 o -6 6 0 1 182.10 173.88 3.32 o -6 6 0 2 11.22 10.32 1.37 o -4 6 0 -2 7.49 7.25 1.49 o -4 6 0 -1 52.58 53.01 2.09 o -4 6 0 0 814.66 798.50 4.38 o -4 6 0 1 47.12 45.97 0.84 o -4 6 0 2 0.17 -0.37 0.68 < -2 6 0 -2 0.01 0.28 0.67 < -2 6 0 -1 109.12 100.10 1.68 o -2 6 0 0 141.54 131.88 1.32 o -2 6 0 1 15.33 12.70 1.14 o -2 6 0 2 2.91 3.84 1.74 < 0 6 0 -2 8.72 8.43 0.86 o 0 6 0 0 8884.75 8145.27 9.68 o 0 6 0 1 120.88 119.61 1.28 o 0 6 0 2 0.49 -0.16 1.26 < 2 6 0 -2 2.87 3.17 0.70 o 2 6 0 -1 2.48 3.45 1.18 < 2 6 0 0 4.73 5.59 1.01 o 2 6 0 1 23.53 25.64 1.09 o 2 6 0 2 1.14 0.02 1.00 < 4 6 0 -2 3.43 3.87 1.31 < 4 6 0 -1 45.11 49.82 1.49 o 4 6 0 0 2279.65 2488.84 8.14 o 4 6 0 1 155.11 163.35 2.23 o 4 6 0 2 0.38 -0.56 1.31 < 6 6 0 -2 23.78 23.99 1.45 o 6 6 0 -1 288.93 294.98 2.34 o 6 6 0 0 388.76 399.17 2.70 o 6 6 0 1 0.59 0.20 1.70 < 6 6 0 2 3.12 1.62 2.30 < 8 6 0 -2 6.43 7.47 2.46 o 8 6 0 -1 2.66 2.04 2.64 < 8 6 0 0 341.09 328.75 5.39 o 8 6 0 1 61.20 57.16 3.67 o 8 6 0 2 0.42 -3.61 3.58 < 10 6 0 -2 9.92 10.16 2.88 o 10 6 0 -1 118.97 121.94 4.84 o -9 7 0 0 427.31 397.14 4.72 o -9 7 0 1 25.55 24.27 2.47 o -9 7 0 2 17.40 17.69 1.99 o -7 7 0 -2 5.85 4.85 2.26 < -7 7 0 -1 34.39 33.64 2.85 o -7 7 0 0 73.19 68.09 2.09 o -7 7 0 1 236.61 238.15 2.87 o -7 7 0 2 13.96 14.61 1.82 o -5 7 0 -2 0.09 -0.17 1.56 < -5 7 0 -1 6.62 8.00 1.63 o -5 7 0 0 2450.67 2426.94 8.38 o -5 7 0 1 9.21 10.70 1.49 o -5 7 0 2 5.30 5.17 1.42 o -3 7 0 -2 1.34 0.02 1.09 < -3 7 0 -1 22.35 21.07 1.68 o -3 7 0 0 86.68 85.11 1.71 o -3 7 0 1 275.35 257.34 2.21 o -3 7 0 2 9.29 8.71 1.17 o -1 7 0 -2 0.07 -0.25 0.78 < -1 7 0 -1 0.01 -0.09 0.65 < -1 7 0 0 880.64 892.07 4.25 o -1 7 0 1 25.91 25.36 1.49 o -1 7 0 2 0.46 -1.12 0.96 < 1 7 0 -2 10.53 11.56 0.89 o 1 7 0 -1 90.41 92.75 1.28 o 1 7 0 0 442.63 450.79 3.97 o 1 7 0 1 3.48 3.50 1.42 < 1 7 0 2 0.12 -0.36 1.68 < 3 7 0 -2 0.15 -0.14 0.86 < 3 7 0 -1 78.93 86.33 1.40 o 3 7 0 0 45.12 43.59 1.60 o 3 7 0 1 9.97 9.57 1.32 o 3 7 0 2 2.51 2.08 1.35 < 5 7 0 -2 3.11 4.29 1.23 o 5 7 0 -1 1.48 0.73 1.29 < 5 7 0 0 1124.15 1196.68 4.43 o 5 7 0 1 74.73 74.02 1.76 o 5 7 0 2 0.59 0.82 1.65 < 7 7 0 -2 3.48 3.00 1.42 < 7 7 0 -1 94.93 92.04 2.15 o 7 7 0 0 450.42 453.18 5.79 o 7 7 0 1 0.19 1.70 3.00 < 7 7 0 2 3.07 3.20 3.31 < 9 7 0 -2 0.34 0.72 2.91 < 9 7 0 -1 19.91 20.29 3.33 o -10 8 0 2 2.34 2.26 4.14 < -8 8 0 -1 88.72 85.05 3.02 o -8 8 0 0 200.00 192.82 3.05 o -8 8 0 1 0.64 2.07 2.24 < -8 8 0 2 3.57 4.39 2.08 < -6 8 0 -2 1.93 1.96 1.82 < -6 8 0 -1 40.77 40.60 2.16 o -6 8 0 0 384.96 387.10 4.01 o -6 8 0 1 16.26 15.57 1.90 o -6 8 0 2 0.03 0.12 1.65 < -4 8 0 -2 4.69 4.81 1.71 < -4 8 0 -1 284.53 271.49 3.88 o -4 8 0 0 545.50 522.88 3.90 o -4 8 0 1 122.26 115.95 1.90 o -4 8 0 2 0.03 -1.54 1.28 < -2 8 0 -2 2.28 2.41 1.00 < -2 8 0 -1 0.95 1.24 1.04 < -2 8 0 0 4120.48 4170.80 9.90 o -2 8 0 1 0.92 1.71 1.65 < -2 8 0 2 3.94 3.20 1.24 < 0 8 0 -2 3.67 4.12 0.98 o 0 8 0 -1 134.44 135.75 1.64 o 0 8 0 0 81.77 91.30 2.23 o 0 8 0 1 119.87 124.78 1.98 o 0 8 0 2 0.98 0.34 1.17 < 2 8 0 -2 1.72 1.99 0.90 < 2 8 0 -1 52.50 54.02 1.85 o 2 8 0 0 3868.64 4248.58 8.31 o 2 8 0 1 74.69 77.89 1.56 o 2 8 0 2 4.36 4.90 1.40 o 4 8 0 -2 0.59 0.78 1.29 < 4 8 0 -1 0.49 1.14 1.74 < 4 8 0 0 815.46 950.91 4.86 o 4 8 0 1 54.43 56.52 2.07 o 4 8 0 2 5.25 4.89 1.68 < 6 8 0 -2 4.57 4.15 1.51 < 6 8 0 -1 4.54 5.40 1.63 o 6 8 0 0 772.59 780.47 4.37 o 6 8 0 1 180.60 169.64 2.96 o 6 8 0 2 1.33 0.17 2.15 < 8 8 0 -2 0.03 -3.36 4.14 < 8 8 0 -1 8.81 7.73 4.12 < 8 8 0 0 345.73 319.23 8.10 o -9 9 0 1 126.65 126.88 5.46 o -9 9 0 2 11.68 10.13 2.52 o -7 9 0 -2 1.63 2.74 2.47 < -7 9 0 -1 29.23 31.45 2.58 o -7 9 0 0 287.98 290.92 3.99 o -7 9 0 1 24.59 22.47 2.21 o -7 9 0 2 2.18 2.82 1.73 < -5 9 0 -2 6.84 6.10 1.63 o -5 9 0 -1 0.87 2.96 2.30 < -5 9 0 0 160.46 148.16 2.40 o -5 9 0 1 117.23 112.59 2.15 o -5 9 0 2 3.35 3.91 1.71 < -3 9 0 -2 4.72 4.34 1.20 o -3 9 0 -1 45.57 46.08 1.60 o -3 9 0 0 25.81 29.67 1.73 o -3 9 0 1 0.31 0.54 1.48 < -3 9 0 2 0.24 0.65 2.01 < -1 9 0 -2 0.56 0.36 1.29 < -1 9 0 -1 57.62 62.89 1.82 o -1 9 0 0 54.12 53.76 1.96 o -1 9 0 1 85.52 88.73 1.74 o -1 9 0 2 0.08 0.16 1.46 < 1 9 0 -2 3.22 3.87 0.98 o 1 9 0 -1 17.69 15.89 1.43 o 1 9 0 0 60.71 62.21 1.67 o 1 9 0 1 6.71 6.33 1.29 o 1 9 0 2 0.01 -1.04 1.59 < 3 9 0 -2 0.01 0.45 1.42 < 3 9 0 -1 1.22 1.88 1.51 < 3 9 0 0 97.70 106.82 1.99 o 3 9 0 1 1.73 2.75 1.56 < 3 9 0 2 0.93 1.54 1.65 < 5 9 0 -2 5.85 6.58 2.05 o 5 9 0 -1 60.74 59.86 2.18 o 5 9 0 0 712.56 727.74 4.36 o 5 9 0 1 10.32 9.20 1.88 o 5 9 0 2 6.39 4.54 2.24 < 7 9 0 -2 2.56 1.82 1.88 < 7 9 0 -1 9.36 6.15 2.41 < 7 9 0 0 9.08 6.67 3.07 < 9 9 0 -2 8.43 7.50 4.57 < -8 10 0 1 104.72 101.12 3.74 o -8 10 0 2 3.98 3.10 2.05 < -6 10 0 -2 1.83 2.35 1.79 < -6 10 0 -1 110.62 107.85 2.32 o -6 10 0 0 423.32 417.77 3.46 o -6 10 0 1 24.64 25.10 1.76 o -6 10 0 2 4.14 4.75 1.82 < -4 10 0 -2 1.26 1.79 1.60 < -4 10 0 -1 0.39 0.34 1.54 < -4 10 0 0 317.64 308.38 3.12 o -4 10 0 1 59.13 67.29 2.27 o -4 10 0 2 2.74 5.82 2.27 < -2 10 0 -2 1.60 1.77 1.62 < -2 10 0 -1 49.18 55.42 2.05 o -2 10 0 0 444.14 440.09 3.77 o -2 10 0 1 87.57 90.86 2.32 o -2 10 0 2 2.35 3.28 1.48 < 0 10 0 -2 1.66 1.17 1.70 < 0 10 0 -1 5.00 4.33 1.71 < 0 10 0 0 1189.09 1257.35 4.71 o 0 10 0 1 0.04 -0.67 1.49 < 0 10 0 2 0.00 1.09 1.90 < 2 10 0 -2 1.88 0.68 1.56 < 2 10 0 -1 19.02 22.28 1.37 o 2 10 0 0 378.58 403.34 3.60 o 2 10 0 1 14.71 18.06 2.30 o 2 10 0 2 0.35 1.31 1.82 < 4 10 0 -2 0.61 1.10 1.84 < 4 10 0 -1 0.00 1.31 2.58 < 4 10 0 0 209.41 224.56 3.71 o 4 10 0 1 62.72 56.26 2.86 o 4 10 0 2 0.08 -0.76 2.24 < 6 10 0 -2 2.58 1.48 1.98 < 6 10 0 -1 1.38 0.92 2.08 < 6 10 0 0 97.64 96.74 3.27 o 6 10 0 1 5.66 4.05 3.45 < -7 11 0 0 231.95 235.84 4.81 o -7 11 0 1 30.83 32.83 2.35 o -7 11 0 2 5.26 3.84 2.07 < -5 11 0 -2 1.37 0.16 1.62 < -5 11 0 -1 120.56 118.30 2.57 o -5 11 0 0 36.61 39.24 2.09 o -5 11 0 1 30.66 30.78 2.46 o -5 11 0 2 1.85 3.89 2.77 < -3 11 0 -2 0.01 -0.17 1.99 < -3 11 0 -1 21.33 19.92 2.08 o -3 11 0 0 319.58 322.73 4.75 o -3 11 0 1 45.23 53.87 3.00 o -3 11 0 2 0.13 -0.75 2.02 < -1 11 0 -2 1.46 2.43 1.90 < -1 11 0 -1 7.43 6.38 1.98 o -1 11 0 0 541.61 549.89 4.77 o -1 11 0 1 82.44 80.69 3.02 o -1 11 0 2 0.99 1.62 1.79 < 1 11 0 -2 0.67 0.75 1.90 < 1 11 0 -1 51.91 51.32 2.07 o 1 11 0 0 879.43 917.90 5.35 o 1 11 0 1 0.29 0.42 2.27 < 1 11 0 2 0.85 0.31 2.36 < 3 11 0 -2 6.45 9.55 2.29 o 3 11 0 -1 46.12 50.39 3.13 o 3 11 0 0 731.31 764.78 6.14 o 3 11 0 1 17.57 18.86 2.61 o 3 11 0 2 6.55 7.17 2.60 < 5 11 0 -2 0.35 -0.42 1.99 < 5 11 0 -1 2.02 2.82 2.19 < 5 11 0 0 192.88 198.31 3.43 o 5 11 0 1 0.75 0.84 2.83 < 7 11 0 -2 2.64 2.41 2.27 < 7 11 0 -1 71.37 64.85 5.35 o -6 12 0 0 91.59 100.69 3.39 o -6 12 0 1 164.29 164.27 4.52 o -6 12 0 2 4.65 3.75 3.14 < -4 12 0 -2 4.39 4.95 2.05 < -4 12 0 -1 2.03 1.74 2.07 < -4 12 0 0 34.82 40.08 3.30 o -4 12 0 1 46.06 43.28 3.36 o -4 12 0 2 2.26 1.46 2.83 < -2 12 0 -2 0.42 1.56 2.27 < -2 12 0 -1 26.36 26.30 2.47 o -2 12 0 0 339.08 357.66 4.39 o -2 12 0 1 0.40 -0.47 2.27 < -2 12 0 2 0.13 -0.30 2.35 < 0 12 0 -2 0.77 1.10 1.66 < 0 12 0 -1 6.33 6.57 1.88 o 0 12 0 0 105.90 109.63 2.62 o 0 12 0 1 61.85 64.54 2.47 o 0 12 0 2 0.01 -0.73 3.25 < 2 12 0 -2 0.06 1.24 1.98 < 2 12 0 -1 22.96 25.13 2.66 o 2 12 0 0 133.63 146.08 3.57 o 2 12 0 1 41.18 46.99 2.99 o 2 12 0 2 0.60 2.32 2.85 < 4 12 0 -2 2.06 2.21 2.47 < 4 12 0 -1 0.83 0.40 2.66 < 4 12 0 0 45.52 49.56 3.14 o 4 12 0 1 18.57 20.68 4.78 o 6 12 0 -2 7.55 6.61 2.38 < -3 13 0 -2 0.01 -1.59 2.18 < -3 13 0 -1 72.67 79.02 3.21 o -3 13 0 0 215.91 231.20 4.10 o -3 13 0 1 187.47 200.22 3.99 o -3 13 0 2 0.01 -0.20 2.72 < -1 13 0 -2 0.15 -0.59 1.84 < -1 13 0 -1 26.28 27.56 2.13 o -1 13 0 0 537.79 565.78 4.79 o -1 13 0 1 8.26 8.46 2.36 o -1 13 0 2 0.19 -0.62 2.30 < 1 13 0 -2 5.60 3.61 2.35 < 1 13 0 -1 19.97 18.47 2.30 o 1 13 0 0 469.86 495.60 5.52 o 1 13 0 1 13.11 14.03 3.63 o 3 13 0 -2 1.02 1.48 2.69 < 3 13 0 -1 43.92 48.66 3.16 o 3 13 0 0 173.35 175.96 6.99 o 5 13 0 -2 8.13 8.35 2.83 < -2 14 0 -2 5.92 6.72 3.56 < -2 14 0 -1 0.21 -0.31 3.44 < -2 14 0 0 379.25 373.98 8.81 o 0 14 0 -2 0.94 1.34 2.32 < 0 14 0 -1 73.54 71.31 3.25 o 0 14 0 0 18.60 22.73 4.65 o 2 14 0 -2 0.84 0.34 2.89 < -2 -14 1 2 0.66 1.01 3.44 < 0 -14 1 0 342.86 354.60 8.59 o 0 -14 1 1 0.83 0.44 3.39 < 0 -14 1 2 2.36 0.30 4.71 < -5 -13 1 2 0.26 1.06 3.47 < -3 -13 1 0 116.15 120.01 3.72 o -3 -13 1 1 20.53 22.37 2.51 o -3 -13 1 2 6.12 6.66 2.04 o -1 -13 1 -2 0.05 1.37 3.53 < -1 -13 1 -1 57.71 59.95 3.31 o -1 -13 1 0 911.64 955.18 7.22 o -1 -13 1 1 0.83 -0.68 2.61 < -1 -13 1 2 0.15 -1.57 2.16 < 1 -13 1 -2 0.94 -0.96 2.33 < 1 -13 1 -1 141.34 143.42 3.14 o 1 -13 1 0 146.54 158.14 3.15 o 1 -13 1 1 28.22 29.69 2.41 o 1 -13 1 2 0.06 0.45 2.47 < 3 -13 1 -2 0.23 0.48 2.12 < 3 -13 1 -1 3.08 4.22 2.12 < 3 -13 1 0 986.98 1008.72 6.15 o 3 -13 1 1 0.39 -0.51 3.36 < 3 -13 1 2 0.22 -1.14 4.79 < -6 -12 1 1 50.25 52.91 5.20 o -6 -12 1 2 0.32 0.00 1.94 < -4 -12 1 -1 59.05 52.07 3.11 o -4 -12 1 0 8.66 11.50 2.40 o -4 -12 1 1 13.86 14.80 2.60 o -4 -12 1 2 0.41 0.09 2.15 < -2 -12 1 -2 0.42 0.36 2.61 < -2 -12 1 -1 29.07 35.62 3.63 o -2 -12 1 0 225.79 242.38 4.13 o -2 -12 1 1 58.01 63.25 2.47 o -2 -12 1 2 1.14 1.63 1.71 < 0 -12 1 -2 0.13 1.94 2.58 < 0 -12 1 -1 8.49 6.49 2.07 o 0 -12 1 0 134.68 143.90 2.83 o 0 -12 1 1 33.65 31.73 2.18 o 0 -12 1 2 3.29 4.09 1.94 < 2 -12 1 -2 2.24 2.69 1.88 < 2 -12 1 -1 11.38 11.34 1.87 o 2 -12 1 0 5.90 6.60 1.82 o 2 -12 1 1 5.79 6.33 2.02 o 2 -12 1 2 1.81 3.66 2.01 < 4 -12 1 -2 1.74 0.95 2.46 < 4 -12 1 -1 111.74 121.17 3.35 o 4 -12 1 0 25.73 26.06 2.68 o 4 -12 1 1 20.50 18.47 2.23 o 4 -12 1 2 0.02 -0.72 2.92 < 6 -12 1 -2 6.49 6.07 2.83 < 6 -12 1 -1 0.37 0.30 3.42 < -7 -11 1 1 8.14 8.70 4.51 < -7 -11 1 2 0.19 0.17 2.07 < -5 -11 1 -1 67.41 60.03 2.74 o -5 -11 1 0 717.85 701.13 5.28 o -5 -11 1 1 92.09 85.80 2.69 o -5 -11 1 2 15.72 14.63 2.40 o -3 -11 1 -2 0.09 -1.28 2.27 < -3 -11 1 -1 2.48 1.62 2.10 < -3 -11 1 0 559.64 592.66 5.51 o -3 -11 1 1 25.81 27.73 2.18 o -3 -11 1 2 0.23 0.22 1.82 < -1 -11 1 -2 1.60 2.15 2.40 < -1 -11 1 -1 38.03 42.57 3.08 o -1 -11 1 0 789.92 820.98 5.12 o -1 -11 1 1 8.92 7.25 1.76 o -1 -11 1 2 4.03 3.16 1.56 < 1 -11 1 -2 0.46 0.25 1.84 < 1 -11 1 -1 25.71 27.59 1.93 o 1 -11 1 0 479.15 478.96 3.54 o 1 -11 1 1 7.73 9.68 1.62 o 1 -11 1 2 0.04 0.03 1.49 < 3 -11 1 -2 0.15 -1.10 2.12 < 3 -11 1 -1 35.70 36.33 2.40 o 3 -11 1 0 106.90 114.15 2.49 o 3 -11 1 1 98.37 103.29 2.15 o 3 -11 1 2 0.01 0.81 1.82 < 5 -11 1 -2 0.18 -0.45 2.13 < 5 -11 1 -1 3.49 1.26 1.96 < 5 -11 1 0 595.72 589.14 4.06 o 5 -11 1 1 16.65 18.41 2.07 o 5 -11 1 2 3.73 4.53 2.10 < 7 -11 1 -2 0.14 -0.86 1.91 < 7 -11 1 -1 0.38 3.73 4.99 < -8 -10 1 2 0.11 -0.45 2.50 < -6 -10 1 -1 103.25 96.42 3.39 o -6 -10 1 0 85.93 84.00 2.69 o -6 -10 1 1 6.55 6.75 2.43 < -6 -10 1 2 0.83 0.98 1.98 < -4 -10 1 -2 0.87 0.89 2.21 < -4 -10 1 -1 6.28 6.21 2.40 < -4 -10 1 0 88.37 99.82 2.63 o -4 -10 1 1 20.45 19.04 1.96 o -4 -10 1 2 0.71 0.56 1.74 < -2 -10 1 -2 1.40 0.93 2.19 < -2 -10 1 -1 47.17 48.37 3.03 o -2 -10 1 0 1318.59 1461.35 7.68 o -2 -10 1 1 20.58 23.50 2.23 o -2 -10 1 2 2.54 2.64 1.40 < 0 -10 1 -2 0.01 -0.81 1.57 < 0 -10 1 -1 53.61 53.75 1.98 o 0 -10 1 0 71.30 74.74 2.05 o 0 -10 1 1 26.38 25.71 1.48 o 0 -10 1 2 1.86 2.02 1.29 < 2 -10 1 -2 0.80 1.73 1.74 < 2 -10 1 -1 7.13 7.02 1.91 o 2 -10 1 0 988.29 1015.81 5.16 o 2 -10 1 1 21.15 21.25 1.31 o 2 -10 1 2 2.53 3.78 1.24 o 4 -10 1 -2 0.44 -0.06 1.87 < 4 -10 1 -1 31.82 29.69 2.68 o 4 -10 1 0 355.38 362.94 3.06 o 4 -10 1 1 54.53 49.74 1.65 o 4 -10 1 2 5.22 5.66 1.45 o 6 -10 1 -2 2.10 2.16 1.77 < 6 -10 1 -1 151.37 151.74 2.24 o 6 -10 1 0 426.79 438.22 4.58 o 6 -10 1 1 24.46 22.58 2.15 o 6 -10 1 2 0.06 -0.34 2.13 < 8 -10 1 -2 0.39 -0.06 1.87 < 8 -10 1 -1 8.72 9.57 4.45 < -9 -9 1 2 5.72 6.44 3.63 < -7 -9 1 -1 15.41 14.61 5.10 < -7 -9 1 0 897.06 877.68 11.85 o -7 -9 1 1 73.82 72.60 3.28 o -7 -9 1 2 2.47 3.31 1.96 < -5 -9 1 -2 2.85 1.45 1.98 < -5 -9 1 -1 0.20 0.56 1.94 < -5 -9 1 0 55.65 57.50 2.21 o -5 -9 1 1 14.85 15.76 1.94 o -5 -9 1 2 1.04 0.37 1.74 < -3 -9 1 -2 4.90 6.92 2.18 o -3 -9 1 -1 7.50 8.34 2.13 o -3 -9 1 0 468.45 536.22 4.79 o -3 -9 1 1 77.60 84.05 2.15 o -3 -9 1 2 0.60 0.39 1.52 < -1 -9 1 -2 2.70 2.61 1.80 < -1 -9 1 -1 28.79 30.73 1.73 o -1 -9 1 0 194.41 201.03 2.17 o -1 -9 1 1 8.77 9.46 1.45 o -1 -9 1 2 2.70 2.36 1.18 < 1 -9 1 -2 2.72 3.66 1.42 < 1 -9 1 -1 46.25 44.88 1.90 o 1 -9 1 0 100.32 113.13 1.88 o 1 -9 1 1 52.30 51.93 1.48 o 1 -9 1 2 0.28 -0.53 1.04 < 3 -9 1 -2 3.16 1.87 1.56 < 3 -9 1 -1 79.46 82.07 2.13 o 3 -9 1 0 340.74 337.84 2.71 o 3 -9 1 1 3.22 4.20 1.20 o 3 -9 1 2 1.31 0.86 1.09 < 5 -9 1 -2 1.89 3.75 1.37 < 5 -9 1 -1 6.65 5.96 1.38 o 5 -9 1 0 160.40 157.69 2.23 o 5 -9 1 1 116.48 118.56 1.96 o 5 -9 1 2 0.39 0.40 1.57 < 7 -9 1 -2 11.16 12.14 1.68 o 7 -9 1 -1 143.72 146.24 2.44 o 7 -9 1 0 12.38 12.31 1.82 o 7 -9 1 1 1.15 0.34 2.07 < 7 -9 1 2 6.33 5.93 4.31 < 9 -9 1 -2 13.42 10.80 3.00 o -8 -8 1 0 374.60 346.57 5.99 o -8 -8 1 2 2.81 1.79 2.05 < -6 -8 1 -2 0.04 1.09 2.91 < -6 -8 1 -1 7.30 7.23 2.13 o -6 -8 1 0 239.50 233.83 3.49 o -6 -8 1 1 16.54 16.59 1.77 o -6 -8 1 2 5.24 5.68 1.71 o -4 -8 1 -2 0.24 0.72 1.76 < -4 -8 1 -1 109.07 112.94 2.41 o -4 -8 1 0 2217.14 2387.55 7.99 o -4 -8 1 1 40.07 40.68 1.77 o -4 -8 1 2 6.01 6.58 1.48 o -2 -8 1 -2 0.07 -1.04 1.51 < -2 -8 1 -1 2.13 1.54 1.31 < -2 -8 1 0 108.04 121.10 1.99 o -2 -8 1 1 6.43 8.57 1.09 o -2 -8 1 2 1.71 1.76 1.04 < 0 -8 1 -2 1.27 0.17 1.42 < 0 -8 1 -1 14.30 14.70 1.03 o 0 -8 1 0 3568.81 3796.26 5.90 o 0 -8 1 1 14.44 15.43 0.76 o 0 -8 1 2 7.15 7.31 0.86 o 2 -8 1 -2 1.15 0.73 1.62 < 2 -8 1 -1 30.34 30.19 1.49 o 2 -8 1 0 1461.37 1391.58 5.17 o 2 -8 1 1 95.33 94.82 1.42 o 2 -8 1 2 0.47 0.78 0.89 < 4 -8 1 -2 3.78 3.30 1.09 o 4 -8 1 -1 40.40 36.15 1.35 o 4 -8 1 0 396.34 383.73 2.78 o 4 -8 1 1 18.96 20.06 1.26 o 4 -8 1 2 0.68 0.11 1.18 < 6 -8 1 -2 0.01 -0.54 1.40 < 6 -8 1 -1 6.80 6.04 1.87 o 6 -8 1 0 650.35 667.41 5.00 o 6 -8 1 1 55.36 53.64 1.91 o 6 -8 1 2 1.01 0.54 1.70 < 8 -8 1 -2 0.87 -0.64 2.04 < 8 -8 1 -1 42.79 42.11 2.65 o 8 -8 1 0 16.03 16.63 2.24 o 8 -8 1 1 94.41 88.96 5.29 o -9 -7 1 0 183.62 177.18 4.16 o -9 -7 1 1 105.39 101.10 3.60 o -9 -7 1 2 8.89 7.48 2.71 < -7 -7 1 -2 0.43 -3.33 4.39 < -7 -7 1 -1 0.27 -1.99 4.20 < -7 -7 1 0 226.82 230.71 4.22 o -7 -7 1 1 26.28 24.15 4.08 o -7 -7 1 2 6.73 5.63 1.84 o -5 -7 1 -2 4.10 3.98 1.56 < -5 -7 1 -1 26.97 27.25 1.63 o -5 -7 1 0 0.34 0.86 1.38 < -5 -7 1 1 125.47 129.46 2.54 o -5 -7 1 2 1.85 0.95 1.23 < -3 -7 1 -2 0.87 0.53 1.68 < -3 -7 1 -1 15.13 18.62 1.57 o -3 -7 1 0 56.89 60.90 1.54 o -3 -7 1 1 0.33 0.25 1.07 < -3 -7 1 2 0.00 0.61 1.20 < -1 -7 1 -2 0.93 -0.14 1.40 < -1 -7 1 -1 92.75 96.99 1.35 o -1 -7 1 0 1441.18 1593.67 4.00 o -1 -7 1 1 2.53 3.35 0.68 o -1 -7 1 2 0.09 -0.90 0.96 < 1 -7 1 -2 0.20 -0.25 0.95 < 1 -7 1 -1 270.12 265.55 2.40 o 1 -7 1 0 22.42 19.73 1.18 o 1 -7 1 1 31.92 30.11 1.06 o 1 -7 1 2 1.32 1.23 0.65 < 3 -7 1 -2 0.29 0.93 1.00 < 3 -7 1 -1 1.42 1.18 0.95 < 3 -7 1 0 3051.19 2930.29 6.38 o 3 -7 1 1 22.08 22.78 1.04 o 3 -7 1 2 0.36 -0.30 0.90 < 5 -7 1 -2 4.08 3.89 1.71 < 5 -7 1 -1 320.70 326.42 3.41 o 5 -7 1 0 63.75 61.20 1.82 o 5 -7 1 1 20.25 20.29 1.45 o 5 -7 1 2 6.65 5.45 1.43 o 7 -7 1 -2 6.93 6.86 1.62 o 7 -7 1 -1 59.80 58.67 2.01 o 7 -7 1 0 601.87 597.54 4.40 o 7 -7 1 1 4.63 4.42 1.93 < 7 -7 1 2 1.49 2.22 1.77 < 9 -7 1 -2 3.08 2.64 2.01 < 9 -7 1 -1 85.15 80.86 2.68 o -10 -6 1 1 3.08 2.55 2.54 < -10 -6 1 2 3.12 4.14 2.40 < -8 -6 1 -2 9.98 10.36 3.50 < -8 -6 1 -1 1.07 2.16 3.19 < -8 -6 1 0 121.25 117.89 3.91 o -8 -6 1 1 104.34 107.28 3.08 o -8 -6 1 2 2.23 2.07 2.66 < -6 -6 1 -2 0.91 3.50 2.63 < -6 -6 1 -1 124.73 122.88 2.65 o -6 -6 1 0 1571.85 1593.77 6.70 o -6 -6 1 1 112.19 116.62 2.49 o -6 -6 1 2 4.86 6.10 1.28 o -4 -6 1 -2 17.17 17.71 1.28 o -4 -6 1 -1 19.42 21.85 1.35 o -4 -6 1 0 102.72 121.17 1.71 o -4 -6 1 1 4.57 4.76 1.06 o -4 -6 1 2 0.20 -0.76 0.81 < -2 -6 1 -2 9.50 11.48 1.26 o -2 -6 1 -1 18.25 20.52 1.14 o -2 -6 1 0 6470.94 6924.49 9.13 o -2 -6 1 1 144.13 157.82 1.81 o -2 -6 1 2 1.68 1.76 0.61 < 0 -6 1 -2 0.91 0.70 0.93 < 0 -6 1 -1 67.63 72.62 1.18 o 0 -6 1 0 230.97 239.09 1.31 o 0 -6 1 1 73.95 75.40 1.01 o 0 -6 1 2 4.32 4.85 0.86 o 2 -6 1 -2 1.13 1.04 0.98 < 2 -6 1 -1 18.64 16.71 0.98 o 2 -6 1 0 712.63 686.73 2.88 o 2 -6 1 1 27.90 26.02 0.76 o 2 -6 1 2 0.95 0.03 0.87 < 4 -6 1 -2 6.18 5.43 0.84 o 4 -6 1 -1 37.40 36.23 1.35 o 4 -6 1 0 762.48 757.97 3.88 o 4 -6 1 1 122.24 119.75 1.70 o 4 -6 1 2 0.13 -1.01 1.54 < 6 -6 1 -2 1.85 2.10 1.57 < 6 -6 1 -1 29.22 29.46 1.87 o 6 -6 1 0 11.52 12.37 1.73 o 6 -6 1 1 84.77 77.98 2.90 o 6 -6 1 2 1.16 0.59 1.99 < 8 -6 1 -2 6.23 5.94 2.29 < 8 -6 1 -1 54.19 48.49 2.51 o 8 -6 1 0 282.24 260.39 3.82 o 8 -6 1 1 33.28 35.70 2.75 o 8 -6 1 2 2.15 3.83 2.78 < 10 -6 1 -2 13.55 15.54 2.74 o -11 -5 1 2 5.70 6.52 2.41 < -9 -5 1 -1 151.14 143.66 3.91 o -9 -5 1 0 629.78 631.10 5.95 o -9 -5 1 1 26.12 23.26 2.32 o -9 -5 1 2 0.58 1.00 1.93 < -7 -5 1 -2 4.57 4.22 2.82 < -7 -5 1 -1 36.69 37.81 2.46 o -7 -5 1 0 14.98 13.26 2.10 o -7 -5 1 1 92.12 95.36 2.52 o -7 -5 1 2 1.96 2.80 1.84 < -5 -5 1 -2 1.13 0.64 1.18 < -5 -5 1 -1 278.38 279.46 2.42 o -5 -5 1 0 1312.86 1339.26 5.96 o -5 -5 1 1 130.88 132.06 1.73 o -5 -5 1 2 15.40 14.39 1.04 o -3 -5 1 -2 1.07 1.15 1.48 < -3 -5 1 -1 124.25 142.47 1.84 o -3 -5 1 0 2505.32 2793.75 7.22 o -3 -5 1 1 18.09 20.88 1.03 o -3 -5 1 2 3.96 3.75 0.59 o -1 -5 1 -2 0.49 -1.12 1.28 < -1 -5 1 -1 0.01 0.95 1.10 < -1 -5 1 0 2548.39 2892.43 5.55 o -1 -5 1 1 49.58 49.73 1.29 o -1 -5 1 2 7.66 7.34 0.39 o 1 -5 1 -2 0.24 -0.17 1.17 < 1 -5 1 0 4217.90 3971.01 9.46 o 1 -5 1 1 3.22 2.57 0.39 o 1 -5 1 2 0.86 1.54 0.76 < 3 -5 1 -2 2.24 1.66 1.26 < 3 -5 1 -1 56.87 53.02 0.78 o 3 -5 1 0 421.04 467.30 2.28 o 3 -5 1 1 27.86 27.56 0.96 o 3 -5 1 2 0.03 -1.06 0.87 < 5 -5 1 -2 7.54 8.00 1.10 o 5 -5 1 -1 48.52 47.55 1.62 o 5 -5 1 0 4143.10 3952.61 10.24 o 5 -5 1 1 34.94 31.60 1.48 o 5 -5 1 2 0.07 -0.22 1.40 < 7 -5 1 -2 1.23 2.44 2.01 < 7 -5 1 -1 13.53 13.97 1.82 o 7 -5 1 0 125.38 126.17 4.53 o 7 -5 1 1 51.79 50.73 2.44 o 7 -5 1 2 1.09 0.84 1.93 < 9 -5 1 -2 5.55 3.67 2.69 < 9 -5 1 -1 56.08 53.63 2.75 o 9 -5 1 0 304.22 291.15 4.36 o -10 -4 1 0 93.90 89.08 2.71 o -10 -4 1 1 194.43 183.64 3.38 o -10 -4 1 2 24.06 24.41 2.41 o -8 -4 1 -2 1.97 1.59 2.60 < -8 -4 1 -1 28.23 29.94 2.29 o -8 -4 1 0 173.48 177.59 3.01 o -8 -4 1 1 116.02 119.31 2.49 o -8 -4 1 2 10.86 11.36 1.56 o -6 -4 1 -2 9.46 10.13 2.47 o -6 -4 1 -1 14.03 15.08 2.29 o -6 -4 1 0 155.75 158.82 3.24 o -6 -4 1 1 135.49 128.69 2.88 o -6 -4 1 2 14.19 13.13 1.23 o -4 -4 1 -2 2.81 2.22 1.29 < -4 -4 1 -1 73.19 74.74 1.87 o -4 -4 1 0 1020.37 1126.98 4.96 o -4 -4 1 1 383.56 415.23 3.37 o -4 -4 1 2 13.13 12.34 1.06 o -2 -4 1 -2 0.02 0.40 1.76 < -2 -4 1 -1 43.40 47.55 1.34 o -2 -4 1 0 637.61 678.66 2.26 o -2 -4 1 1 10.75 10.64 0.67 o -2 -4 1 2 0.01 0.31 0.37 < 0 -4 1 -2 0.96 0.73 0.53 < 0 -4 1 -1 133.01 148.49 0.95 o 0 -4 1 0 2117.47 2267.84 3.54 o 0 -4 1 1 53.14 52.59 0.39 o 0 -4 1 2 1.28 0.86 0.28 o 2 -4 1 -2 0.03 0.44 0.50 < 2 -4 1 -1 75.57 66.54 0.69 o 2 -4 1 0 275.65 285.04 2.64 o 2 -4 1 1 32.72 32.70 1.73 o 2 -4 1 2 0.20 0.54 0.58 < 4 -4 1 -2 1.00 0.67 0.84 < 4 -4 1 -1 72.64 71.61 1.09 o 4 -4 1 0 5.62 6.02 0.84 o 4 -4 1 1 0.13 0.78 1.03 < 4 -4 1 2 8.86 8.76 0.92 o 6 -4 1 -2 12.09 12.60 1.29 o 6 -4 1 -1 254.35 238.34 2.45 o 6 -4 1 0 193.24 186.35 2.34 o 6 -4 1 1 0.11 0.54 1.48 < 6 -4 1 2 1.24 0.16 1.49 < 8 -4 1 -2 5.11 6.11 2.24 < 8 -4 1 -1 92.29 89.98 2.57 o 8 -4 1 0 168.04 161.63 2.80 o 8 -4 1 1 5.74 5.24 2.04 < 8 -4 1 2 7.06 6.44 2.27 < 10 -4 1 -2 18.73 22.14 3.11 o 10 -4 1 -1 128.89 126.30 3.61 o -11 -3 1 1 6.29 5.07 3.10 < -11 -3 1 2 0.50 0.47 2.44 < -9 -3 1 -2 0.01 -0.05 2.41 < -9 -3 1 -1 31.21 30.98 2.26 o -9 -3 1 0 10.64 13.41 2.01 o -9 -3 1 1 6.52 4.85 1.77 < -9 -3 1 2 0.17 0.39 1.84 < -7 -3 1 -2 1.38 1.34 1.77 < -7 -3 1 -1 141.83 154.52 2.52 o -7 -3 1 0 2708.16 2804.48 8.52 o -7 -3 1 1 38.47 40.94 1.46 o -7 -3 1 2 1.40 2.71 1.06 < -5 -3 1 -2 1.44 2.35 2.05 < -5 -3 1 -1 21.73 26.28 2.13 o -5 -3 1 0 355.99 410.76 6.01 o -5 -3 1 1 53.05 56.36 1.88 o -5 -3 1 2 8.79 10.07 1.00 o -3 -3 1 -2 3.82 4.82 1.06 o -3 -3 1 -1 27.69 31.75 1.15 o -3 -3 1 0 5127.91 5266.25 10.34 o -3 -3 1 1 77.55 76.03 0.87 o -3 -3 1 2 0.33 0.47 0.48 < -1 -3 1 -2 7.98 8.74 0.58 o -1 -3 1 -1 4.19 4.20 0.48 o -1 -3 1 0 988.87 808.23 2.25 o -1 -3 1 1 4.59 5.74 0.25 o -1 -3 1 2 0.37 0.23 0.22 < 1 -3 1 -2 0.80 0.51 0.39 < 1 -3 1 -1 95.44 86.60 0.55 o 1 -3 1 0 7395.11 7425.71 3.38 o 1 -3 1 1 83.61 86.30 0.53 o 1 -3 1 2 1.12 1.07 0.36 o 3 -3 1 -2 0.00 -0.44 0.47 < 3 -3 1 -1 24.40 21.31 0.95 o 3 -3 1 0 4143.59 3702.51 7.26 o 3 -3 1 1 20.55 18.08 1.14 o 3 -3 1 2 0.10 1.14 0.68 < 5 -3 1 -1 77.44 77.95 1.26 o 5 -3 1 0 7.27 8.81 1.00 o 5 -3 1 1 322.95 317.68 2.59 o 5 -3 1 2 1.98 1.06 1.66 < 7 -3 1 -2 0.80 0.93 1.12 < 7 -3 1 -1 8.48 6.13 1.52 o 7 -3 1 0 696.22 685.50 4.51 o 7 -3 1 1 36.40 35.68 2.10 o 7 -3 1 2 3.43 3.49 2.12 < 9 -3 1 -2 3.78 4.26 2.40 < 9 -3 1 -1 2.78 3.63 2.27 < 9 -3 1 0 68.21 66.22 3.66 o 9 -3 1 1 106.65 107.75 3.47 o 11 -3 1 -2 0.65 0.33 4.89 < -10 -2 1 -1 21.35 20.57 3.84 o -10 -2 1 0 27.95 30.58 2.93 o -10 -2 1 1 39.73 42.48 2.52 o -10 -2 1 2 20.05 24.04 2.33 o -8 -2 1 -2 4.08 4.36 2.18 < -8 -2 1 -1 85.41 84.13 2.21 o -8 -2 1 0 99.74 108.31 2.12 o -8 -2 1 1 76.12 79.05 1.90 o -8 -2 1 2 2.28 3.14 1.38 < -6 -2 1 -2 8.09 8.31 1.54 o -6 -2 1 -1 86.11 87.44 2.29 o -6 -2 1 0 149.28 154.36 2.04 o -6 -2 1 1 3.98 5.66 1.07 o -6 -2 1 2 2.06 2.96 0.93 o -4 -2 1 -2 0.74 1.60 2.38 < -4 -2 1 -1 160.90 170.60 2.63 o -4 -2 1 0 2292.89 2503.21 7.39 o -4 -2 1 1 65.91 68.79 1.39 o -4 -2 1 2 0.12 0.06 0.42 < -2 -2 1 -2 0.03 0.19 0.53 < -2 -2 1 -1 291.73 326.36 1.20 o -2 -2 1 0 36.36 43.68 0.58 o -2 -2 1 1 47.71 53.19 0.51 o -2 -2 1 2 5.82 5.17 0.25 o 0 -2 1 -2 0.90 0.72 0.33 < 0 -2 1 -1 70.07 68.32 0.50 o 0 -2 1 0 12368.30 11554.50 3.09 o 0 -2 1 1 17.81 16.62 0.19 o 0 -2 1 2 1.27 1.52 0.22 o 2 -2 1 -2 0.82 0.78 0.31 < 2 -2 1 -1 69.57 69.86 0.55 o 2 -2 1 0 3495.10 3586.29 3.49 o 2 -2 1 1 9.96 9.21 1.03 o 2 -2 1 2 2.58 2.12 0.51 o 4 -2 1 -2 6.57 7.03 0.51 o 4 -2 1 -1 28.58 29.10 0.54 o 4 -2 1 0 2113.46 2066.18 3.62 o 4 -2 1 1 1.50 1.18 0.79 < 4 -2 1 2 1.73 1.62 1.03 < 6 -2 1 -2 2.01 1.91 0.72 < 6 -2 1 -1 120.03 121.89 1.31 o 6 -2 1 0 1285.67 1339.07 3.73 o 6 -2 1 1 13.24 14.00 1.85 o 6 -2 1 2 1.79 2.08 2.05 < 8 -2 1 -2 25.61 29.89 1.99 o 8 -2 1 -1 127.36 133.52 3.07 o 8 -2 1 0 125.18 135.74 4.06 o 8 -2 1 1 65.67 65.26 2.96 o 8 -2 1 2 2.42 2.43 3.39 < 10 -2 1 -2 0.51 1.14 2.35 < 10 -2 1 -1 12.13 13.88 3.50 o -11 -1 1 1 132.05 135.46 4.84 o -11 -1 1 2 6.21 6.86 2.82 < -9 -1 1 -2 2.35 2.99 2.82 < -9 -1 1 -1 14.88 16.12 2.40 o -9 -1 1 0 1205.08 1225.89 6.14 o -9 -1 1 1 55.97 60.02 2.21 o -9 -1 1 2 5.72 7.48 1.76 o -7 -1 1 -2 4.52 5.85 1.54 o -7 -1 1 -1 141.42 148.78 2.15 o -7 -1 1 0 9.43 21.84 1.40 o -7 -1 1 1 420.86 442.88 2.37 o -7 -1 1 2 43.45 44.38 1.51 o -5 -1 1 -2 9.95 9.65 1.57 o -5 -1 1 -1 0.36 0.92 1.07 < -5 -1 1 0 1960.37 2077.06 6.16 o -5 -1 1 1 164.53 175.52 1.93 o -5 -1 1 2 0.05 0.75 1.06 < -3 -1 1 -2 11.44 11.17 1.01 o -3 -1 1 -1 126.27 134.68 1.32 o -3 -1 1 0 5890.72 5986.39 5.48 o -3 -1 1 1 280.97 270.27 1.48 o -3 -1 1 2 9.42 8.59 0.62 o -1 -1 1 -2 4.10 2.99 0.34 o -1 -1 1 -1 4.03 4.90 0.36 o -1 -1 1 0 878.89 836.18 1.24 o -1 -1 1 1 64.80 58.80 0.28 o -1 -1 1 2 0.09 0.33 0.20 < 1 -1 1 -2 1.33 1.14 0.19 o 1 -1 1 -1 33.90 31.96 0.19 o 1 -1 1 0 7364.52 7531.71 3.79 o 1 -1 1 1 0.46 0.28 0.42 < 1 -1 1 2 1.18 1.29 0.78 < 3 -1 1 -2 2.59 2.52 0.31 o 3 -1 1 -1 0.25 1.07 0.61 < 3 -1 1 0 839.87 945.59 2.25 o 3 -1 1 1 84.17 85.73 1.90 o 3 -1 1 2 0.59 0.70 1.21 < 5 -1 1 -2 9.39 9.97 0.95 o 5 -1 1 -1 239.52 233.91 1.47 o 5 -1 1 0 2454.09 2542.95 5.57 o 5 -1 1 1 25.01 25.19 1.74 o 5 -1 1 2 1.59 2.08 1.63 < 7 -1 1 -2 5.33 4.48 1.18 o 7 -1 1 -1 10.54 10.36 1.26 o 7 -1 1 0 69.80 75.16 2.07 o 7 -1 1 1 30.05 29.88 2.30 o 7 -1 1 2 2.13 2.38 2.44 < 9 -1 1 -2 8.29 10.55 1.79 o 9 -1 1 -1 137.01 133.89 3.33 o 9 -1 1 0 2.95 7.02 2.69 < 9 -1 1 1 12.60 14.39 2.94 o 11 -1 1 -2 14.16 14.02 5.12 < -12 0 1 2 19.04 18.87 5.38 o -10 0 1 -1 115.35 112.02 6.72 o -10 0 1 0 128.14 131.01 4.47 o -10 0 1 1 0.60 -0.79 2.50 < -10 0 1 2 1.59 2.77 1.94 < -8 0 1 -2 0.25 0.78 2.01 < -8 0 1 -1 67.50 74.30 2.05 o -8 0 1 0 35.60 40.83 1.85 o -8 0 1 1 7.50 8.12 1.54 o -8 0 1 2 6.60 5.40 1.40 o -6 0 1 -2 4.71 4.87 1.31 o -6 0 1 -1 204.10 217.60 1.95 o -6 0 1 0 1884.74 2083.18 4.50 o -6 0 1 1 7.45 7.48 1.03 o -6 0 1 2 4.38 5.62 1.42 o -4 0 1 -2 6.63 5.63 1.12 o -4 0 1 -1 293.81 327.22 2.86 o -4 0 1 0 25.15 18.29 0.73 o -4 0 1 1 74.40 73.61 0.93 o -4 0 1 2 5.48 5.09 0.48 o -2 0 1 -2 0.01 -0.23 0.37 < -2 0 1 -1 49.93 45.10 0.47 o -2 0 1 0 20847.90 20476.90 9.66 o -2 0 1 1 80.74 75.18 0.55 o -2 0 1 2 2.30 1.84 0.26 o 0 0 1 -2 0.48 0.53 0.19 < 0 0 1 -1 20.96 19.41 0.20 o 0 0 1 0 1462.85 1418.35 1.55 o 0 0 1 1 21.99 19.92 0.40 o 0 0 1 2 1.54 1.84 0.51 o 2 0 1 -2 1.96 1.57 0.30 o 2 0 1 -1 5.61 5.45 0.40 o 2 0 1 0 1981.74 1901.20 3.20 o 2 0 1 1 46.12 51.64 0.93 o 2 0 1 2 3.10 3.33 0.68 o 4 0 1 -2 1.18 1.37 0.51 < 4 0 1 -1 56.04 55.78 0.73 o 4 0 1 0 4497.67 4870.22 14.19 o 4 0 1 1 23.73 24.77 1.26 o 4 0 1 2 0.07 0.05 1.52 < 6 0 1 -2 6.92 6.99 1.48 o 6 0 1 -1 29.96 31.95 2.01 o 6 0 1 0 308.88 329.61 2.71 o 6 0 1 1 84.93 88.34 2.35 o 6 0 1 2 0.38 1.38 1.79 < 8 0 1 -2 0.77 1.10 1.14 < 8 0 1 -1 8.32 8.32 1.45 o 8 0 1 0 1298.41 1342.02 6.30 o 8 0 1 1 99.12 100.04 3.27 o 8 0 1 2 0.06 -2.07 2.71 < 10 0 1 -2 0.95 0.28 2.52 < 10 0 1 -1 2.13 3.33 5.43 < 10 0 1 0 61.36 65.95 6.68 o -11 1 1 1 112.90 119.09 4.62 o -11 1 1 2 25.73 28.13 2.93 o -9 1 1 -2 13.48 11.62 4.57 < -9 1 1 -1 1.03 0.54 3.05 < -9 1 1 0 331.54 364.30 4.15 o -9 1 1 1 88.27 93.69 2.23 o -9 1 1 2 17.27 21.01 1.54 o -7 1 1 -2 11.00 12.07 1.34 o -7 1 1 -1 15.91 19.59 1.31 o -7 1 1 0 599.12 638.16 3.67 o -7 1 1 1 304.85 328.22 2.70 o -7 1 1 2 14.71 16.88 1.14 o -5 1 1 -2 2.87 4.61 1.20 o -5 1 1 -1 37.39 39.06 1.57 o -5 1 1 0 43.26 66.82 1.35 o -5 1 1 1 80.11 79.73 2.55 o -5 1 1 2 14.08 12.43 1.00 o -3 1 1 -2 19.47 17.44 0.64 o -3 1 1 -1 40.91 40.27 0.68 o -3 1 1 0 1942.00 2245.74 3.09 o -3 1 1 1 225.42 213.33 0.91 o -3 1 1 2 1.18 1.35 0.40 o -1 1 1 -2 1.01 1.04 0.30 o -1 1 1 -1 80.98 76.73 0.41 o -1 1 1 0 17.65 17.56 0.31 o -1 1 1 1 43.32 37.12 0.39 o -1 1 1 2 1.32 0.39 0.42 < 1 1 1 -1 18.48 17.03 0.34 o 1 1 1 0 5787.10 5921.44 4.84 o 1 1 1 1 39.56 40.49 0.95 o 1 1 1 2 0.41 0.14 1.04 < 3 1 1 -2 0.90 0.28 0.34 < 3 1 1 -1 41.44 45.10 0.95 o 3 1 1 0 222.12 253.08 1.98 o 3 1 1 1 29.20 33.79 1.15 o 3 1 1 2 0.31 -0.47 1.03 < 5 1 1 -2 25.63 23.65 0.81 o 5 1 1 -1 291.71 301.93 3.77 o 5 1 1 0 4362.84 4407.56 10.92 o 5 1 1 1 57.31 56.75 1.71 o 5 1 1 2 5.23 4.11 1.59 < 7 1 1 -2 3.04 3.49 1.28 < 7 1 1 -1 51.15 52.00 1.70 o 7 1 1 0 59.98 63.23 1.90 o 7 1 1 1 5.78 5.07 1.68 o 7 1 1 2 6.58 5.37 2.30 < 9 1 1 -2 22.23 23.14 1.71 o 9 1 1 -1 179.41 177.34 2.59 o 9 1 1 0 284.66 276.52 4.28 o 9 1 1 1 67.04 63.22 3.38 o 11 1 1 -2 6.73 7.59 3.95 < -10 2 1 -1 55.54 59.40 5.98 o -10 2 1 0 231.74 233.57 4.94 o -10 2 1 1 41.33 42.14 2.41 o -10 2 1 2 0.58 2.36 1.94 < -8 2 1 -2 1.27 0.89 4.12 < -8 2 1 -1 93.01 96.48 3.18 o -8 2 1 0 741.62 762.71 4.14 o -8 2 1 1 107.25 114.90 2.02 o -8 2 1 2 7.29 9.43 1.35 o -6 2 1 -2 9.53 10.60 1.28 o -6 2 1 -1 75.39 78.45 1.85 o -6 2 1 0 870.18 861.65 5.56 o -6 2 1 1 78.78 85.79 1.74 o -6 2 1 2 4.38 4.82 1.01 o -4 2 1 -2 0.76 0.79 0.79 < -4 2 1 -1 124.62 127.67 1.26 o -4 2 1 0 7044.24 7138.85 7.20 o -4 2 1 1 326.76 313.80 1.47 o -4 2 1 2 11.13 10.44 0.70 o -2 2 1 -2 0.65 0.37 0.36 < -2 2 1 -1 3.04 3.87 0.30 o -2 2 1 0 176.34 166.05 0.69 o -2 2 1 1 18.09 13.94 0.31 o -2 2 1 2 0.05 0.09 0.45 < 0 2 1 -2 0.52 0.79 0.22 o 0 2 1 -1 1.01 0.87 0.19 o 0 2 1 0 14479.90 15219.50 8.27 o 0 2 1 1 3.51 2.16 0.39 o 0 2 1 2 3.41 2.16 0.62 o 2 2 1 -2 1.60 0.93 0.40 < 2 2 1 -1 4.39 5.35 0.47 o 2 2 1 0 2629.82 2880.89 3.94 o 2 2 1 1 0.58 -0.08 0.72 < 2 2 1 2 1.46 1.43 1.03 < 4 2 1 -2 4.20 3.69 0.64 o 4 2 1 -1 9.98 10.46 0.82 o 4 2 1 0 1738.85 1894.49 5.31 o 4 2 1 1 200.29 211.26 2.23 o 4 2 1 2 0.03 0.33 1.32 < 6 2 1 -2 0.24 0.58 1.40 < 6 2 1 -1 0.03 0.16 1.24 < 6 2 1 0 317.64 332.81 3.02 o 6 2 1 1 71.56 69.28 2.01 o 6 2 1 2 0.81 1.71 1.79 < 8 2 1 -2 1.99 1.77 1.49 < 8 2 1 -1 39.35 40.16 2.32 o 8 2 1 0 1.49 3.05 1.91 < 8 2 1 1 56.50 52.15 2.33 o 8 2 1 2 6.15 5.23 3.47 < 10 2 1 -2 1.70 2.12 1.88 < 10 2 1 -1 3.61 6.72 3.50 < 10 2 1 0 414.52 423.76 9.87 o -11 3 1 1 8.86 10.78 2.86 o -11 3 1 2 9.99 10.88 2.71 o -9 3 1 -2 3.11 4.59 3.38 < -9 3 1 -1 51.05 47.85 3.38 o -9 3 1 0 195.95 208.80 3.57 o -9 3 1 1 10.27 12.03 1.73 o -9 3 1 2 8.92 8.48 1.65 o -7 3 1 -2 4.44 4.25 1.71 < -7 3 1 -1 198.72 199.71 2.59 o -7 3 1 0 1620.61 1590.21 4.85 o -7 3 1 1 2.95 2.96 1.04 < -7 3 1 2 4.16 2.77 1.07 < -5 3 1 -2 4.19 4.01 0.92 o -5 3 1 -1 157.79 157.11 2.38 o -5 3 1 0 12.48 16.21 1.21 o -5 3 1 1 23.77 24.37 1.26 o -5 3 1 2 0.05 0.26 1.70 < -3 3 1 -2 0.78 0.22 0.75 < -3 3 1 -1 455.36 446.60 1.83 o -3 3 1 0 3053.49 2959.13 4.10 o -3 3 1 1 0.08 1.03 0.72 < -3 3 1 2 1.15 1.46 0.47 o -1 3 1 -2 1.70 1.43 0.31 o -1 3 1 -1 121.68 110.63 0.62 o -1 3 1 0 321.76 205.98 0.77 o -1 3 1 1 182.73 169.78 0.75 o -1 3 1 2 3.10 2.74 0.51 o 1 3 1 -2 2.05 1.43 0.34 o 1 3 1 -1 84.60 79.07 0.65 o 1 3 1 0 6920.39 7435.49 6.75 o 1 3 1 1 30.89 34.21 1.59 o 3 3 1 -2 3.07 3.80 0.58 o 3 3 1 -1 42.11 44.60 0.82 o 3 3 1 0 5127.63 5510.91 7.81 o 3 3 1 1 0.10 -0.08 0.84 < 3 3 1 2 5.42 4.50 1.31 o 5 3 1 -2 1.08 1.32 1.00 < 5 3 1 -1 1.94 3.30 1.10 < 5 3 1 0 155.99 178.85 2.27 o 5 3 1 1 13.23 13.69 1.56 o 5 3 1 2 3.49 2.89 1.88 < 7 3 1 -2 6.46 7.33 1.60 o 7 3 1 -1 84.33 82.50 2.05 o 7 3 1 0 1367.79 1365.91 6.14 o 7 3 1 1 40.94 40.66 2.82 o 7 3 1 2 0.25 -0.11 2.35 < 9 3 1 -2 1.51 2.54 1.77 < 9 3 1 -1 26.42 27.21 2.16 o 9 3 1 0 214.37 212.69 3.32 o 9 3 1 1 17.17 17.12 5.66 o 11 3 1 -2 2.33 2.52 3.70 < -10 4 1 -1 11.30 13.93 4.45 o -10 4 1 0 15.84 14.89 2.79 o -10 4 1 1 196.07 202.16 3.85 o -10 4 1 2 15.87 20.24 2.49 o -8 4 1 -2 6.87 5.88 2.80 < -8 4 1 -1 30.65 30.33 2.24 o -8 4 1 0 115.69 107.77 1.95 o -8 4 1 1 166.13 163.32 2.40 o -8 4 1 2 12.12 13.41 1.51 o -6 4 1 -2 10.79 9.74 1.54 o -6 4 1 -1 0.41 0.61 1.15 < -6 4 1 0 151.89 159.43 1.74 o -6 4 1 1 242.77 240.45 2.71 o -6 4 1 2 17.98 18.08 1.21 o -4 4 1 -2 13.16 13.93 1.00 o -4 4 1 -1 10.48 8.84 0.93 o -4 4 1 0 12.60 11.17 0.81 o -4 4 1 1 631.36 609.60 3.93 o -4 4 1 2 7.17 6.41 0.76 o -2 4 1 -2 7.78 6.89 0.45 o -2 4 1 -1 14.61 13.38 0.54 o -2 4 1 0 3255.15 3163.16 3.80 o -2 4 1 1 51.23 50.76 0.68 o -2 4 1 2 0.37 0.08 0.81 < 0 4 1 -2 7.23 6.22 0.62 o 0 4 1 -1 43.50 40.60 0.50 o 0 4 1 0 734.78 766.83 1.68 o 0 4 1 1 179.68 175.56 1.26 o 0 4 1 2 0.03 -0.30 1.01 < 2 4 1 -2 2.76 2.58 0.42 o 2 4 1 -1 5.17 4.00 0.64 o 2 4 1 0 206.18 219.24 2.00 o 2 4 1 1 7.65 8.09 1.68 o 2 4 1 2 0.10 -0.14 1.17 < 4 4 1 -2 1.27 0.36 1.23 < 4 4 1 -1 7.81 8.68 1.59 o 4 4 1 0 262.13 279.40 2.23 o 4 4 1 1 9.98 9.74 1.06 o 4 4 1 2 0.05 1.18 1.48 < 6 4 1 -2 4.78 5.18 1.00 o 6 4 1 -1 229.66 234.21 2.24 o 6 4 1 0 18.41 15.59 1.99 o 6 4 1 1 5.19 4.54 2.10 < 6 4 1 2 2.55 1.79 1.90 < 8 4 1 -2 21.16 19.73 2.02 o 8 4 1 -1 50.04 46.55 2.35 o 8 4 1 0 0.37 -0.31 2.32 < 8 4 1 1 1.75 0.17 2.49 < 8 4 1 2 1.39 -0.31 3.58 < 10 4 1 -2 4.10 3.66 2.68 < 10 4 1 -1 83.49 81.26 3.44 o -11 5 1 2 0.41 0.48 2.78 < -9 5 1 -2 4.28 4.42 2.75 < -9 5 1 -1 24.82 25.22 2.61 o -9 5 1 0 833.09 773.90 5.97 o -9 5 1 1 27.31 25.04 2.41 o -9 5 1 2 0.60 -0.37 2.07 < -7 5 1 -2 0.69 -0.61 1.91 < -7 5 1 -1 240.60 236.61 2.68 o -7 5 1 0 15.48 17.64 1.49 o -7 5 1 1 216.49 220.52 2.51 o -7 5 1 2 8.94 10.81 1.37 o -5 5 1 -2 0.64 0.68 1.43 < -5 5 1 -1 34.63 36.74 1.65 o -5 5 1 0 1938.45 1916.64 6.83 o -5 5 1 1 15.10 12.67 1.35 o -5 5 1 2 0.01 -0.78 1.43 < -3 5 1 -2 0.01 0.00 0.81 < -3 5 1 -1 131.93 127.09 1.34 o -3 5 1 0 2658.07 2552.16 7.09 o -3 5 1 1 257.62 247.65 1.61 o -3 5 1 2 9.71 9.40 0.78 o -1 5 1 -2 0.02 0.00 0.48 < -1 5 1 -1 91.24 84.23 1.26 o -1 5 1 0 4177.86 4792.09 9.16 o -1 5 1 1 3.46 3.03 0.56 o -1 5 1 2 0.24 1.26 0.72 < 1 5 1 -2 9.96 8.48 0.84 o 1 5 1 -1 38.80 39.99 1.00 o 1 5 1 0 4639.31 4569.23 7.64 o 1 5 1 1 16.67 15.58 0.90 o 1 5 1 2 1.54 0.44 1.56 < 3 5 1 -2 10.81 8.87 0.78 o 3 5 1 -1 2.68 1.56 1.24 < 3 5 1 0 186.87 231.32 2.06 o 3 5 1 1 18.66 16.57 1.37 o 3 5 1 2 0.12 -0.11 1.38 < 5 5 1 -2 1.69 2.54 1.37 < 5 5 1 -1 3.13 2.55 1.31 < 5 5 1 0 3493.19 3641.08 8.95 o 5 5 1 1 70.64 71.63 1.82 o 5 5 1 2 0.23 1.04 1.51 < 7 5 1 -2 9.15 7.67 1.79 o 7 5 1 -1 18.09 19.46 2.12 o 7 5 1 0 94.82 93.81 2.83 o 7 5 1 1 53.65 51.11 2.38 o 7 5 1 2 0.01 0.51 2.22 < 9 5 1 -2 0.21 -0.64 2.16 < 9 5 1 -1 25.88 24.37 2.72 o 9 5 1 0 206.06 180.55 3.85 o -10 6 1 0 12.74 10.07 4.00 < -10 6 1 1 5.72 6.72 2.60 < -10 6 1 2 4.23 4.05 2.46 < -8 6 1 -2 3.63 3.94 2.30 < -8 6 1 -1 51.13 47.39 2.57 o -8 6 1 0 7.27 7.62 2.12 o -8 6 1 1 53.41 53.35 2.29 o -8 6 1 2 34.11 36.21 2.19 o -6 6 1 -2 12.42 12.15 2.24 o -6 6 1 -1 17.09 15.98 1.84 o -6 6 1 0 171.61 170.49 2.77 o -6 6 1 1 102.01 104.40 1.95 o -6 6 1 2 6.89 6.07 1.38 o -4 6 1 -2 0.50 -0.79 1.09 < -4 6 1 -1 336.33 329.64 3.10 o -4 6 1 0 122.79 117.75 1.56 o -4 6 1 1 58.62 55.38 1.15 o -4 6 1 2 1.24 0.87 0.84 < -2 6 1 -2 4.47 3.98 1.09 o -2 6 1 -1 14.59 13.94 0.64 o -2 6 1 0 3536.86 3244.49 13.20 o -2 6 1 1 74.54 70.41 1.57 o -2 6 1 2 6.67 6.35 1.29 o 0 6 1 -2 2.15 1.63 0.34 o 0 6 1 -1 177.05 148.11 1.48 o 0 6 1 0 101.00 97.96 1.29 o 0 6 1 1 97.34 100.44 1.79 o 0 6 1 2 0.58 0.19 1.03 < 2 6 1 -2 2.62 3.30 1.10 < 2 6 1 -1 12.34 11.31 0.87 o 2 6 1 0 820.59 854.91 3.96 o 2 6 1 1 18.30 18.64 1.57 o 2 6 1 2 2.51 2.07 1.43 < 4 6 1 -2 4.36 5.66 1.38 o 4 6 1 -1 141.04 150.58 1.82 o 4 6 1 0 1480.41 1632.56 5.21 o 4 6 1 1 24.62 27.43 1.51 o 4 6 1 2 2.37 2.13 1.60 < 6 6 1 -2 2.02 1.54 1.14 < 6 6 1 -1 0.41 -1.15 1.20 < 6 6 1 0 250.06 261.23 2.73 o 6 6 1 1 1.77 2.66 1.65 < 6 6 1 2 4.94 4.68 2.57 < 8 6 1 -2 5.06 7.03 2.64 < 8 6 1 -1 93.35 90.17 3.67 o 8 6 1 0 1015.42 950.96 6.63 o 8 6 1 1 30.28 28.54 2.94 o 10 6 1 -2 3.07 2.35 2.72 < -9 7 1 -1 88.61 83.72 3.18 o -9 7 1 0 3.55 0.86 2.40 < -9 7 1 1 206.06 204.97 3.18 o -9 7 1 2 7.14 8.25 2.18 o -7 7 1 -2 1.96 3.59 2.61 < -7 7 1 -1 3.77 2.54 1.96 < -7 7 1 0 906.91 879.11 4.96 o -7 7 1 1 71.79 72.98 2.99 o -7 7 1 2 1.05 2.43 1.73 < -5 7 1 -2 3.49 2.60 1.73 < -5 7 1 -1 86.30 82.73 1.87 o -5 7 1 0 545.92 570.30 3.26 o -5 7 1 1 362.14 350.62 2.57 o -5 7 1 2 8.75 8.92 1.12 o -3 7 1 -2 16.07 14.55 1.37 o -3 7 1 -1 35.24 33.77 0.90 o -3 7 1 0 196.36 201.01 2.23 o -3 7 1 1 92.70 85.98 1.71 o -3 7 1 2 0.10 -0.06 1.38 < -1 7 1 -2 0.68 0.73 0.70 < -1 7 1 -1 60.37 59.63 1.25 o -1 7 1 0 2320.18 2311.65 8.38 o -1 7 1 1 73.38 78.31 1.70 o -1 7 1 2 0.65 0.12 1.12 < 1 7 1 -2 6.80 6.30 0.67 o 1 7 1 -1 97.17 89.16 1.32 o 1 7 1 0 2.21 2.61 1.29 < 1 7 1 1 108.00 105.37 2.57 o 1 7 1 2 0.22 1.42 1.93 < 3 7 1 -2 1.33 0.82 1.15 < 3 7 1 -1 13.95 16.54 1.07 o 3 7 1 0 2462.41 2610.69 6.07 o 3 7 1 1 75.65 76.33 1.74 o 3 7 1 2 4.31 5.10 1.48 o 5 7 1 -2 1.49 1.21 1.37 < 5 7 1 -1 61.48 61.20 1.87 o 5 7 1 0 217.20 217.65 2.49 o 5 7 1 1 23.15 22.76 2.02 o 5 7 1 2 0.05 -0.16 1.80 < 7 7 1 -2 0.67 1.56 1.38 < 7 7 1 -1 4.71 4.51 1.62 < 7 7 1 0 138.20 139.79 3.33 o 7 7 1 1 102.74 95.22 3.41 o 9 7 1 -2 3.77 4.20 3.16 < 9 7 1 -1 35.30 29.11 3.63 o -8 8 1 -2 14.67 15.65 2.19 o -8 8 1 -1 54.65 52.40 2.37 o -8 8 1 0 209.27 188.15 3.38 o -8 8 1 1 4.91 5.43 2.16 < -8 8 1 2 0.02 -0.42 2.01 < -6 8 1 -2 0.02 -0.65 1.62 < -6 8 1 -1 186.78 188.11 3.04 o -6 8 1 0 78.79 81.04 2.32 o -6 8 1 1 2.97 2.10 1.65 < -6 8 1 2 0.01 0.05 1.59 < -4 8 1 -2 10.07 9.66 1.65 o -4 8 1 -1 53.23 55.48 1.85 o -4 8 1 0 2156.46 2033.84 7.19 o -4 8 1 1 0.07 -0.50 1.24 < -4 8 1 2 0.03 0.90 2.82 < -2 8 1 -2 0.01 0.37 1.07 < -2 8 1 -1 156.87 155.67 2.20 o -2 8 1 0 23.19 24.83 1.90 o -2 8 1 1 66.75 69.81 2.29 o -2 8 1 2 2.48 2.32 1.40 < 0 8 1 -2 0.54 -0.62 1.35 < 0 8 1 -1 1.85 2.26 1.38 < 0 8 1 0 3077.31 3090.33 7.18 o 0 8 1 1 16.58 17.69 1.32 o 0 8 1 2 0.05 0.26 1.34 < 2 8 1 -2 7.17 5.45 1.91 < 2 8 1 -1 2.61 3.97 1.26 o 2 8 1 0 1428.16 1465.80 7.80 o 2 8 1 1 76.15 80.58 1.74 o 2 8 1 2 0.50 1.57 1.51 < 4 8 1 -2 1.68 -0.22 1.24 < 4 8 1 -1 2.35 4.12 1.35 o 4 8 1 0 896.48 930.70 4.47 o 4 8 1 1 79.01 76.53 2.24 o 4 8 1 2 0.21 -0.22 1.87 < 6 8 1 -2 14.46 14.70 1.42 o 6 8 1 -1 67.95 65.91 1.81 o 6 8 1 0 700.35 681.52 4.34 o 6 8 1 1 29.70 28.97 2.46 o 6 8 1 2 3.66 2.77 2.83 < 8 8 1 -2 0.02 -1.29 2.96 < 8 8 1 -1 3.05 3.67 3.25 < 8 8 1 0 83.95 82.68 6.38 o -9 9 1 0 248.76 234.18 6.50 o -9 9 1 2 13.77 13.30 3.28 o -7 9 1 -2 5.15 6.97 2.30 o -7 9 1 -1 1.69 0.54 2.18 < -7 9 1 0 159.57 153.73 3.10 o -7 9 1 1 105.25 107.27 2.76 o -7 9 1 2 16.30 15.42 1.99 o -5 9 1 -2 7.61 8.35 1.77 o -5 9 1 -1 12.83 13.46 1.82 o -5 9 1 0 135.94 121.35 3.18 o -5 9 1 1 10.72 8.90 1.68 o -5 9 1 2 8.70 9.38 2.64 o -3 9 1 -2 0.05 0.45 1.24 < -3 9 1 -1 70.89 65.43 1.95 o -3 9 1 0 8.21 9.54 1.60 o -3 9 1 1 169.66 178.33 4.38 o -3 9 1 2 5.77 5.76 1.71 o -1 9 1 -2 3.72 3.98 1.34 < -1 9 1 -1 3.87 4.11 1.29 o -1 9 1 0 2.39 2.50 1.40 < -1 9 1 1 1.34 1.17 1.28 < -1 9 1 2 0.60 0.50 1.45 < 1 9 1 -2 3.05 3.83 1.10 o 1 9 1 -1 72.48 71.61 1.68 o 1 9 1 0 51.98 60.69 1.87 o 1 9 1 1 4.06 3.75 1.57 < 1 9 1 2 0.00 0.48 2.41 < 3 9 1 -2 3.14 3.44 1.38 < 3 9 1 -1 45.34 48.69 1.49 o 3 9 1 0 632.45 648.65 3.86 o 3 9 1 1 14.75 16.01 1.73 o 3 9 1 2 4.47 4.61 1.85 < 5 9 1 -2 0.67 0.89 1.62 < 5 9 1 -1 8.89 6.94 1.82 o 5 9 1 0 0.92 1.17 1.76 < 5 9 1 1 28.35 24.60 2.71 o 5 9 1 2 2.13 1.26 2.86 < 7 9 1 -2 5.44 6.61 2.15 o 7 9 1 -1 131.03 124.98 2.96 o 7 9 1 0 297.04 281.68 4.47 o -8 10 1 0 191.53 186.40 5.92 o -8 10 1 1 12.18 10.55 2.47 o -8 10 1 2 0.82 2.83 2.38 < -6 10 1 -2 0.22 -1.07 2.13 < -6 10 1 -1 13.41 13.32 1.93 o -6 10 1 0 269.44 263.79 3.15 o -6 10 1 1 71.87 74.55 2.65 o -6 10 1 2 0.74 1.40 4.09 < -4 10 1 -2 2.36 1.65 1.54 < -4 10 1 -1 82.06 77.14 2.01 o -4 10 1 0 213.01 231.24 3.21 o -4 10 1 1 161.72 164.81 3.69 o -4 10 1 2 1.62 1.00 2.41 < -2 10 1 -2 0.03 -0.09 1.57 < -2 10 1 -1 0.94 2.18 2.04 < -2 10 1 0 2062.77 2123.40 7.98 o -2 10 1 1 6.13 4.22 1.46 < -2 10 1 2 0.21 0.56 1.59 < 0 10 1 -2 0.02 0.11 1.26 < 0 10 1 -1 51.13 50.69 1.65 o 0 10 1 0 186.44 192.14 2.45 o 0 10 1 1 140.18 135.97 2.37 o 0 10 1 2 0.76 1.71 1.87 < 2 10 1 -2 0.15 0.51 1.26 < 2 10 1 -1 6.22 7.03 1.37 o 2 10 1 0 1115.59 1187.38 5.76 o 2 10 1 1 49.38 51.03 1.82 o 2 10 1 2 0.81 0.72 1.88 < 4 10 1 -2 3.33 5.73 1.56 o 4 10 1 -1 6.43 7.58 1.70 o 4 10 1 0 128.76 132.84 2.83 o 4 10 1 1 12.62 12.43 3.21 o 4 10 1 2 2.56 3.84 2.92 < 6 10 1 -2 0.05 0.06 1.76 < 6 10 1 -1 33.40 31.01 2.46 o 6 10 1 0 345.91 358.99 4.21 o 8 10 1 -2 0.29 1.66 2.64 < -7 11 1 -1 90.59 94.42 5.04 o -7 11 1 0 19.16 15.64 2.63 o -7 11 1 1 16.52 18.62 2.75 o -7 11 1 2 2.81 -0.14 3.30 < -5 11 1 -2 3.17 2.88 1.71 < -5 11 1 -1 28.19 33.49 2.12 o -5 11 1 0 229.28 232.36 3.71 o -5 11 1 1 97.01 101.85 3.69 o -5 11 1 2 0.46 0.53 2.83 < -3 11 1 -2 2.69 1.04 1.94 < -3 11 1 -1 57.53 61.07 3.07 o -3 11 1 0 90.59 92.38 3.33 o -3 11 1 1 83.69 84.00 2.60 o -3 11 1 2 0.01 -1.37 1.84 < -1 11 1 -2 0.03 -0.23 1.94 < -1 11 1 -1 112.86 122.24 2.18 o -1 11 1 0 710.38 742.55 4.95 o -1 11 1 1 4.12 2.27 1.73 < -1 11 1 2 0.01 -0.96 1.84 < 1 11 1 -2 4.30 5.49 1.42 o 1 11 1 -1 0.76 0.36 1.60 < 1 11 1 0 487.11 499.56 3.87 o 1 11 1 1 0.04 0.14 2.02 < 1 11 1 2 1.59 2.16 1.98 < 3 11 1 -2 0.05 0.61 1.80 < 3 11 1 -1 13.58 18.52 2.07 o 3 11 1 0 158.08 156.55 2.99 o 3 11 1 1 6.38 7.00 2.41 < 3 11 1 2 0.02 -0.08 2.88 < 5 11 1 -2 2.15 0.73 2.47 < 5 11 1 -1 26.70 24.51 2.77 o 5 11 1 0 1041.37 1052.19 7.55 o 7 11 1 -2 9.39 9.30 3.42 < -6 12 1 -2 5.44 4.73 4.12 < -6 12 1 -1 31.20 35.73 4.45 o -6 12 1 2 6.46 5.65 4.48 < -4 12 1 -2 0.02 -0.59 2.22 < -4 12 1 -1 15.99 12.63 3.00 o -4 12 1 0 247.32 256.97 4.98 o -4 12 1 1 0.71 1.59 3.02 < -4 12 1 2 1.83 0.72 3.89 < -2 12 1 -2 4.17 5.60 2.60 < -2 12 1 -1 15.21 17.05 2.71 o -2 12 1 0 11.09 10.35 2.85 o -2 12 1 1 179.44 187.08 4.38 o -2 12 1 2 1.81 0.34 2.41 < 0 12 1 -2 0.01 -0.31 2.30 < 0 12 1 -1 33.56 32.66 2.54 o 0 12 1 0 218.00 230.95 4.42 o 0 12 1 1 10.90 12.45 2.99 o 0 12 1 2 0.79 0.72 2.80 < 2 12 1 -2 1.34 1.66 1.91 < 2 12 1 -1 0.11 0.02 2.49 < 2 12 1 0 4.24 5.35 3.25 < 2 12 1 1 49.15 55.73 3.10 o 2 12 1 2 0.24 0.76 5.17 < 4 12 1 -2 1.71 1.65 2.97 < 4 12 1 -1 45.17 47.37 3.07 o 4 12 1 0 0.04 -0.36 2.83 < 6 12 1 -2 0.36 2.04 2.89 < -3 13 1 -2 0.34 -0.54 3.05 < -3 13 1 -1 56.52 57.50 3.64 o -3 13 1 0 170.18 168.68 4.53 o -3 13 1 1 0.92 0.34 4.15 < -3 13 1 2 0.36 0.56 4.17 < -1 13 1 -2 4.43 6.41 3.00 < -1 13 1 -1 4.21 4.89 2.97 < -1 13 1 0 711.67 754.68 6.31 o -1 13 1 1 12.24 10.83 3.28 o 1 13 1 -2 1.39 3.17 2.15 < 1 13 1 -1 61.05 62.66 2.60 o 1 13 1 0 169.66 171.74 3.88 o 1 13 1 1 57.17 54.86 5.94 o 3 13 1 -2 5.17 5.82 2.77 < 3 13 1 -1 13.10 14.41 2.88 o 3 13 1 0 1165.11 1217.17 14.01 o 5 13 1 -2 2.40 2.89 4.68 < -2 14 1 -2 0.01 0.28 3.34 < -2 14 1 -1 66.79 68.31 5.26 o 0 14 1 -2 0.01 1.31 2.32 < 0 14 1 -1 0.84 0.59 2.60 < 2 14 1 -2 2.58 0.75 2.96 < -3 -13 2 0 435.74 380.61 8.26 o -3 -13 2 1 0.00 1.51 2.66 < -3 -13 2 2 0.92 1.32 2.72 < -1 -13 2 -2 1.14 1.31 5.21 < -1 -13 2 -1 41.81 47.94 3.24 o -1 -13 2 0 233.60 245.58 4.25 o -1 -13 2 1 13.98 16.46 2.79 o -1 -13 2 2 0.50 -0.50 3.25 < 1 -13 2 -2 0.08 -0.78 2.41 < 1 -13 2 -1 2.48 1.57 2.33 < 1 -13 2 0 576.27 571.53 5.62 o 1 -13 2 1 10.31 8.88 2.75 o 1 -13 2 2 0.57 1.87 4.75 < 3 -13 2 -2 0.36 2.38 4.70 < -6 -12 2 2 0.10 -0.68 2.26 < -4 -12 2 -1 8.99 6.63 2.41 < -4 -12 2 0 199.79 192.16 2.73 o -4 -12 2 1 93.65 83.68 2.21 o -4 -12 2 2 3.83 3.41 1.68 < -2 -12 2 -2 0.77 1.17 2.36 < -2 -12 2 -1 10.74 13.71 2.30 o -2 -12 2 0 13.61 14.69 1.98 o -2 -12 2 1 13.86 16.07 2.61 o -2 -12 2 2 3.20 3.47 2.43 < 0 -12 2 -2 1.86 1.91 2.52 < 0 -12 2 -1 0.05 -0.50 2.07 < 0 -12 2 0 0.04 0.40 2.01 < 0 -12 2 1 10.02 9.93 2.40 o 0 -12 2 2 0.85 0.47 2.33 < 2 -12 2 -2 0.04 -0.76 2.44 < 2 -12 2 -1 36.20 35.95 2.26 o 2 -12 2 0 6.10 15.84 2.57 o 2 -12 2 1 37.62 44.69 3.49 o 2 -12 2 2 1.04 2.44 3.02 < 4 -12 2 -2 1.41 0.36 2.16 < 4 -12 2 -1 2.15 1.18 2.55 < 4 -12 2 0 72.92 78.11 3.07 o -7 -11 2 2 6.93 7.83 2.07 o -5 -11 2 -2 0.09 1.57 4.82 < -5 -11 2 -1 67.77 65.57 2.37 o -5 -11 2 0 473.23 451.36 3.60 o -5 -11 2 1 0.85 0.54 1.71 < -5 -11 2 2 0.30 0.61 1.60 < -3 -11 2 -2 6.96 10.30 2.29 o -3 -11 2 -1 33.77 35.84 2.41 o -3 -11 2 0 458.91 472.98 3.85 o -3 -11 2 1 15.39 15.73 1.62 o -3 -11 2 2 2.24 2.47 1.31 < -1 -11 2 -2 0.62 1.14 2.43 < -1 -11 2 -1 98.29 108.96 2.62 o -1 -11 2 0 1003.70 1005.77 4.85 o -1 -11 2 1 19.53 21.94 2.29 o -1 -11 2 2 0.32 0.45 1.87 < 1 -11 2 -2 2.23 1.49 1.99 < 1 -11 2 -1 61.32 63.31 2.27 o 1 -11 2 0 84.90 88.10 2.75 o 1 -11 2 1 71.09 74.27 2.66 o 1 -11 2 2 1.00 1.49 2.15 < 3 -11 2 -2 1.60 2.24 1.70 < 3 -11 2 -1 6.42 7.05 1.93 o 3 -11 2 0 1476.64 1509.85 6.74 o 3 -11 2 1 0.63 -0.11 2.16 < 3 -11 2 2 1.96 2.01 3.94 < 5 -11 2 -2 0.03 0.54 1.98 < 5 -11 2 -1 20.12 21.57 2.19 o 5 -11 2 0 14.58 12.57 3.00 o 5 -11 2 1 77.75 73.04 3.66 o -8 -10 2 2 0.84 1.49 2.12 < -6 -10 2 -1 7.54 8.09 2.40 o -6 -10 2 0 32.41 33.11 2.13 o -6 -10 2 1 65.64 63.87 2.46 o -6 -10 2 2 0.24 0.64 1.71 < -4 -10 2 -2 1.70 0.86 2.15 < -4 -10 2 -1 109.31 109.28 2.71 o -4 -10 2 0 1002.59 1037.65 5.32 o -4 -10 2 1 17.97 16.06 1.65 o -4 -10 2 2 5.09 4.81 1.24 o -2 -10 2 -2 1.29 0.96 1.90 < -2 -10 2 -1 6.34 8.40 1.91 o -2 -10 2 0 72.01 82.01 2.02 o -2 -10 2 1 48.84 51.23 1.56 o -2 -10 2 2 0.17 0.36 1.09 < 0 -10 2 -2 0.36 -0.33 1.99 < 0 -10 2 -1 7.78 6.74 1.70 o 0 -10 2 0 885.56 901.17 4.11 o 0 -10 2 1 39.98 40.47 1.87 o 0 -10 2 2 7.36 6.57 1.62 o 2 -10 2 -2 1.32 0.86 1.48 < 2 -10 2 -1 0.46 0.68 1.63 < 2 -10 2 0 281.49 279.64 2.46 o 2 -10 2 1 19.85 20.66 1.56 o 2 -10 2 2 0.18 0.98 1.94 < 4 -10 2 -2 2.02 2.01 1.35 < 4 -10 2 -1 134.54 138.90 2.24 o 4 -10 2 0 356.85 353.89 3.09 o 4 -10 2 1 8.68 9.15 2.10 o 4 -10 2 2 0.05 0.89 1.90 < 6 -10 2 -2 3.34 2.46 1.76 < 6 -10 2 -1 0.57 0.50 1.93 < 6 -10 2 0 347.29 333.15 3.72 o 6 -10 2 1 1.39 0.82 4.23 < -7 -9 2 -1 5.23 5.04 2.82 < -7 -9 2 0 37.07 34.17 2.44 o -7 -9 2 1 5.58 4.95 2.13 < -7 -9 2 2 2.15 1.46 1.80 < -5 -9 2 -2 2.49 1.18 2.01 < -5 -9 2 -1 3.62 3.14 1.94 < -5 -9 2 0 234.56 228.93 2.80 o -5 -9 2 1 213.42 200.72 2.59 o -5 -9 2 2 12.08 11.45 1.42 o -3 -9 2 -2 0.85 1.38 1.88 < -3 -9 2 -1 42.21 45.83 2.38 o -3 -9 2 0 513.99 533.66 4.09 o -3 -9 2 1 0.27 0.86 1.20 < -3 -9 2 2 0.03 -0.28 0.86 < -1 -9 2 -2 1.44 0.47 1.94 < -1 -9 2 -1 44.67 47.46 2.18 o -1 -9 2 0 61.12 61.26 1.49 o -1 -9 2 1 0.12 0.65 0.89 < -1 -9 2 2 0.29 1.03 1.07 < 1 -9 2 -2 0.08 1.45 1.51 < 1 -9 2 -1 61.95 64.60 1.46 o 1 -9 2 0 924.25 935.57 4.19 o 1 -9 2 1 15.20 15.17 1.26 o 1 -9 2 2 1.71 1.66 1.38 < 3 -9 2 -2 0.19 -0.58 1.42 < 3 -9 2 -1 18.61 19.36 1.29 o 3 -9 2 0 202.65 214.65 2.09 o 3 -9 2 1 77.75 75.88 1.71 o 3 -9 2 2 1.15 2.49 1.37 < 5 -9 2 -2 0.58 0.82 1.52 < 5 -9 2 -1 77.27 77.42 1.73 o 5 -9 2 0 151.68 146.98 2.30 o 5 -9 2 1 2.68 3.49 1.85 < 5 -9 2 2 4.35 4.76 1.90 < 7 -9 2 -2 5.16 5.79 1.71 o 7 -9 2 -1 30.28 30.51 2.24 o 7 -9 2 0 0.76 0.90 2.07 < -8 -8 2 0 79.94 74.46 2.88 o -8 -8 2 1 12.52 11.67 2.16 o -8 -8 2 2 1.46 1.37 2.41 < -6 -8 2 -2 0.01 0.54 2.18 < -6 -8 2 -1 73.29 68.42 2.77 o -6 -8 2 0 1038.79 1016.19 5.76 o -6 -8 2 1 7.47 9.10 1.82 o -6 -8 2 2 0.36 1.06 1.65 < -4 -8 2 -2 4.04 4.00 2.04 < -4 -8 2 -1 22.21 22.73 1.79 o -4 -8 2 0 81.45 85.30 2.52 o -4 -8 2 1 2.03 0.75 1.26 < -4 -8 2 2 0.60 0.36 0.95 < -2 -8 2 -2 7.56 8.26 1.63 o -2 -8 2 -1 28.50 30.83 1.76 o -2 -8 2 0 2576.80 2718.75 7.93 o -2 -8 2 1 30.59 32.30 1.24 o -2 -8 2 2 2.23 3.59 0.93 o 0 -8 2 -2 2.20 3.70 1.60 < 0 -8 2 -1 4.62 5.77 1.38 o 0 -8 2 0 1663.80 1652.51 5.11 o 0 -8 2 1 17.31 18.10 1.07 o 0 -8 2 2 0.93 0.65 1.07 < 2 -8 2 -2 0.18 1.06 0.90 < 2 -8 2 -1 84.11 84.01 1.42 o 2 -8 2 0 665.59 665.32 3.25 o 2 -8 2 1 3.38 3.19 1.01 o 2 -8 2 2 0.06 0.26 1.04 < 4 -8 2 -2 0.81 1.46 1.07 < 4 -8 2 -1 11.96 11.50 1.07 o 4 -8 2 0 1066.18 1058.96 4.02 o 4 -8 2 1 18.09 16.76 1.26 o 4 -8 2 2 0.69 0.72 1.63 < 6 -8 2 -2 0.29 -0.34 1.28 < 6 -8 2 -1 166.53 165.65 2.32 o 6 -8 2 0 180.76 185.01 2.85 o 6 -8 2 1 120.85 118.67 2.62 o 6 -8 2 2 0.24 0.45 1.87 < 8 -8 2 -2 0.19 -0.19 1.66 < 8 -8 2 -1 5.22 4.59 1.85 < 8 -8 2 0 558.06 520.70 8.67 o -9 -7 2 0 50.19 51.65 3.24 o -9 -7 2 1 18.47 15.17 2.47 o -9 -7 2 2 8.92 9.48 2.32 o -7 -7 2 -2 17.62 16.48 2.96 o -7 -7 2 -1 7.00 4.96 3.19 < -7 -7 2 0 41.92 41.80 2.80 o -7 -7 2 1 148.23 139.65 2.41 o -7 -7 2 2 0.83 1.15 1.68 < -5 -7 2 -2 2.76 1.84 1.68 < -5 -7 2 -1 16.21 17.10 1.73 o -5 -7 2 0 122.91 120.99 2.32 o -5 -7 2 1 2.07 1.43 1.35 < -5 -7 2 2 0.01 -0.48 1.23 < -3 -7 2 -2 6.49 7.97 1.56 o -3 -7 2 -1 100.44 102.37 2.30 o -3 -7 2 0 179.92 185.89 2.02 o -3 -7 2 1 25.70 27.23 1.18 o -3 -7 2 2 0.92 0.34 0.70 < -1 -7 2 -2 1.08 2.63 1.23 < -1 -7 2 -1 2.45 3.89 1.12 o -1 -7 2 0 0.41 1.48 1.21 < -1 -7 2 1 11.89 11.20 1.06 o -1 -7 2 2 2.83 3.89 1.18 o 1 -7 2 -2 1.59 1.85 0.78 < 1 -7 2 -1 29.39 32.30 0.81 o 1 -7 2 0 801.76 803.32 2.96 o 1 -7 2 1 46.11 46.73 1.17 o 1 -7 2 2 3.16 3.83 1.14 o 3 -7 2 -2 3.15 2.88 0.67 o 3 -7 2 -1 48.56 47.11 1.18 o 3 -7 2 0 1.04 2.15 0.95 < 3 -7 2 1 1.51 2.36 1.01 < 3 -7 2 2 0.00 -0.40 1.04 < 5 -7 2 -2 6.85 8.48 1.07 o 5 -7 2 -1 19.06 17.86 1.12 o 5 -7 2 0 306.32 305.29 2.34 o 5 -7 2 1 11.01 11.86 1.65 o 5 -7 2 2 0.00 -0.19 1.51 < 7 -7 2 -2 5.81 5.63 1.73 o 7 -7 2 -1 34.37 34.72 1.74 o 7 -7 2 0 344.11 341.91 3.24 o 7 -7 2 1 9.92 9.07 1.87 o 7 -7 2 2 1.31 0.54 3.45 < 9 -7 2 -2 9.50 8.68 2.18 o 9 -7 2 -1 89.41 83.96 5.07 o -10 -6 2 1 47.35 42.37 3.17 o -10 -6 2 2 1.40 1.99 2.83 < -8 -6 2 -2 0.01 -0.47 2.80 < -8 -6 2 -1 165.00 161.84 3.80 o -8 -6 2 0 490.67 448.95 5.04 o -8 -6 2 1 130.13 122.73 3.11 o -8 -6 2 2 11.38 10.75 1.99 o -6 -6 2 -2 1.42 1.38 1.96 < -6 -6 2 -1 33.89 37.25 2.77 o -6 -6 2 0 221.82 215.62 2.80 o -6 -6 2 1 10.02 11.50 1.80 o -6 -6 2 2 4.70 3.36 1.24 < -4 -6 2 -2 7.67 8.04 1.48 o -4 -6 2 -1 103.27 105.40 1.76 o -4 -6 2 0 2660.05 2678.17 5.81 o -4 -6 2 1 303.67 294.67 2.40 o -4 -6 2 2 17.20 16.06 1.00 o -2 -6 2 -2 0.36 0.09 1.09 < -2 -6 2 -1 16.93 18.11 1.38 o -2 -6 2 0 872.78 878.15 3.15 o -2 -6 2 1 11.61 10.75 0.86 o -2 -6 2 2 2.16 2.88 1.01 < 0 -6 2 -2 1.71 1.49 0.65 < 0 -6 2 -1 4.16 5.60 0.92 o 0 -6 2 0 671.90 749.02 2.61 o 0 -6 2 1 35.88 37.12 1.20 o 0 -6 2 2 0.88 1.18 0.92 < 2 -6 2 -2 0.04 0.47 0.72 < 2 -6 2 -1 53.90 51.88 0.92 o 2 -6 2 0 2188.30 2132.90 4.33 o 2 -6 2 1 40.97 40.42 0.90 o 2 -6 2 2 0.11 -0.42 0.79 < 4 -6 2 -2 0.11 0.20 0.87 < 4 -6 2 -1 8.45 9.04 0.89 o 4 -6 2 0 112.11 111.02 1.37 o 4 -6 2 1 13.19 12.99 0.93 o 4 -6 2 2 1.19 1.45 1.15 < 6 -6 2 -2 0.05 -0.28 1.21 < 6 -6 2 -1 30.25 25.81 1.70 o 6 -6 2 0 609.10 588.75 3.61 o 6 -6 2 1 33.59 33.86 1.71 o 6 -6 2 2 0.76 -0.26 1.70 < 8 -6 2 -2 1.60 0.68 2.08 < 8 -6 2 -1 14.72 12.88 2.38 o 8 -6 2 0 83.91 82.12 2.58 o 8 -6 2 1 33.42 33.83 3.63 o -11 -5 2 2 5.50 5.17 5.66 < -9 -5 2 -2 11.67 9.41 5.31 < -9 -5 2 -1 23.68 23.76 2.60 o -9 -5 2 0 49.21 53.81 2.66 o -9 -5 2 1 62.96 63.40 2.60 o -9 -5 2 2 9.92 10.49 2.26 o -7 -5 2 -2 1.13 1.32 2.46 < -7 -5 2 -1 32.65 34.33 2.51 o -7 -5 2 0 384.35 376.67 5.32 o -7 -5 2 1 12.02 11.09 1.71 o -7 -5 2 2 4.07 4.29 1.52 < -5 -5 2 -2 4.33 3.42 1.93 < -5 -5 2 -1 166.10 167.95 2.69 o -5 -5 2 0 790.00 772.83 3.86 o -5 -5 2 1 4.52 4.82 1.10 o -5 -5 2 2 0.53 1.96 1.06 < -3 -5 2 -2 1.89 2.64 1.20 < -3 -5 2 -1 22.19 24.10 1.12 o -3 -5 2 0 553.44 593.92 1.95 o -3 -5 2 1 25.29 22.94 0.76 o -3 -5 2 2 0.67 0.33 1.10 < -1 -5 2 -2 2.21 3.84 1.17 o -1 -5 2 -1 156.22 154.34 2.31 o -1 -5 2 0 2798.80 2584.75 3.81 o -1 -5 2 1 25.27 24.46 0.72 o -1 -5 2 2 0.79 1.15 0.62 < 1 -5 2 -2 0.90 2.54 0.48 o 1 -5 2 -1 82.60 83.17 0.90 o 1 -5 2 0 216.11 223.49 0.98 o 1 -5 2 1 62.51 62.14 1.01 o 1 -5 2 2 0.87 0.23 0.89 < 3 -5 2 -2 0.10 0.54 0.54 < 3 -5 2 -1 43.88 41.43 0.92 o 3 -5 2 0 5362.90 5181.10 6.50 o 3 -5 2 1 0.45 0.59 0.87 < 3 -5 2 2 0.06 -0.28 0.89 < 5 -5 2 -2 2.95 2.46 1.17 < 5 -5 2 -1 110.55 104.87 1.87 o 5 -5 2 0 200.81 188.43 2.35 o 5 -5 2 1 80.31 74.82 1.67 o 5 -5 2 2 5.21 4.45 1.29 o 7 -5 2 -2 2.18 0.45 1.76 < 7 -5 2 -1 63.56 57.88 2.33 o 7 -5 2 0 450.39 433.15 3.84 o 7 -5 2 1 29.23 27.00 2.13 o 7 -5 2 2 0.00 0.75 2.05 < 9 -5 2 -2 1.29 2.66 2.19 < 9 -5 2 -1 37.40 36.37 2.75 o -10 -4 2 -1 46.85 49.64 6.38 o -10 -4 2 0 150.06 150.85 3.39 o -10 -4 2 1 94.86 98.39 3.02 o -10 -4 2 2 14.63 16.37 2.46 o -8 -4 2 -2 13.38 14.19 2.32 o -8 -4 2 -1 43.71 41.16 2.40 o -8 -4 2 0 1.00 0.79 1.96 < -8 -4 2 1 42.75 41.81 1.99 o -8 -4 2 2 1.42 2.86 1.70 < -6 -4 2 -2 7.43 7.58 2.04 o -6 -4 2 -1 51.94 53.91 1.99 o -6 -4 2 0 1219.23 1212.80 5.24 o -6 -4 2 1 296.40 278.84 2.76 o -6 -4 2 2 17.69 15.86 1.63 o -4 -4 2 -2 9.12 8.84 1.24 o -4 -4 2 -1 115.84 110.12 1.62 o -4 -4 2 0 801.43 822.70 3.23 o -4 -4 2 1 10.83 11.22 0.87 o -4 -4 2 2 0.23 -0.44 0.72 < -2 -4 2 -2 13.71 11.73 1.42 o -2 -4 2 -1 0.98 0.79 0.78 < -2 -4 2 0 3715.71 3345.32 4.49 o -2 -4 2 1 82.74 74.36 1.31 o -2 -4 2 2 0.50 0.59 0.56 < 0 -4 2 -2 0.94 -0.90 1.49 < 0 -4 2 -1 50.98 50.12 0.47 o 0 -4 2 0 237.36 300.93 0.98 o 0 -4 2 1 33.57 33.97 0.75 o 0 -4 2 2 2.24 2.74 0.87 o 2 -4 2 -2 1.96 2.36 0.76 o 2 -4 2 -1 8.27 7.87 0.48 o 2 -4 2 0 20.08 21.22 0.81 o 2 -4 2 1 3.86 4.17 0.78 o 2 -4 2 2 0.56 0.28 0.68 < 4 -4 2 -2 2.16 2.60 0.76 o 4 -4 2 -1 23.01 23.53 0.79 o 4 -4 2 0 38.79 38.61 1.23 o 4 -4 2 1 14.98 12.67 1.01 o 4 -4 2 2 0.06 0.42 1.03 < 6 -4 2 -2 3.78 3.61 1.06 o 6 -4 2 -1 27.24 24.49 1.48 o 6 -4 2 0 410.95 395.55 3.06 o 6 -4 2 1 43.44 43.37 1.73 o 6 -4 2 2 0.15 0.03 1.71 < 8 -4 2 -2 11.22 12.46 1.74 o 8 -4 2 -1 67.45 65.55 2.24 o 8 -4 2 0 124.52 119.06 2.76 o 8 -4 2 1 0.08 1.62 2.21 < 10 -4 2 -2 11.84 13.41 2.77 o -11 -3 2 1 2.34 2.33 2.80 < -11 -3 2 2 2.54 1.79 2.38 < -9 -3 2 -2 2.00 1.93 2.18 < -9 -3 2 -1 162.58 162.01 2.90 o -9 -3 2 0 1345.93 1347.31 6.92 o -9 -3 2 1 40.87 38.54 2.30 o -9 -3 2 2 1.82 1.84 1.98 < -7 -3 2 -2 0.12 0.47 1.90 < -7 -3 2 -1 160.43 160.83 2.38 o -7 -3 2 0 161.20 165.88 2.60 o -7 -3 2 1 29.46 26.44 1.93 o -7 -3 2 2 4.13 3.98 1.40 < -5 -3 2 -2 0.53 1.35 2.02 < -5 -3 2 -1 156.49 157.28 2.41 o -5 -3 2 0 1780.57 1705.82 5.27 o -5 -3 2 1 242.32 228.20 1.89 o -5 -3 2 2 5.47 5.31 0.82 o -3 -3 2 -2 3.85 3.11 1.38 < -3 -3 2 -1 395.85 382.16 2.16 o -3 -3 2 0 3647.25 3233.75 4.84 o -3 -3 2 1 50.09 51.58 1.46 o -3 -3 2 2 5.12 3.72 0.40 o -1 -3 2 -2 5.94 6.33 0.64 o -1 -3 2 -1 19.51 19.17 0.44 o -1 -3 2 0 3033.17 3062.55 2.40 o -1 -3 2 1 69.70 67.84 0.47 o -1 -3 2 2 0.85 0.67 0.48 < 1 -3 2 -2 0.26 -0.37 0.26 < 1 -3 2 -1 67.01 66.04 0.36 o 1 -3 2 0 12607.30 12003.00 5.90 o 1 -3 2 1 37.41 37.38 0.56 o 1 -3 2 2 0.77 1.28 0.62 < 3 -3 2 -2 2.36 1.96 0.56 o 3 -3 2 -1 24.12 26.47 0.61 o 3 -3 2 0 7.88 8.00 1.15 o 3 -3 2 1 59.84 58.34 0.86 o 3 -3 2 2 3.93 3.63 1.09 o 5 -3 2 -2 0.56 1.31 0.89 < 5 -3 2 -1 9.52 8.25 0.93 o 5 -3 2 0 3152.23 2970.60 7.81 o 5 -3 2 1 32.95 31.84 1.65 o 5 -3 2 2 0.24 0.90 1.38 < 7 -3 2 -2 1.10 1.93 1.38 < 7 -3 2 -1 0.44 0.58 1.49 < 7 -3 2 0 229.08 229.07 3.61 o 7 -3 2 1 35.58 33.98 2.29 o 7 -3 2 2 0.00 0.14 1.96 < 9 -3 2 -2 1.59 1.57 1.94 < 9 -3 2 -1 0.01 -0.79 2.10 < 9 -3 2 0 206.43 198.18 3.44 o -10 -2 2 -1 4.79 3.75 2.97 < -10 -2 2 0 23.71 29.30 2.72 o -10 -2 2 1 187.37 200.23 3.49 o -10 -2 2 2 15.62 15.23 2.12 o -8 -2 2 -2 5.28 5.71 1.70 o -8 -2 2 -1 9.63 9.80 1.73 o -8 -2 2 0 62.51 67.25 2.23 o -8 -2 2 1 22.04 24.13 1.91 o -8 -2 2 2 8.44 8.74 1.63 o -6 -2 2 -2 18.99 19.26 1.43 o -6 -2 2 -1 38.59 39.45 1.26 o -6 -2 2 0 663.53 700.28 4.00 o -6 -2 2 1 212.40 218.53 2.42 o -6 -2 2 2 11.39 9.93 1.48 o -4 -2 2 -2 0.30 0.89 1.26 < -4 -2 2 -1 85.66 92.20 2.02 o -4 -2 2 0 1324.50 1293.98 5.47 o -4 -2 2 2 0.13 -0.02 0.58 < -2 -2 2 -2 2.55 1.84 0.62 < -2 -2 2 -1 68.40 61.31 0.79 o -2 -2 2 0 4725.89 4649.05 5.61 o -2 -2 2 1 16.74 16.85 0.37 o -2 -2 2 2 0.27 -0.20 0.51 < 0 -2 2 -2 0.00 0.00 0.25 < 0 -2 2 -1 1.41 1.91 0.19 o 0 -2 2 0 455.49 449.16 0.70 o 0 -2 2 1 5.39 5.24 0.28 o 0 -2 2 2 0.88 1.31 0.42 o 2 -2 2 -2 1.91 1.91 0.25 o 2 -2 2 -1 42.76 42.99 0.44 o 2 -2 2 0 938.16 886.41 1.76 o 2 -2 2 1 10.76 10.41 0.72 o 2 -2 2 2 0.06 -0.37 0.81 < 4 -2 2 -2 0.02 -0.02 0.47 < 4 -2 2 -1 17.41 15.96 0.81 o 4 -2 2 0 1103.96 1107.12 4.55 o 4 -2 2 1 5.75 6.69 1.32 o 4 -2 2 2 0.18 0.02 1.51 < 6 -2 2 -2 21.10 20.51 0.76 o 6 -2 2 -1 276.38 279.48 2.56 o 6 -2 2 0 109.54 111.42 2.57 o 6 -2 2 1 63.89 64.88 2.47 o 6 -2 2 2 1.59 -0.17 2.27 < 8 -2 2 -2 3.21 4.92 2.05 < 8 -2 2 -1 11.69 12.59 2.32 o 8 -2 2 0 1169.84 1139.20 7.11 o 8 -2 2 1 1.82 1.57 2.52 < 8 -2 2 2 1.30 1.57 3.34 < 10 -2 2 -2 4.93 5.76 2.60 < 10 -2 2 -1 118.90 112.26 3.63 o -11 -1 2 0 317.65 315.09 8.79 o -11 -1 2 1 42.34 42.95 2.82 o -11 -1 2 2 0.41 1.07 2.21 < -9 -1 2 -2 2.08 2.47 2.74 < -9 -1 2 -1 47.07 47.85 2.55 o -9 -1 2 0 34.90 49.86 2.35 o -9 -1 2 1 91.95 99.88 2.58 o -9 -1 2 2 24.17 27.79 1.79 o -7 -1 2 -2 5.53 6.44 1.42 o -7 -1 2 -1 53.14 58.64 1.93 o -7 -1 2 0 666.73 695.02 4.22 o -7 -1 2 1 284.83 296.84 2.82 o -7 -1 2 2 2.97 4.17 1.17 o -5 -1 2 -2 6.25 5.59 1.09 o -5 -1 2 -1 4.86 6.99 0.96 o -5 -1 2 0 1317.15 1370.29 4.83 o -5 -1 2 1 76.70 80.21 1.28 o -5 -1 2 2 16.88 17.63 0.98 o -3 -1 2 -2 21.39 23.22 0.87 o -3 -1 2 -1 63.10 56.33 1.49 o -3 -1 2 0 602.94 510.96 2.93 o -3 -1 2 1 448.58 462.60 2.75 o -3 -1 2 2 8.40 6.86 0.95 o -1 -1 2 -2 0.42 0.62 0.36 < -1 -1 2 -1 38.26 39.76 0.39 o -1 -1 2 0 1875.13 1623.75 1.62 o -1 -1 2 1 23.03 21.04 0.48 o -1 -1 2 2 0.08 -0.22 0.51 < 1 -1 2 -2 1.42 1.07 0.12 o 1 -1 2 -1 8.72 8.29 0.19 o 1 -1 2 0 7.24 11.53 0.33 o 1 -1 2 1 0.00 -0.17 0.70 < 1 -1 2 2 0.39 1.03 0.95 < 3 -1 2 -2 0.13 -0.54 0.59 < 3 -1 2 -1 31.28 31.48 0.70 o 3 -1 2 0 1883.81 2070.32 6.60 o 3 -1 2 1 14.42 14.36 1.17 o 3 -1 2 2 0.20 0.96 1.23 < 5 -1 2 -2 2.75 2.55 0.68 o 5 -1 2 -1 1.73 1.28 0.98 < 5 -1 2 0 0.41 2.05 1.09 < 5 -1 2 1 29.91 31.88 1.43 o 5 -1 2 2 0.65 1.87 1.76 < 7 -1 2 -2 0.25 -1.32 1.57 < 7 -1 2 -1 28.77 30.41 2.09 o 7 -1 2 0 15.06 21.10 2.71 o 7 -1 2 1 33.15 31.60 3.10 o 7 -1 2 2 0.93 0.26 2.63 < 9 -1 2 -2 12.84 11.03 2.30 o 9 -1 2 -1 56.66 59.84 3.03 o 9 -1 2 0 6.35 6.95 2.86 < -10 0 2 -1 86.55 89.36 4.42 o -10 0 2 0 69.71 76.90 2.79 o -10 0 2 1 0.03 -1.35 2.02 < -10 0 2 2 10.67 9.16 2.08 o -8 0 2 -2 8.40 8.35 2.21 o -8 0 2 -1 87.72 97.30 2.86 o -8 0 2 0 576.47 634.21 4.32 o -8 0 2 1 2.11 2.69 1.43 < -8 0 2 2 2.55 1.49 1.32 < -6 0 2 -2 0.61 1.48 1.18 < -6 0 2 -1 350.92 369.04 2.95 o -6 0 2 0 364.99 373.63 2.84 o -6 0 2 1 7.59 7.53 1.06 o -6 0 2 2 0.12 0.30 1.09 < -4 0 2 -2 0.03 0.14 1.03 < -4 0 2 0 5674.74 6135.02 15.95 o -4 0 2 1 37.98 36.82 1.15 o -4 0 2 2 0.01 0.17 1.10 < -2 0 2 -2 1.44 1.85 0.61 o -2 0 2 -1 240.65 245.31 1.39 o -2 0 2 0 4727.26 5032.28 5.57 o -2 0 2 1 21.70 19.39 0.45 o -2 0 2 2 1.31 0.67 0.58 < 0 0 2 -2 3.61 3.42 0.23 o 0 0 2 -1 65.16 59.18 0.41 o 0 0 2 0 1774.91 1611.52 1.71 o 0 0 2 1 6.12 7.28 0.61 o 0 0 2 2 1.16 2.50 1.29 < 2 0 2 -2 0.15 0.26 0.31 < 2 0 2 -1 0.68 0.72 0.48 < 2 0 2 0 9866.61 10650.70 8.19 o 2 0 2 1 4.43 4.42 0.56 o 2 0 2 2 1.50 0.79 0.87 < 4 0 2 -2 5.98 5.71 1.21 o 4 0 2 -1 30.58 33.05 1.53 o 4 0 2 0 1488.87 1532.65 5.24 o 4 0 2 1 12.48 12.26 1.37 o 4 0 2 2 1.24 0.33 1.82 < 6 0 2 -2 3.87 1.35 1.49 < 6 0 2 -1 27.15 27.00 1.76 o 6 0 2 0 2440.43 2499.13 7.72 o 6 0 2 1 99.28 96.00 3.47 o 6 0 2 2 3.61 3.20 2.64 < 8 0 2 -2 1.93 1.52 1.65 < 8 0 2 -1 16.06 15.75 2.16 o 8 0 2 0 13.04 11.40 2.50 o 8 0 2 1 41.81 37.55 3.00 o 8 0 2 2 0.03 -0.16 4.78 < 10 0 2 -2 0.36 1.35 2.71 < 10 0 2 -1 6.64 4.53 2.85 < -11 1 2 0 46.40 60.77 4.45 o -11 1 2 1 80.20 85.39 3.08 o -11 1 2 2 21.46 22.89 2.58 o -9 1 2 -2 15.67 21.14 3.53 o -9 1 2 -1 5.32 6.88 2.46 < -9 1 2 0 523.59 549.76 3.82 o -9 1 2 1 95.94 104.52 2.41 o -9 1 2 2 5.71 6.83 1.70 o -7 1 2 -2 1.59 2.63 1.54 < -7 1 2 -1 0.10 0.72 1.43 < -7 1 2 0 31.92 44.21 1.46 o -7 1 2 1 238.57 249.34 2.26 o -7 1 2 2 37.11 39.03 1.49 o -5 1 2 -2 32.81 33.44 1.28 o -5 1 2 -1 57.63 57.65 1.63 o -5 1 2 0 12.19 42.10 1.46 o -5 1 2 1 40.29 45.20 1.45 o -5 1 2 2 0.12 0.62 0.68 < -3 1 2 -2 1.98 0.86 0.81 < -3 1 2 -1 40.94 42.04 0.73 o -3 1 2 0 537.30 562.97 3.24 o -3 1 2 1 266.31 260.80 1.47 o -3 1 2 2 4.03 3.08 0.65 o -1 1 2 -2 1.90 1.07 0.33 o -1 1 2 -1 121.64 117.75 0.56 o -1 1 2 0 37.74 26.29 0.83 o -1 1 2 1 0.07 0.72 0.39 < -1 1 2 2 2.10 1.07 0.58 < 1 1 2 -2 0.17 -0.19 0.30 < 1 1 2 -1 12.75 11.06 0.54 o 1 1 2 0 473.12 474.74 2.61 o 1 1 2 2 3.86 2.52 0.93 < 3 1 2 -2 0.77 1.54 0.64 < 3 1 2 -1 19.15 21.37 0.86 o 3 1 2 0 2037.62 2337.33 5.52 o 3 1 2 1 1.55 2.66 0.82 o 3 1 2 2 0.10 0.59 1.21 < 5 1 2 -2 3.06 3.77 1.23 o 5 1 2 -1 25.70 26.62 1.63 o 5 1 2 0 38.27 37.63 1.53 o 5 1 2 1 9.75 8.60 1.74 o 5 1 2 2 1.00 0.20 1.96 < 7 1 2 -2 3.20 2.66 1.65 < 7 1 2 -1 54.63 51.54 2.19 o 7 1 2 0 112.52 112.07 2.74 o 7 1 2 1 0.02 -1.94 2.99 < 7 1 2 2 0.61 -0.36 2.58 < 9 1 2 -2 14.80 16.63 1.94 o 9 1 2 -1 123.39 119.11 3.41 o 9 1 2 0 164.97 159.35 3.89 o -10 2 2 -1 141.20 144.59 3.75 o -10 2 2 0 229.26 224.39 3.52 o -10 2 2 1 136.59 139.42 2.96 o -10 2 2 2 7.35 8.43 2.13 o -8 2 2 -2 1.51 0.39 2.13 < -8 2 2 -1 71.19 78.88 2.13 o -8 2 2 0 51.01 50.48 1.90 o -8 2 2 1 35.75 37.24 1.56 o -8 2 2 2 0.11 -0.59 1.23 < -6 2 2 -2 0.84 0.84 1.24 < -6 2 2 -1 253.86 267.38 2.18 o -6 2 2 0 2413.14 2505.34 6.57 o -6 2 2 1 345.72 339.72 2.28 o -6 2 2 2 17.84 17.52 1.20 o -4 2 2 -2 2.67 2.38 1.80 < -4 2 2 -1 108.28 102.13 1.85 o -4 2 2 0 11.48 12.28 1.00 o -4 2 2 1 299.49 291.88 2.04 o -4 2 2 2 10.37 10.60 0.90 o -2 2 2 -2 20.13 17.82 0.53 o -2 2 2 -1 128.95 123.47 0.95 o -2 2 2 0 8250.40 7631.43 6.14 o -2 2 2 1 188.64 181.77 1.43 o -2 2 2 2 0.01 -0.37 0.56 < 0 2 2 -2 2.32 1.59 0.25 o 0 2 2 -1 78.55 68.38 0.48 o 0 2 2 0 2163.70 2119.74 3.75 o 0 2 2 1 222.31 216.93 2.06 o 2 2 2 -2 2.90 2.01 0.44 o 2 2 2 -1 32.73 32.34 1.35 o 2 2 2 0 1859.49 1821.22 7.49 o 2 2 2 2 1.75 1.68 1.24 < 4 2 2 -2 4.38 5.17 0.65 o 4 2 2 -1 37.84 43.84 1.40 o 4 2 2 0 887.16 992.38 3.74 o 4 2 2 1 19.33 17.88 1.52 o 4 2 2 2 0.86 0.96 2.43 < 6 2 2 -2 1.61 2.15 1.29 < 6 2 2 -1 88.42 86.21 2.01 o 6 2 2 0 8.30 8.76 1.60 o 6 2 2 1 7.74 9.26 1.82 o 6 2 2 2 0.07 1.07 2.41 < 8 2 2 -2 0.08 0.28 1.91 < 8 2 2 -1 0.73 0.58 2.08 < 8 2 2 0 849.10 818.27 7.88 o 8 2 2 1 46.81 40.93 3.77 o 10 2 2 -2 4.23 5.52 2.75 < 10 2 2 -1 44.75 42.12 6.24 o -11 3 2 1 27.07 27.76 3.14 o -11 3 2 2 23.99 24.40 2.49 o -9 3 2 -2 11.92 13.51 2.69 o -9 3 2 -1 31.74 31.49 2.26 o -9 3 2 0 772.08 761.39 4.94 o -9 3 2 1 98.59 104.57 2.16 o -9 3 2 2 12.11 12.49 1.59 o -7 3 2 -2 16.36 15.70 1.60 o -7 3 2 -1 124.56 123.90 1.87 o -7 3 2 0 5.51 5.71 1.18 o -7 3 2 1 2.88 2.19 1.17 < -7 3 2 2 2.88 2.40 1.24 < -5 3 2 -2 7.90 6.80 1.29 o -5 3 2 -1 88.92 95.04 1.59 o -5 3 2 0 507.96 506.82 2.58 o -5 3 2 1 157.57 154.35 2.01 o -5 3 2 2 10.74 11.11 1.40 o -3 3 2 -2 5.65 4.01 0.70 o -3 3 2 -1 233.59 220.24 1.56 o -3 3 2 0 1620.04 1595.09 4.41 o -3 3 2 1 1.22 1.24 0.62 < -1 3 2 -2 1.45 1.35 0.37 o -1 3 2 -1 107.33 94.07 0.59 o -1 3 2 0 1362.72 1342.64 2.80 o -1 3 2 1 0.14 0.09 0.44 < -1 3 2 2 0.04 -0.03 0.64 < 1 3 2 -2 7.67 5.99 0.42 o 1 3 2 -1 3.52 2.38 0.50 o 1 3 2 0 10822.40 11152.90 15.16 o 1 3 2 2 1.10 0.16 1.24 < 3 3 2 -2 4.15 2.85 0.68 o 3 3 2 -1 0.04 0.05 0.87 < 3 3 2 0 16.79 13.99 1.87 o 3 3 2 1 0.02 0.25 1.04 < 3 3 2 2 1.12 1.49 1.66 < 5 3 2 -2 8.18 8.60 1.07 o 5 3 2 -1 86.21 91.80 2.07 o 5 3 2 0 3627.13 3720.48 8.51 o 5 3 2 1 75.15 75.58 2.04 o 5 3 2 2 0.63 0.87 1.88 < 7 3 2 -2 9.91 10.11 1.56 o 7 3 2 -1 79.97 76.08 2.18 o 7 3 2 0 360.76 365.15 3.68 o 7 3 2 1 2.65 4.17 2.18 < 7 3 2 2 2.83 3.45 2.74 < 9 3 2 -2 8.42 8.01 1.98 o 9 3 2 -1 7.09 7.44 3.21 < 9 3 2 0 410.12 384.76 6.31 o -10 4 2 -1 13.50 15.51 2.96 o -10 4 2 0 10.21 9.52 2.77 o -10 4 2 1 76.03 82.36 2.65 o -10 4 2 2 6.57 6.50 2.10 o -8 4 2 -2 0.43 1.15 2.12 < -8 4 2 -1 4.95 5.10 1.68 o -8 4 2 0 417.11 430.61 3.57 o -8 4 2 1 58.60 64.35 1.96 o -8 4 2 2 23.04 26.44 1.71 o -6 4 2 -2 16.63 18.11 1.38 o -6 4 2 -1 8.67 8.81 1.12 o -6 4 2 0 31.22 36.38 1.42 o -6 4 2 1 404.88 424.55 2.92 o -6 4 2 2 15.94 18.48 1.21 o -4 4 2 -2 0.60 1.03 1.20 < -4 4 2 -1 13.87 14.17 1.23 o -4 4 2 0 5035.83 4954.70 17.18 o -4 4 2 1 10.73 10.86 1.24 o -4 4 2 2 2.74 2.43 0.92 < -2 4 2 -2 8.98 8.28 0.84 o -2 4 2 -1 0.10 -0.03 0.48 < -2 4 2 0 639.38 642.57 1.97 o -2 4 2 1 240.82 233.64 2.34 o 0 4 2 -2 0.14 -0.16 0.34 < 0 4 2 -1 68.12 64.21 0.79 o 0 4 2 0 1609.40 1603.33 4.10 o 0 4 2 1 40.57 39.58 1.20 o 0 4 2 2 0.86 1.66 2.07 < 2 4 2 -2 3.22 2.32 0.61 o 2 4 2 0 1.84 2.61 1.49 < 2 4 2 1 25.68 23.85 1.56 o 2 4 2 2 0.01 -0.12 1.99 < 4 4 2 -2 0.15 -0.48 0.78 < 4 4 2 -1 43.07 43.53 1.32 o 4 4 2 0 0.58 1.82 1.15 < 4 4 2 1 73.28 71.26 2.09 o 4 4 2 2 0.03 1.00 2.13 < 6 4 2 -2 2.14 1.56 1.38 < 6 4 2 -1 9.30 8.51 1.63 o 6 4 2 0 102.29 102.09 2.69 o 6 4 2 1 5.16 5.90 1.96 o 6 4 2 2 0.20 -0.53 2.15 < 8 4 2 -2 1.45 2.01 1.73 < 8 4 2 -1 29.63 27.25 2.21 o 8 4 2 0 523.81 502.13 5.15 o 8 4 2 1 12.89 14.30 3.50 o 10 4 2 -2 4.42 4.75 2.69 < -11 5 2 2 4.53 5.23 2.97 < -9 5 2 -2 0.52 0.28 2.54 < -9 5 2 -1 125.01 123.72 3.33 o -9 5 2 0 20.31 17.49 2.51 o -9 5 2 1 61.24 62.87 2.29 o -9 5 2 2 0.03 1.01 1.80 < -7 5 2 -2 1.45 0.82 1.60 < -7 5 2 -1 168.78 170.67 2.44 o -7 5 2 0 781.24 772.35 4.33 o -7 5 2 1 33.42 34.93 1.60 o -7 5 2 2 2.39 1.49 1.23 < -5 5 2 -2 0.06 -0.70 1.14 < -5 5 2 -1 139.73 138.63 1.92 o -5 5 2 0 937.29 949.14 4.07 o -5 5 2 1 114.75 112.79 1.84 o -5 5 2 2 2.58 1.79 0.78 < -3 5 2 -2 9.60 10.24 0.96 o -3 5 2 -1 567.10 545.28 2.83 o -3 5 2 0 1748.19 1680.21 4.23 o -3 5 2 2 0.11 0.65 1.80 < -1 5 2 -2 1.03 1.28 0.53 < -1 5 2 -1 2.75 2.85 0.68 o -1 5 2 0 3753.93 3539.94 10.46 o -1 5 2 1 16.14 19.11 0.93 o -1 5 2 2 0.50 0.96 1.00 < 1 5 2 -2 5.35 4.64 0.47 o 1 5 2 -1 99.49 102.16 1.43 o 1 5 2 0 364.17 433.71 2.82 o 1 5 2 1 132.74 130.61 2.71 o 1 5 2 2 0.24 0.40 1.80 < 3 5 2 -2 0.57 3.08 2.27 < 3 5 2 -1 0.01 0.25 1.29 < 3 5 2 0 5075.15 5143.78 10.44 o 3 5 2 1 7.62 7.55 1.57 o 3 5 2 2 4.03 2.22 1.63 < 5 5 2 -2 0.79 -0.12 1.04 < 5 5 2 -1 0.13 -0.73 1.10 < 5 5 2 0 380.15 423.05 3.46 o 5 5 2 1 2.74 2.36 2.21 < 5 5 2 2 1.40 0.95 2.54 < 7 5 2 -2 2.38 2.88 1.43 < 7 5 2 -1 0.57 1.99 2.55 < 7 5 2 0 386.44 365.03 3.90 o 7 5 2 1 96.65 85.78 2.82 o 9 5 2 -2 1.10 0.75 2.38 < 9 5 2 -1 1.12 2.26 2.66 < -10 6 2 0 0.78 0.67 2.85 < -10 6 2 1 55.81 58.98 3.17 o -10 6 2 2 19.05 16.94 3.21 o -8 6 2 -2 21.01 19.43 2.41 o -8 6 2 -1 5.52 5.04 2.27 < -8 6 2 0 5.54 6.67 2.12 o -8 6 2 1 228.26 240.44 2.79 o -8 6 2 2 13.64 13.58 1.63 o -6 6 2 -2 5.38 6.92 1.48 o -6 6 2 -1 155.53 155.10 2.26 o -6 6 2 0 52.65 55.09 2.44 o -6 6 2 1 7.08 8.12 1.06 o -6 6 2 2 2.25 1.59 1.10 < -4 6 2 -2 21.84 21.92 1.57 o -4 6 2 -1 5.87 8.07 1.26 o -4 6 2 0 787.17 768.58 3.85 o -4 6 2 1 224.30 209.98 2.13 o -4 6 2 2 5.67 4.45 1.43 o -2 6 2 -2 9.46 8.22 0.79 o -2 6 2 -1 148.40 149.06 1.22 o -2 6 2 0 15.17 10.91 1.29 o -2 6 2 1 3.74 2.88 1.31 < -2 6 2 2 0.21 -0.61 1.62 < 0 6 2 -2 0.22 -0.11 0.65 < 0 6 2 -1 43.95 44.03 1.01 o 0 6 2 0 97.88 109.72 1.32 o 0 6 2 1 54.13 53.48 1.37 o 0 6 2 2 0.42 0.86 1.17 < 2 6 2 -2 7.79 7.02 0.82 o 2 6 2 -1 19.75 17.83 1.68 o 2 6 2 0 1376.25 1336.97 7.40 o 2 6 2 1 7.70 6.72 1.74 o 2 6 2 2 0.12 -1.84 1.60 < 4 6 2 -2 3.93 4.33 1.12 o 4 6 2 -1 1.16 1.56 1.40 < 4 6 2 0 251.33 258.52 2.87 o 4 6 2 1 0.54 1.31 1.62 < 4 6 2 2 0.01 -0.86 2.01 < 6 6 2 -2 5.64 4.65 1.57 < 6 6 2 -1 53.10 50.75 2.04 o 6 6 2 0 1026.91 1003.74 5.71 o 6 6 2 1 27.16 27.25 2.82 o 6 6 2 2 4.08 3.52 2.91 < 8 6 2 -2 8.16 8.43 2.43 o 8 6 2 -1 43.83 38.89 2.49 o 8 6 2 0 5.42 3.42 2.41 < 10 6 2 -2 6.59 4.75 2.83 < -9 7 2 -1 11.32 13.38 2.79 o -9 7 2 0 370.13 354.30 4.27 o -9 7 2 1 15.48 15.57 2.97 o -9 7 2 2 0.37 1.09 2.82 < -7 7 2 -2 0.28 -0.42 2.07 < -7 7 2 -1 74.01 80.28 2.68 o -7 7 2 0 188.85 181.43 2.90 o -7 7 2 1 199.52 199.48 2.94 o -7 7 2 2 22.61 23.59 2.41 o -5 7 2 -2 8.71 10.18 1.48 o -5 7 2 -1 63.73 64.90 1.56 o -5 7 2 0 182.15 188.97 2.54 o -5 7 2 1 45.31 46.51 1.37 o -5 7 2 2 5.34 6.10 1.62 o -3 7 2 -2 1.20 0.79 0.78 < -3 7 2 -1 9.61 8.81 0.90 o -3 7 2 0 1101.12 1069.77 5.11 o -3 7 2 1 155.72 153.35 3.99 o -3 7 2 2 7.17 10.24 2.82 o -1 7 2 -2 4.05 3.80 1.80 < -1 7 2 -1 60.02 59.89 1.60 o -1 7 2 0 447.88 462.31 2.64 o -1 7 2 1 111.16 105.59 1.71 o -1 7 2 2 2.30 3.59 1.57 < 1 7 2 -2 1.61 2.08 0.89 < 1 7 2 -1 6.86 6.94 1.34 o 1 7 2 0 1619.35 1576.24 6.50 o 1 7 2 1 8.31 8.96 2.13 o 1 7 2 2 0.77 0.70 2.29 < 3 7 2 -2 1.47 1.85 1.73 < 3 7 2 -1 3.17 4.93 1.59 o 3 7 2 0 11.53 11.84 1.42 o 3 7 2 1 8.85 10.27 1.45 o 3 7 2 2 0.05 -0.93 1.85 < 5 7 2 -2 0.14 -0.42 1.28 < 5 7 2 -1 0.03 0.50 1.42 < 5 7 2 0 132.77 138.80 2.69 o 5 7 2 1 54.57 52.15 2.88 o 5 7 2 2 0.09 -2.04 3.45 < 7 7 2 -2 1.21 1.79 1.63 < 7 7 2 -1 3.10 2.86 2.08 < 7 7 2 0 80.50 76.76 3.32 o 7 7 2 1 2.29 2.50 3.86 < 9 7 2 -2 5.01 4.81 2.68 < -8 8 2 -2 1.60 2.58 2.02 < -8 8 2 -1 119.61 116.77 3.10 o -8 8 2 0 35.31 37.58 3.33 o -8 8 2 1 2.22 2.61 2.77 < -8 8 2 2 7.21 7.75 2.72 < -6 8 2 -2 6.57 6.61 1.76 o -6 8 2 -1 73.40 73.57 2.30 o -6 8 2 0 703.51 709.64 4.81 o -6 8 2 1 0.02 -0.26 1.60 < -6 8 2 2 4.87 1.76 3.00 < -4 8 2 -2 1.23 0.67 1.42 < -4 8 2 -1 191.67 186.67 2.51 o -4 8 2 0 23.71 24.79 1.85 o -4 8 2 1 60.16 60.71 3.63 o -4 8 2 2 0.00 0.14 3.11 < -2 8 2 -2 0.60 0.39 1.42 < -2 8 2 -1 75.37 74.26 2.01 o -2 8 2 0 1685.36 1776.79 7.12 o -2 8 2 1 0.09 0.47 1.42 < -2 8 2 2 1.36 1.51 1.34 < 0 8 2 -2 2.09 2.46 1.17 < 0 8 2 -1 47.60 45.99 1.37 o 0 8 2 0 1551.55 1536.12 5.40 o 0 8 2 1 133.38 133.05 2.09 o 0 8 2 2 0.38 0.03 2.19 < 2 8 2 -2 1.10 0.92 1.14 < 2 8 2 -1 65.81 62.60 2.43 o 2 8 2 0 975.60 993.91 7.12 o 2 8 2 1 2.06 1.87 1.93 < 2 8 2 2 2.18 1.79 1.70 < 4 8 2 -2 10.79 11.79 1.28 o 4 8 2 -1 84.24 86.51 1.88 o 4 8 2 0 1050.87 1076.05 4.93 o 4 8 2 1 8.64 9.37 2.13 o 4 8 2 2 4.91 4.37 2.38 < 6 8 2 -2 0.10 -0.84 1.80 < 6 8 2 -1 19.93 17.88 2.13 o 6 8 2 0 278.05 290.49 3.82 o 6 8 2 1 5.50 3.73 3.05 < 8 8 2 -2 7.59 6.29 2.64 < 8 8 2 -1 59.42 53.85 4.00 o -9 9 2 2 10.63 7.97 3.21 < -7 9 2 -2 11.84 12.56 2.40 o -7 9 2 -1 9.59 8.54 2.26 o -7 9 2 0 74.46 71.78 3.36 o -7 9 2 1 7.71 7.36 2.64 < -7 9 2 2 6.98 5.32 3.77 < -5 9 2 -2 3.60 2.33 1.74 < -5 9 2 -1 3.54 4.54 1.71 < -5 9 2 0 93.55 93.49 2.76 o -5 9 2 1 361.13 353.48 6.72 o -5 9 2 2 6.71 7.76 3.75 < -3 9 2 -2 11.54 11.84 1.31 o -3 9 2 -1 0.38 1.10 1.87 < -3 9 2 0 2.47 3.14 2.82 < -3 9 2 1 8.21 6.29 2.15 < -3 9 2 2 0.38 0.30 1.76 < -1 9 2 -2 0.25 -3.17 1.70 < -1 9 2 -1 83.10 85.83 2.01 o -1 9 2 0 108.95 107.51 1.98 o -1 9 2 1 5.82 4.65 1.46 o -1 9 2 2 0.63 0.05 1.96 < 1 9 2 -2 4.00 3.06 1.23 < 1 9 2 -1 3.65 2.80 1.29 < 1 9 2 0 536.24 522.60 4.07 o 1 9 2 1 64.50 62.18 3.05 o 1 9 2 2 0.43 0.81 2.77 < 3 9 2 -2 0.00 -0.64 2.01 < 3 9 2 -1 37.49 41.07 1.71 o 3 9 2 0 230.35 251.37 2.82 o 3 9 2 1 34.27 35.77 2.02 o 3 9 2 2 0.19 0.25 2.30 < 5 9 2 -2 0.25 -0.50 1.56 < 5 9 2 -1 41.36 38.67 2.29 o 5 9 2 0 387.26 393.14 4.15 o 5 9 2 1 23.15 21.92 3.11 o 7 9 2 -2 9.30 7.28 1.99 o 7 9 2 -1 33.84 28.34 2.97 o -8 10 2 0 221.82 213.95 6.54 o -8 10 2 1 25.34 24.30 3.25 o -8 10 2 2 2.37 2.16 4.36 < -6 10 2 -2 0.61 0.36 2.12 < -6 10 2 -1 96.99 99.92 2.76 o -6 10 2 0 3.39 2.27 2.58 < -6 10 2 1 163.43 170.70 6.13 o -6 10 2 2 2.99 5.43 3.95 < -4 10 2 -2 0.64 0.84 1.51 < -4 10 2 -1 26.11 26.84 2.32 o -4 10 2 0 1890.58 1898.28 15.21 o -4 10 2 1 0.82 -0.06 2.47 < -4 10 2 2 0.98 -0.11 2.08 < -2 10 2 -2 0.31 0.00 2.01 < -2 10 2 -1 113.33 118.84 3.07 o -2 10 2 0 20.04 21.50 1.85 o -2 10 2 1 293.07 304.64 3.15 o -2 10 2 2 1.99 4.43 1.80 < 0 10 2 -2 0.03 0.58 1.31 < 0 10 2 -1 0.75 1.49 1.46 < 0 10 2 0 1341.56 1323.94 5.72 o 0 10 2 1 20.87 18.31 2.66 o 0 10 2 2 0.07 0.28 2.83 < 2 10 2 -2 5.00 5.15 1.57 o 2 10 2 -1 5.95 3.13 2.41 < 2 10 2 0 305.83 312.51 4.07 o 2 10 2 1 87.36 89.48 2.37 o 2 10 2 2 0.34 0.73 2.15 < 4 10 2 -2 0.21 -0.44 1.60 < 4 10 2 -1 55.57 62.31 2.15 o 4 10 2 0 431.61 427.94 4.32 o 4 10 2 1 6.73 3.11 2.52 < 6 10 2 -2 5.63 7.03 2.57 < 6 10 2 -1 20.17 20.66 2.89 o -7 11 2 0 99.67 90.59 5.48 o -5 11 2 -2 6.68 7.09 2.69 < -5 11 2 -1 31.74 32.89 4.70 o -5 11 2 0 44.69 52.15 3.44 o -5 11 2 1 4.46 4.47 3.00 < -5 11 2 2 2.87 3.72 2.32 < -3 11 2 -2 0.05 0.45 2.50 < -3 11 2 -1 174.60 170.14 5.25 o -3 11 2 0 183.06 184.96 3.22 o -3 11 2 1 0.58 -0.14 1.85 < -3 11 2 2 1.29 -0.12 1.94 < -1 11 2 -2 8.60 12.84 3.08 o -1 11 2 -1 0.28 0.20 1.57 < -1 11 2 0 496.69 508.08 3.98 o -1 11 2 1 18.48 22.28 2.47 o -1 11 2 2 1.93 2.01 2.99 < 1 11 2 -2 1.17 0.72 1.82 < 1 11 2 -1 85.71 84.58 2.46 o 1 11 2 0 14.44 14.97 2.99 o 1 11 2 1 54.56 49.52 3.49 o 1 11 2 2 0.08 0.47 2.13 < 3 11 2 -2 2.70 3.80 1.74 < 3 11 2 -1 14.68 15.64 1.82 o 3 11 2 0 1454.29 1485.09 6.47 o 3 11 2 1 19.62 20.13 3.03 o 5 11 2 -2 2.78 3.67 2.26 < 5 11 2 -1 0.75 0.20 3.30 < 5 11 2 0 134.91 132.99 4.86 o 7 11 2 -2 2.49 3.24 4.54 < -4 12 2 -2 6.46 7.97 3.13 < -4 12 2 -1 22.71 21.61 3.08 o -4 12 2 0 0.88 0.67 2.43 < -4 12 2 1 209.74 210.91 3.86 o -4 12 2 2 3.86 2.27 2.77 < -2 12 2 -2 0.90 0.82 2.16 < -2 12 2 -1 20.92 23.01 1.99 o -2 12 2 0 338.72 331.55 3.60 o -2 12 2 1 1.68 0.56 2.58 < -2 12 2 2 1.62 1.15 2.68 < 0 12 2 -2 0.23 -0.39 1.79 < 0 12 2 -1 0.32 0.96 1.84 < 0 12 2 0 86.56 91.97 3.66 o 0 12 2 1 91.81 87.44 4.00 o 0 12 2 2 0.49 0.93 3.50 < 2 12 2 -2 1.33 2.24 2.40 < 2 12 2 -1 8.84 6.86 2.27 o 2 12 2 0 18.10 16.10 2.22 o 2 12 2 1 7.95 6.08 3.10 < 4 12 2 -2 1.04 2.33 2.32 < 4 12 2 -1 18.54 20.69 2.60 o 6 12 2 -2 0.18 -0.82 4.85 < -3 13 2 -2 4.71 6.61 3.22 < -3 13 2 -1 2.44 3.05 4.08 < -3 13 2 0 268.77 268.66 5.19 o -1 13 2 -2 1.68 2.83 2.85 < -1 13 2 -1 106.47 108.39 4.00 o -1 13 2 0 322.64 325.23 8.56 o 1 13 2 -2 2.20 3.36 2.97 < 1 13 2 -1 0.95 1.34 3.53 < 1 13 2 0 707.38 758.00 11.85 o 3 13 2 -2 1.45 1.98 2.71 < 3 13 2 -1 6.80 8.07 5.24 < -2 14 2 -2 0.31 -1.42 4.31 < -2 14 2 -1 7.73 8.88 4.92 < 0 14 2 -2 4.22 4.81 3.33 < -1 -13 3 -1 15.79 17.41 5.13 o -1 -13 3 1 17.73 16.94 4.99 o 1 -13 3 -1 5.39 4.76 5.01 < -4 -12 3 -1 0.01 0.37 2.57 < -4 -12 3 0 0.47 2.22 3.00 < -4 -12 3 1 8.52 11.48 4.78 < -2 -12 3 -2 5.84 5.15 2.38 < -2 -12 3 -1 3.86 5.07 2.58 < -2 -12 3 0 51.57 49.30 2.96 o -2 -12 3 1 13.34 14.07 3.24 o -2 -12 3 2 0.12 1.24 3.03 < 0 -12 3 -2 0.26 -0.48 2.60 < 0 -12 3 -1 15.96 20.06 2.66 o 0 -12 3 0 62.93 60.76 3.50 o 0 -12 3 1 2.91 2.58 4.42 < 0 -12 3 2 1.30 1.01 4.34 < 2 -12 3 -2 0.97 1.17 3.14 < 2 -12 3 -1 20.31 19.43 3.22 o 2 -12 3 0 9.05 10.24 3.22 o 2 -12 3 1 4.76 6.41 4.89 < 4 -12 3 -2 0.63 0.87 4.75 < -5 -11 3 -1 5.90 5.40 2.05 < -5 -11 3 0 107.74 92.76 2.44 o -5 -11 3 1 7.82 6.05 1.91 o -5 -11 3 2 0.90 1.12 2.47 < -3 -11 3 -2 0.25 -0.61 1.71 < -3 -11 3 -1 133.73 118.40 2.09 o -3 -11 3 0 873.49 825.22 4.67 o -3 -11 3 1 44.13 44.80 2.69 o -3 -11 3 2 3.47 1.90 2.78 < -1 -11 3 -2 1.06 1.84 1.90 < -1 -11 3 -1 17.10 17.30 2.49 o -1 -11 3 0 59.11 54.17 2.63 o -1 -11 3 1 33.88 37.21 3.00 o -1 -11 3 2 0.06 -0.23 2.69 < 1 -11 3 -2 1.15 1.96 1.93 < 1 -11 3 -1 10.10 9.09 2.35 o 1 -11 3 0 1464.30 1430.00 7.65 o 1 -11 3 1 20.34 20.13 3.02 o 1 -11 3 2 2.72 3.58 2.97 < 3 -11 3 -2 1.08 1.09 2.33 < 3 -11 3 -1 20.76 21.07 3.11 o 3 -11 3 0 91.27 85.76 3.00 o 3 -11 3 1 44.68 53.22 3.53 o 5 -11 3 -2 0.00 -0.42 2.47 < -6 -10 3 -1 33.82 31.25 2.21 o -6 -10 3 0 357.92 330.54 3.52 o -6 -10 3 1 3.00 3.78 1.71 < -6 -10 3 2 0.40 1.37 1.85 < -4 -10 3 -2 1.90 -0.12 2.07 < -4 -10 3 -1 8.07 9.57 1.71 o -4 -10 3 0 29.09 26.87 1.70 o -4 -10 3 1 62.03 53.29 1.88 o -4 -10 3 2 2.10 3.06 1.79 < -2 -10 3 -2 2.41 2.78 1.56 < -2 -10 3 -1 3.59 3.06 1.31 < -2 -10 3 0 162.46 159.10 1.90 o -2 -10 3 1 15.42 16.85 1.73 o -2 -10 3 2 2.78 4.71 2.54 < 0 -10 3 -2 0.02 -0.47 1.38 < 0 -10 3 -1 33.36 35.34 1.91 o 0 -10 3 0 620.77 648.23 5.10 o 0 -10 3 1 6.39 5.76 2.05 < 0 -10 3 2 0.02 0.12 2.57 < 2 -10 3 -2 0.20 -0.16 1.71 < 2 -10 3 -1 111.54 110.26 2.80 o 2 -10 3 0 36.76 38.34 2.47 o 2 -10 3 1 1.15 1.45 2.19 < 2 -10 3 2 0.06 2.58 3.75 < 4 -10 3 -2 0.23 0.08 1.76 < 4 -10 3 -1 7.93 7.36 2.83 < 4 -10 3 0 783.78 808.69 7.28 o 4 -10 3 1 10.14 8.64 2.88 < 4 -10 3 2 0.10 -1.00 4.43 < 6 -10 3 -2 0.93 -0.64 2.26 < 6 -10 3 -1 101.94 98.35 3.89 o -7 -9 3 -1 5.08 5.76 3.49 < -7 -9 3 0 68.27 59.37 2.69 o -7 -9 3 1 171.04 154.03 3.15 o -7 -9 3 2 6.96 6.16 1.88 o -5 -9 3 -2 1.16 2.13 2.10 < -5 -9 3 -1 68.78 66.21 2.10 o -5 -9 3 0 787.37 704.71 4.28 o -5 -9 3 1 13.91 14.77 1.40 o -5 -9 3 2 0.09 1.24 1.28 < -3 -9 3 -2 17.35 16.35 1.56 o -3 -9 3 -1 46.88 45.36 2.01 o -3 -9 3 0 36.39 34.27 1.29 o -3 -9 3 1 5.80 5.09 1.31 o -3 -9 3 2 0.02 -0.25 1.54 < -1 -9 3 -2 1.32 0.67 1.37 < -1 -9 3 -1 44.01 44.19 1.31 o -1 -9 3 0 1464.51 1432.77 5.46 o -1 -9 3 1 73.98 76.72 2.35 o -1 -9 3 2 0.43 -2.83 3.31 < 1 -9 3 -2 1.56 1.56 1.23 < 1 -9 3 -1 36.74 35.91 1.82 o 1 -9 3 0 63.71 72.35 2.29 o 1 -9 3 1 36.34 36.97 1.81 o 1 -9 3 2 4.30 4.15 1.88 < 3 -9 3 -2 2.31 2.78 1.40 < 3 -9 3 -1 7.02 8.29 1.77 o 3 -9 3 0 462.28 470.52 4.32 o 3 -9 3 1 1.60 2.80 2.49 < 3 -9 3 2 0.01 -0.09 2.57 < 5 -9 3 -2 2.78 2.75 1.51 < 5 -9 3 -1 14.54 14.98 1.82 o 5 -9 3 0 25.08 25.67 2.05 o 5 -9 3 1 23.18 20.24 2.05 o 7 -9 3 -2 1.41 1.93 2.05 < 7 -9 3 -1 7.04 7.48 3.10 < -8 -8 3 0 345.46 311.75 4.80 o -8 -8 3 1 24.52 22.84 2.49 o -8 -8 3 2 0.05 -0.23 1.93 < -6 -8 3 -2 0.06 -0.44 2.49 < -6 -8 3 -1 16.97 14.58 1.88 o -6 -8 3 0 2.41 1.17 1.66 < -6 -8 3 1 41.69 37.52 1.88 o -6 -8 3 2 0.01 -0.53 1.29 < -4 -8 3 -2 0.18 0.34 1.80 < -4 -8 3 -1 187.66 180.48 2.45 o -4 -8 3 0 1339.84 1248.55 4.48 o -4 -8 3 1 106.13 98.66 1.28 o -4 -8 3 2 11.24 12.38 0.95 o -2 -8 3 -2 0.69 0.75 1.10 < -2 -8 3 -1 6.50 5.59 1.04 o -2 -8 3 0 681.55 639.87 2.41 o -2 -8 3 1 13.69 13.58 0.81 o -2 -8 3 2 0.55 0.33 1.01 < 0 -8 3 -2 0.37 0.30 0.96 < 0 -8 3 -1 0.09 0.26 0.84 < 0 -8 3 0 635.38 650.44 2.97 o 0 -8 3 1 33.52 30.31 1.88 o 0 -8 3 2 3.04 3.49 1.74 < 2 -8 3 -2 0.47 1.07 1.10 < 2 -8 3 -1 42.14 44.72 1.46 o 2 -8 3 0 955.70 948.13 4.57 o 2 -8 3 1 1.80 1.03 1.74 < 2 -8 3 2 0.13 0.50 1.65 < 4 -8 3 -2 0.16 -1.59 1.23 < 4 -8 3 -1 75.45 76.40 1.74 o 4 -8 3 0 387.07 382.30 3.35 o 4 -8 3 1 33.21 32.86 1.82 o 4 -8 3 2 0.01 -0.05 1.79 < 6 -8 3 -2 2.50 2.32 1.68 < 6 -8 3 -1 0.25 -0.48 1.77 < 6 -8 3 0 792.45 761.32 4.94 o 6 -8 3 1 3.41 1.20 2.86 < 8 -8 3 -2 0.32 -0.25 2.10 < -9 -7 3 1 170.89 165.73 3.57 o -9 -7 3 2 15.81 14.78 2.46 o -7 -7 3 -2 1.66 2.91 2.30 < -7 -7 3 -1 1.28 1.93 2.08 < -7 -7 3 0 28.92 23.00 2.51 o -7 -7 3 1 23.69 20.51 2.10 o -7 -7 3 2 4.16 3.47 1.66 < -5 -7 3 -2 4.25 3.06 1.85 < -5 -7 3 -1 10.92 9.41 1.80 o -5 -7 3 0 0.06 -0.98 1.48 < -5 -7 3 1 115.37 109.78 1.60 o -5 -7 3 2 6.95 6.77 0.95 o -3 -7 3 -2 0.51 0.02 1.18 < -3 -7 3 -1 8.50 7.36 1.09 o -3 -7 3 0 1.15 1.24 0.78 < -3 -7 3 1 62.48 59.13 1.03 o -3 -7 3 2 0.38 0.95 0.78 < -1 -7 3 -2 0.23 -0.16 0.92 < -1 -7 3 -1 25.39 26.03 0.98 o -1 -7 3 0 127.38 131.74 1.51 o -1 -7 3 1 2.12 1.88 0.93 < -1 -7 3 2 0.45 1.62 1.38 < 1 -7 3 -2 0.00 -0.62 1.04 < 1 -7 3 -1 18.04 19.20 1.04 o 1 -7 3 0 38.43 44.75 1.54 o 1 -7 3 1 17.91 17.10 1.59 o 1 -7 3 2 0.55 1.01 1.51 < 3 -7 3 -2 0.00 -0.36 0.96 < 3 -7 3 -1 7.26 7.76 0.92 o 3 -7 3 0 302.12 304.67 2.43 o 3 -7 3 1 14.20 13.16 1.29 o 3 -7 3 2 0.53 -0.28 1.49 < 5 -7 3 -2 0.47 1.01 1.14 < 5 -7 3 -1 25.42 22.94 1.70 o 5 -7 3 0 205.00 204.27 2.43 o 5 -7 3 1 6.33 4.43 1.59 < 5 -7 3 2 2.95 6.38 2.71 < 7 -7 3 -2 3.85 3.42 1.85 < 7 -7 3 -1 106.23 102.77 2.29 o 7 -7 3 0 57.32 54.33 2.38 o -10 -6 3 2 0.27 -0.02 2.52 < -8 -6 3 -2 0.24 0.40 2.47 < -8 -6 3 -1 22.99 21.36 2.43 o -8 -6 3 0 55.72 44.60 2.51 o -8 -6 3 1 9.77 8.82 2.47 o -8 -6 3 2 1.60 1.49 1.99 < -6 -6 3 -2 8.43 7.20 2.26 o -6 -6 3 -1 60.59 54.70 2.15 o -6 -6 3 0 1494.05 1350.04 6.24 o -6 -6 3 1 86.15 81.03 1.87 o -6 -6 3 2 0.87 0.67 1.40 < -4 -6 3 -2 1.33 2.19 1.51 < -4 -6 3 -1 15.47 15.84 1.34 o -4 -6 3 0 172.02 157.39 1.79 o -4 -6 3 1 41.38 39.01 1.04 o -4 -6 3 2 2.35 2.26 0.86 < -2 -6 3 -2 13.68 14.53 1.10 o -2 -6 3 -1 3.02 2.75 0.86 o -2 -6 3 0 1349.70 1362.63 3.09 o -2 -6 3 1 31.25 31.96 1.04 o -2 -6 3 2 0.07 0.89 0.75 < 0 -6 3 -2 6.07 6.27 1.03 o 0 -6 3 -1 8.59 8.18 0.90 o 0 -6 3 0 1404.80 1391.76 4.37 o 0 -6 3 1 0.61 1.34 1.15 < 0 -6 3 2 0.92 1.90 1.17 < 2 -6 3 -2 1.57 2.57 0.78 o 2 -6 3 -1 49.55 49.51 1.39 o 2 -6 3 0 711.85 682.43 3.13 o 2 -6 3 1 10.62 11.14 1.03 o 2 -6 3 2 0.27 -0.12 1.00 < 4 -6 3 -2 0.41 0.45 0.92 < 4 -6 3 -1 1.57 1.80 0.92 < 4 -6 3 0 603.60 576.49 2.98 o 4 -6 3 1 5.28 3.80 1.17 o 4 -6 3 2 0.49 1.10 1.45 < 6 -6 3 -2 0.05 1.01 1.15 < 6 -6 3 -1 8.80 6.85 1.65 o 6 -6 3 0 0.98 1.99 1.51 < 6 -6 3 1 104.29 98.81 2.26 o 6 -6 3 2 0.53 -0.40 3.00 < 8 -6 3 -2 3.85 3.69 1.73 < 8 -6 3 -1 14.79 16.66 2.22 o -9 -5 3 -1 24.06 24.65 2.63 o -9 -5 3 0 147.87 146.59 3.94 o -9 -5 3 1 32.47 34.02 2.54 o -9 -5 3 2 12.09 13.40 2.33 o -7 -5 3 -2 11.17 10.27 2.44 o -7 -5 3 -1 187.73 168.13 3.39 o -7 -5 3 0 228.43 210.05 3.01 o -7 -5 3 1 0.80 -0.39 1.74 < -7 -5 3 2 1.72 1.79 2.26 < -5 -5 3 -2 5.78 5.12 1.59 o -5 -5 3 -1 19.40 18.56 1.57 o -5 -5 3 0 79.28 75.59 1.73 o -5 -5 3 1 8.75 9.79 1.12 o -5 -5 3 2 0.50 -0.39 1.03 < -3 -5 3 -2 0.48 0.02 1.17 < -3 -5 3 -1 331.04 306.64 2.32 o -3 -5 3 0 1275.83 1275.29 3.42 o -3 -5 3 1 27.22 26.86 0.81 o -3 -5 3 2 4.36 4.93 0.78 o -1 -5 3 -2 0.58 -0.05 0.79 < -1 -5 3 -1 36.21 35.23 1.04 o -1 -5 3 0 102.28 110.79 1.77 o -1 -5 3 1 4.53 4.73 0.98 o -1 -5 3 2 2.04 2.29 0.92 < 1 -5 3 -2 0.20 0.31 0.79 < 1 -5 3 -1 33.79 34.53 1.40 o 1 -5 3 0 4415.13 4339.60 7.38 o 1 -5 3 1 45.59 45.75 1.34 o 1 -5 3 2 2.42 1.62 0.79 < 3 -5 3 -2 3.84 3.86 0.90 o 3 -5 3 -1 21.05 20.37 0.81 o 3 -5 3 0 374.12 362.50 2.18 o 3 -5 3 1 14.81 14.16 1.00 o 3 -5 3 2 0.25 0.19 1.00 < 5 -5 3 -2 2.01 1.57 0.89 < 5 -5 3 -1 2.33 1.24 1.06 < 5 -5 3 0 531.11 500.72 2.87 o 5 -5 3 1 0.41 -0.33 1.34 < 5 -5 3 2 0.01 -0.34 1.52 < 7 -5 3 -2 2.83 2.46 1.71 < 7 -5 3 -1 31.77 29.22 1.71 o 7 -5 3 0 638.39 625.93 4.60 o 7 -5 3 1 23.54 22.11 2.05 o 9 -5 3 -2 4.67 4.62 2.54 < -10 -4 3 0 0.62 -0.45 3.13 < -10 -4 3 1 99.34 99.87 3.21 o -10 -4 3 2 2.84 3.42 2.86 < -8 -4 3 -2 2.86 2.80 2.15 < -8 -4 3 -1 52.89 53.78 2.55 o -8 -4 3 0 664.77 653.85 4.89 o -8 -4 3 1 178.22 167.43 3.19 o -8 -4 3 2 22.86 22.05 2.04 o -6 -4 3 -2 5.13 5.62 1.68 o -6 -4 3 -1 31.36 31.37 1.79 o -6 -4 3 0 97.22 90.60 2.18 o -6 -4 3 1 174.89 166.21 2.38 o -6 -4 3 2 10.28 11.86 1.52 o -4 -4 3 -2 13.43 13.80 1.34 o -4 -4 3 -1 0.00 0.23 1.06 < -4 -4 3 0 2003.44 1975.29 4.99 o -4 -4 3 1 174.88 173.67 1.85 o -4 -4 3 2 2.02 3.36 0.84 o -2 -4 3 -2 1.88 1.04 0.67 < -2 -4 3 -1 39.90 34.57 0.87 o -2 -4 3 0 370.56 352.94 1.48 o -2 -4 3 1 85.21 85.41 0.92 o -2 -4 3 2 2.71 2.38 0.70 o 0 -4 3 -2 1.30 0.37 0.51 < 0 -4 3 -1 16.06 14.95 0.65 o 0 -4 3 0 8.92 10.24 0.75 o 0 -4 3 1 22.59 21.50 1.04 o 0 -4 3 2 0.57 0.05 1.20 < 2 -4 3 -2 0.44 0.64 0.56 < 2 -4 3 -1 53.36 53.25 1.01 o 2 -4 3 0 710.87 711.05 2.94 o 2 -4 3 1 3.47 3.55 0.93 o 2 -4 3 2 0.02 -0.17 0.79 < 4 -4 3 -2 0.01 -0.53 0.72 < 4 -4 3 -1 1.54 1.28 0.75 < 4 -4 3 0 464.58 461.60 2.51 o 4 -4 3 1 25.08 24.12 1.23 o 4 -4 3 2 0.39 0.19 1.40 < 6 -4 3 -2 4.63 3.83 1.09 o 6 -4 3 -1 94.82 86.52 1.63 o 6 -4 3 0 575.25 563.68 4.17 o 6 -4 3 1 0.07 -0.25 1.70 < 6 -4 3 2 1.93 0.33 2.19 < 8 -4 3 -2 3.88 3.17 1.85 < 8 -4 3 -1 16.05 14.73 2.08 o 8 -4 3 0 410.83 403.05 4.12 o -11 -3 3 2 3.02 0.45 3.28 < -9 -3 3 -2 6.73 7.08 2.57 < -9 -3 3 -1 99.48 102.76 3.11 o -9 -3 3 0 50.06 48.58 2.66 o -9 -3 3 1 0.27 0.34 2.18 < -9 -3 3 2 0.23 1.35 2.55 < -7 -3 3 -2 1.32 2.94 1.87 < -7 -3 3 -1 33.44 34.65 2.32 o -7 -3 3 0 78.12 72.52 2.15 o -7 -3 3 1 43.39 44.38 1.70 o -7 -3 3 2 1.15 1.06 1.60 < -5 -3 3 -2 1.21 -1.17 1.57 < -5 -3 3 -1 272.77 262.05 2.65 o -5 -3 3 0 2295.16 2263.08 6.86 o -5 -3 3 1 9.69 10.02 1.14 o -5 -3 3 2 3.99 5.15 1.07 o -3 -3 3 -2 15.37 13.15 0.84 o -3 -3 3 -1 10.50 11.16 0.72 o -3 -3 3 0 123.52 125.20 1.46 o -3 -3 3 1 28.44 27.34 0.70 o -3 -3 3 2 0.89 0.17 0.61 < -1 -3 3 -2 0.53 1.01 0.78 < -1 -3 3 -1 70.84 70.65 0.58 o -1 -3 3 0 8969.23 8376.86 6.37 o -1 -3 3 1 61.40 58.82 0.95 o -1 -3 3 2 1.60 2.89 1.10 < 1 -3 3 -2 0.46 1.03 0.39 < 1 -3 3 -1 17.93 17.88 0.73 o 1 -3 3 0 42.30 43.09 1.03 o 1 -3 3 1 3.91 4.05 1.04 o 1 -3 3 2 0.27 0.47 0.87 < 3 -3 3 -2 0.08 -0.25 1.01 < 3 -3 3 -1 0.23 1.06 0.67 < 3 -3 3 0 3319.19 3172.44 5.04 o 3 -3 3 1 16.32 15.57 1.06 o 3 -3 3 2 0.88 1.37 1.12 < 5 -3 3 -2 0.02 -0.89 0.75 < 5 -3 3 -1 8.39 7.72 1.03 o 5 -3 3 0 669.20 636.57 3.12 o 5 -3 3 1 12.39 11.56 1.49 o 5 -3 3 2 0.02 0.95 1.62 < 7 -3 3 -2 2.33 2.32 1.37 < 7 -3 3 -1 22.88 23.96 2.30 o 7 -3 3 0 144.00 135.67 2.51 o 7 -3 3 1 84.21 75.43 2.40 o 7 -3 3 2 0.19 0.30 3.44 < 9 -3 3 -2 0.51 1.20 2.07 < 9 -3 3 -1 2.80 2.69 2.29 < -10 -2 3 -1 0.03 0.11 2.46 < -10 -2 3 0 19.74 18.14 2.37 o -10 -2 3 1 55.01 57.80 2.82 o -10 -2 3 2 19.12 17.85 2.47 o -8 -2 3 -2 30.19 34.42 2.41 o -8 -2 3 -1 64.69 64.98 2.44 o -8 -2 3 0 374.81 381.31 3.40 o -8 -2 3 1 32.77 36.19 1.79 o -8 -2 3 2 8.25 8.59 1.51 o -6 -2 3 -2 5.12 6.07 1.57 o -6 -2 3 -1 23.22 25.24 1.63 o -6 -2 3 0 528.01 545.33 3.22 o -6 -2 3 1 198.12 203.46 2.48 o -6 -2 3 2 9.32 8.93 1.07 o -4 -2 3 -2 7.45 8.48 1.40 o -4 -2 3 -1 240.93 231.68 1.89 o -4 -2 3 0 1765.84 1802.33 4.69 o -4 -2 3 1 3.94 3.31 0.75 o -4 -2 3 2 0.61 0.53 0.62 < -2 -2 3 -2 13.00 11.73 0.62 o -2 -2 3 0 442.22 419.53 1.70 o -2 -2 3 1 80.19 74.62 1.03 o -2 -2 3 2 0.37 1.70 0.86 < 0 -2 3 -2 0.07 -0.19 0.26 < 0 -2 3 -1 75.95 74.33 0.58 o 0 -2 3 0 196.17 216.70 1.22 o 0 -2 3 1 7.65 8.17 0.59 o 0 -2 3 2 0.00 0.31 1.00 < 2 -2 3 -2 1.34 1.29 0.33 o 2 -2 3 -1 23.10 23.40 0.64 o 2 -2 3 0 1794.99 1855.76 5.08 o 2 -2 3 1 3.09 4.84 1.40 o 2 -2 3 2 0.54 0.11 1.23 < 4 -2 3 -2 2.04 1.01 0.90 < 4 -2 3 -1 52.13 49.62 1.45 o 4 -2 3 0 128.29 129.76 2.04 o 4 -2 3 1 0.20 1.01 1.46 < 4 -2 3 2 0.49 0.26 1.43 < 6 -2 3 -2 7.69 6.81 1.35 o 6 -2 3 -1 15.32 14.69 1.35 o 6 -2 3 0 2008.30 1916.19 7.31 o 6 -2 3 1 1.35 0.23 1.93 < 6 -2 3 2 1.26 0.44 1.91 < 8 -2 3 -2 1.59 2.74 1.84 < 8 -2 3 -1 44.56 40.76 2.33 o 8 -2 3 0 4.38 3.92 2.05 < 8 -2 3 1 2.69 1.85 4.81 < 10 -2 3 -2 13.83 12.82 2.49 o -11 -1 3 1 15.68 14.28 3.17 o -11 -1 3 2 2.50 4.22 3.08 < -9 -1 3 -2 1.04 1.04 2.52 < -9 -1 3 -1 124.21 131.52 2.79 o -9 -1 3 0 525.52 529.37 4.10 o -9 -1 3 1 213.21 224.22 2.90 o -9 -1 3 2 3.48 4.75 2.08 < -7 -1 3 -2 0.12 0.65 1.77 < -7 -1 3 -1 39.92 42.19 1.96 o -7 -1 3 0 665.64 687.42 3.86 o -7 -1 3 1 61.97 66.49 1.67 o -7 -1 3 2 7.26 9.54 1.68 o -5 -1 3 -2 17.34 18.80 1.23 o -5 -1 3 -1 129.11 130.26 1.98 o -5 -1 3 0 723.10 728.63 4.21 o -5 -1 3 1 346.32 350.34 2.32 o -5 -1 3 2 8.09 8.43 1.26 o -3 -1 3 -2 1.86 2.68 1.06 < -3 -1 3 -1 40.29 37.34 0.95 o -3 -1 3 0 2104.15 2054.79 3.82 o -3 -1 3 1 187.10 175.15 1.45 o -3 -1 3 2 2.79 4.12 0.92 o -1 -1 3 -2 9.62 9.10 0.54 o -1 -1 3 -1 1.91 1.59 0.42 o -1 -1 3 0 588.29 620.42 2.66 o -1 -1 3 1 58.82 56.68 1.00 o -1 -1 3 2 0.76 0.65 0.82 < 1 -1 3 -2 1.35 1.45 0.25 o 1 -1 3 -1 17.80 18.92 0.53 o 1 -1 3 0 4228.51 4270.54 5.82 o 1 -1 3 1 11.34 11.50 0.73 o 1 -1 3 2 1.01 1.54 1.29 < 3 -1 3 -2 0.73 0.37 0.45 < 3 -1 3 -1 2.36 2.82 0.78 o 3 -1 3 0 172.58 195.53 1.84 o 3 -1 3 1 2.81 2.01 1.14 < 3 -1 3 2 1.38 0.89 1.60 < 5 -1 3 -2 0.59 -0.16 1.03 < 5 -1 3 -1 0.18 -0.90 1.40 < 5 -1 3 0 134.21 135.54 2.43 o 5 -1 3 1 33.68 31.20 2.23 o 5 -1 3 2 0.09 -0.84 1.99 < 7 -1 3 -2 2.93 2.71 1.87 < 7 -1 3 -1 40.86 41.05 2.47 o 7 -1 3 0 88.11 89.25 3.16 o 7 -1 3 1 11.33 11.67 2.35 o 7 -1 3 2 0.04 1.70 4.92 < 9 -1 3 -2 1.33 1.71 2.99 < 9 -1 3 -1 10.59 10.02 2.79 o -10 0 3 -2 9.14 9.85 3.30 < -10 0 3 -1 44.38 48.97 2.86 o -10 0 3 0 100.57 108.17 3.07 o -10 0 3 1 6.64 7.61 2.32 o -10 0 3 2 12.48 10.58 2.61 o -8 0 3 -2 4.71 5.88 2.07 < -8 0 3 -1 103.16 108.73 2.30 o -8 0 3 0 3.16 5.60 1.63 o -8 0 3 1 1.82 1.18 1.68 < -8 0 3 2 0.25 -0.98 1.59 < -6 0 3 -2 2.55 3.30 1.52 < -6 0 3 -1 202.55 213.48 2.20 o -6 0 3 0 1714.70 1810.25 5.44 o -6 0 3 1 3.33 2.38 1.46 < -6 0 3 2 1.50 1.29 1.12 < -4 0 3 -2 5.81 6.07 1.35 o -4 0 3 -1 145.05 152.72 1.59 o -4 0 3 0 39.26 44.31 1.51 o -4 0 3 1 18.13 17.18 0.64 o -4 0 3 2 5.36 5.21 0.67 o -2 0 3 -2 2.60 2.18 0.68 o -2 0 3 -1 294.97 289.67 1.69 o -2 0 3 0 1864.92 1851.41 4.47 o -2 0 3 1 17.01 13.76 1.52 o -2 0 3 2 0.10 0.20 0.86 < 0 0 3 -2 0.24 -1.04 0.44 < 0 0 3 -1 58.52 55.35 0.87 o 0 0 3 0 2270.11 2290.85 3.50 o 0 0 3 1 42.94 41.55 0.78 o 0 0 3 2 2.59 2.44 0.70 o 2 0 3 -2 0.01 -0.30 0.53 < 2 0 3 -1 2.36 2.61 1.29 < 2 0 3 0 2686.25 2768.47 4.79 o 2 0 3 1 1.55 1.26 1.06 < 2 0 3 2 0.03 0.28 1.54 < 4 0 3 -2 2.51 2.40 1.20 < 4 0 3 -1 8.23 7.69 0.98 o 4 0 3 0 1463.06 1580.11 5.78 o 4 0 3 1 2.64 2.74 1.98 < 4 0 3 2 1.25 2.04 2.16 < 6 0 3 -2 2.81 2.66 1.35 < 6 0 3 -1 16.66 16.54 2.12 o 6 0 3 0 119.43 115.03 2.60 o 6 0 3 1 29.54 28.10 2.32 o 6 0 3 2 0.24 1.37 2.33 < 8 0 3 -2 1.26 3.10 2.60 < 8 0 3 -1 9.52 6.97 3.00 < 8 0 3 0 782.41 769.28 6.58 o 10 0 3 -2 1.57 1.26 2.92 < -11 1 3 0 169.62 167.35 7.86 o -11 1 3 1 42.51 43.20 3.33 o -11 1 3 2 5.47 8.62 3.02 < -9 1 3 -2 4.42 6.52 2.35 < -9 1 3 -1 6.34 8.37 2.21 o -9 1 3 0 24.14 38.18 2.23 o -9 1 3 1 253.77 262.86 2.93 o -9 1 3 2 40.29 44.89 1.88 o -7 1 3 -2 16.63 18.75 1.60 o -7 1 3 -1 0.26 0.50 1.35 < -7 1 3 0 0.54 11.64 1.49 o -7 1 3 1 84.11 83.62 1.90 o -7 1 3 2 7.22 7.16 1.35 o -5 1 3 -2 20.79 21.80 1.18 o -5 1 3 -1 5.39 5.63 1.18 o -5 1 3 0 47.77 61.63 1.71 o -5 1 3 1 372.19 369.42 2.26 o -5 1 3 2 21.83 20.91 0.92 o -3 1 3 -2 10.46 11.97 1.57 o -3 1 3 -1 16.18 15.78 1.40 o -3 1 3 0 13.35 21.29 0.67 o -3 1 3 1 142.14 133.26 1.51 o -3 1 3 2 3.34 2.94 0.93 o -1 1 3 -2 13.12 10.66 0.45 o -1 1 3 -1 35.44 28.56 0.87 o -1 1 3 1 41.35 38.40 0.93 o -1 1 3 2 0.15 0.78 0.67 < 1 1 3 -2 1.61 1.66 0.47 o 1 1 3 0 1458.86 1449.32 6.67 o 1 1 3 1 9.51 9.99 1.20 o 1 1 3 2 0.14 -0.59 1.23 < 3 1 3 -2 3.28 3.30 0.44 o 3 1 3 -1 5.75 5.29 0.81 o 3 1 3 0 2.87 8.14 0.93 o 3 1 3 1 0.96 1.85 1.48 < 3 1 3 2 0.00 -1.48 1.71 < 5 1 3 -2 0.53 -0.16 1.23 < 5 1 3 -1 4.80 4.50 1.66 < 5 1 3 0 144.03 143.41 2.38 o 5 1 3 1 1.15 2.52 2.02 < 5 1 3 2 0.24 -0.26 2.46 < 7 1 3 -2 8.81 7.56 1.71 o 7 1 3 -1 134.63 132.38 3.89 o 7 1 3 0 247.74 246.56 4.94 o 7 1 3 1 0.74 0.16 2.63 < 9 1 3 -2 8.09 7.55 2.64 < 9 1 3 -1 11.79 9.76 2.97 o -10 2 3 -2 2.36 4.05 3.08 < -10 2 3 -1 83.00 93.76 3.05 o -10 2 3 0 34.02 27.64 2.55 o -10 2 3 1 24.13 23.96 2.12 o -10 2 3 2 1.19 0.82 1.94 < -8 2 3 -2 0.72 1.10 1.84 < -8 2 3 -1 60.04 64.24 2.16 o -8 2 3 0 1011.75 1013.73 5.24 o -8 2 3 1 6.10 5.76 1.66 o -8 2 3 2 0.77 1.52 1.29 < -6 2 3 -2 0.18 0.06 1.35 < -6 2 3 -1 260.85 270.25 2.60 o -6 2 3 0 13.18 8.85 1.12 o -6 2 3 1 292.28 301.55 2.56 o -6 2 3 2 7.88 8.35 1.46 o -4 2 3 -2 2.36 2.99 1.15 < -4 2 3 -1 25.01 26.00 1.03 o -4 2 3 0 4105.71 3914.82 6.38 o -4 2 3 1 2.39 3.39 0.64 o -4 2 3 2 0.57 0.05 1.23 < -2 2 3 -2 2.47 2.47 0.58 o -2 2 3 -1 241.56 228.23 1.39 o -2 2 3 0 2781.67 2452.16 7.95 o -2 2 3 1 334.04 318.38 2.59 o -2 2 3 2 6.96 7.17 0.86 o 0 2 3 -2 0.28 0.39 0.56 < 0 2 3 -1 5.95 5.12 0.34 o 0 2 3 0 1496.04 1394.01 2.90 o 0 2 3 1 0.17 -1.09 0.89 < 0 2 3 2 1.08 -0.36 1.37 < 2 2 3 -1 26.49 26.78 2.18 o 2 2 3 0 2878.99 2943.52 8.64 o 2 2 3 1 0.14 -0.39 1.40 < 2 2 3 2 1.76 1.94 1.74 < 4 2 3 -2 1.59 1.23 1.06 < 4 2 3 -1 9.87 10.69 1.15 o 4 2 3 0 108.93 108.76 2.02 o 4 2 3 1 7.83 6.83 2.08 o 4 2 3 2 0.76 0.06 2.22 < 6 2 3 -2 0.00 0.51 1.38 < 6 2 3 -1 0.88 1.14 1.80 < 6 2 3 0 1996.92 1983.30 11.40 o 6 2 3 1 39.92 36.40 2.88 o 6 2 3 2 0.26 0.20 2.85 < 8 2 3 -2 1.26 3.02 2.24 < 8 2 3 -1 0.19 1.09 3.14 < 8 2 3 0 16.32 19.67 2.97 o 10 2 3 -2 1.81 2.02 4.65 < -11 3 3 1 66.09 76.29 3.66 o -11 3 3 2 24.20 26.17 5.07 o -9 3 3 -2 17.42 21.55 2.40 o -9 3 3 -1 104.96 104.82 2.74 o -9 3 3 0 0.52 0.72 1.82 < -9 3 3 1 0.29 1.23 1.91 < -9 3 3 2 1.86 0.87 1.57 < -7 3 3 -2 4.32 6.85 1.40 o -7 3 3 -1 35.94 39.34 1.77 o -7 3 3 0 15.50 17.13 1.38 o -7 3 3 1 69.08 70.86 1.76 o -7 3 3 2 29.72 29.64 1.32 o -5 3 3 -2 17.57 19.36 1.10 o -5 3 3 -1 214.26 211.68 1.90 o -5 3 3 0 882.85 919.23 3.90 o -5 3 3 1 1.02 2.19 1.23 < -5 3 3 2 0.02 -1.01 1.06 < -3 3 3 -2 0.04 -0.96 0.84 < -3 3 3 -1 315.97 305.93 2.22 o -3 3 3 0 18.31 20.10 0.82 o -3 3 3 1 32.69 33.46 1.35 o -3 3 3 2 0.00 1.18 1.14 < -1 3 3 -2 5.02 3.89 0.56 o -1 3 3 -1 93.42 82.05 1.64 o -1 3 3 0 6113.26 5498.78 6.52 o -1 3 3 1 8.80 7.86 0.73 o -1 3 3 2 0.75 0.56 1.01 < 1 3 3 -2 0.10 -0.20 0.61 < 1 3 3 -1 106.38 105.53 2.18 o 1 3 3 0 205.27 190.85 2.28 o 1 3 3 1 76.37 76.51 1.67 o 1 3 3 2 1.45 -0.81 2.01 < 3 3 3 -1 2.06 0.92 1.35 < 3 3 3 0 2878.88 2969.75 8.64 o 3 3 3 1 7.42 8.29 2.10 o 3 3 3 2 0.92 -0.31 2.29 < 5 3 3 -2 5.59 6.35 1.35 o 5 3 3 -1 37.56 33.77 2.65 o 5 3 3 0 788.53 797.69 7.13 o 5 3 3 1 22.83 25.08 2.41 o 5 3 3 2 0.28 0.39 2.61 < 7 3 3 -2 3.09 3.13 1.68 < 7 3 3 -1 0.19 1.28 1.85 < 7 3 3 0 279.03 259.70 4.32 o 7 3 3 1 27.60 24.32 3.11 o 9 3 3 -2 3.24 3.30 3.24 < 9 3 3 -1 53.71 52.06 5.45 o -10 4 3 -1 34.40 41.02 3.28 o -10 4 3 0 145.92 138.79 3.16 o -10 4 3 1 95.96 99.59 2.80 o -10 4 3 2 20.28 22.70 2.63 o -8 4 3 -2 15.65 17.13 1.82 o -8 4 3 -1 42.79 47.00 2.13 o -8 4 3 0 36.87 41.81 2.01 o -8 4 3 1 277.55 296.86 2.77 o -8 4 3 2 7.78 9.68 1.38 o -6 4 3 -2 3.30 4.42 1.26 o -6 4 3 -1 16.45 16.43 1.42 o -6 4 3 0 1849.32 1869.41 5.35 o -6 4 3 1 172.82 174.62 1.84 o -6 4 3 2 7.55 6.77 1.12 o -4 4 3 -2 16.34 16.66 1.09 o -4 4 3 -1 31.93 29.35 1.34 o -4 4 3 0 47.74 47.93 1.10 o -4 4 3 1 344.67 321.82 3.24 o -4 4 3 2 14.73 16.34 1.38 o -2 4 3 -2 24.30 22.95 0.84 o -2 4 3 -1 2.58 1.76 1.37 < -2 4 3 0 404.19 398.86 4.78 o -2 4 3 1 139.02 135.15 1.84 o -2 4 3 2 0.02 0.03 1.06 < 0 4 3 -2 0.06 0.31 0.61 < 0 4 3 -1 27.85 25.12 0.82 o 0 4 3 0 1061.57 1002.81 3.25 o 0 4 3 1 119.41 120.44 2.10 o 0 4 3 2 0.11 0.82 1.52 < 2 4 3 -1 61.09 56.00 2.09 o 2 4 3 0 42.96 40.71 1.77 o 2 4 3 1 12.21 13.79 1.90 o 2 4 3 2 1.07 0.59 1.73 < 4 4 3 -2 0.02 0.98 1.88 < 4 4 3 -1 2.63 3.00 1.24 < 4 4 3 0 660.18 700.78 5.12 o 4 4 3 1 12.76 12.84 2.86 o 4 4 3 2 1.08 1.09 2.49 < 6 4 3 -2 3.24 3.30 1.73 < 6 4 3 -1 30.67 30.36 2.43 o 6 4 3 0 639.58 619.23 4.75 o 6 4 3 1 6.38 7.34 2.72 < 8 4 3 -2 0.56 1.07 2.04 < 8 4 3 -1 18.06 14.00 2.83 o 8 4 3 0 151.70 149.61 6.66 o -9 5 3 -2 4.74 4.50 2.72 < -9 5 3 -1 81.44 83.33 3.19 o -9 5 3 0 254.80 252.08 3.38 o -9 5 3 1 1.82 1.96 1.96 < -9 5 3 2 4.99 6.08 1.82 o -7 5 3 -2 14.39 13.18 1.73 o -7 5 3 -1 75.37 82.66 2.47 o -7 5 3 0 428.83 417.22 4.69 o -7 5 3 1 1.62 0.61 1.37 < -7 5 3 2 0.71 1.91 1.52 < -5 5 3 -2 0.61 0.05 1.17 < -5 5 3 -1 320.36 327.14 2.57 o -5 5 3 0 310.54 306.20 2.01 o -5 5 3 1 49.25 47.75 1.31 o -5 5 3 2 0.03 -0.19 1.57 < -3 5 3 -2 13.28 12.43 1.03 o -3 5 3 -1 35.87 36.18 1.24 o -3 5 3 0 2347.12 2252.54 7.62 o -3 5 3 1 2.27 2.80 1.17 < -3 5 3 2 1.48 1.34 1.20 < -1 5 3 -2 0.95 0.90 1.10 < -1 5 3 -1 141.44 134.17 3.02 o -1 5 3 0 179.38 189.19 3.72 o -1 5 3 1 109.37 104.47 1.53 o -1 5 3 2 1.40 -0.20 1.26 < 1 5 3 -2 1.35 1.18 0.73 < 1 5 3 -1 6.39 6.11 0.89 o 1 5 3 0 5106.29 5029.60 13.32 o 1 5 3 1 3.58 2.83 2.54 < 1 5 3 2 0.24 -0.50 1.76 < 3 5 3 -2 2.62 2.04 1.37 < 3 5 3 -1 4.82 4.53 1.59 < 3 5 3 0 607.32 618.51 4.68 o 3 5 3 1 26.17 26.62 1.99 o 3 5 3 2 0.29 1.48 2.52 < 5 5 3 -2 5.40 5.99 1.17 o 5 5 3 -1 8.50 6.43 1.51 o 5 5 3 0 620.09 628.04 5.34 o 5 5 3 1 91.50 89.98 4.12 o 5 5 3 2 0.73 1.29 2.80 < 7 5 3 -2 1.85 1.46 1.80 < 7 5 3 -1 5.96 5.60 2.19 < 7 5 3 0 475.16 427.99 5.26 o 9 5 3 -2 1.15 -0.48 2.83 < -10 6 3 0 8.09 10.89 3.78 < -10 6 3 1 57.53 59.23 5.42 o -10 6 3 2 23.95 25.42 4.98 o -8 6 3 -2 2.62 6.22 2.43 < -8 6 3 -1 22.38 21.35 2.54 o -8 6 3 0 96.60 95.57 2.30 o -8 6 3 1 28.95 30.23 1.87 o -8 6 3 2 11.55 12.73 1.70 o -6 6 3 -2 13.23 13.83 1.59 o -6 6 3 -1 33.31 31.34 1.49 o -6 6 3 0 460.15 461.68 3.09 o -6 6 3 1 85.37 84.75 1.70 o -6 6 3 2 24.13 22.87 1.60 o -4 6 3 -2 13.95 15.47 1.37 o -4 6 3 -1 48.83 47.30 1.09 o -4 6 3 0 218.88 212.53 1.65 o -4 6 3 1 22.24 21.64 1.40 o -4 6 3 2 2.78 1.20 1.42 < -2 6 3 -2 0.03 -0.12 0.87 < -2 6 3 0 139.80 158.25 2.43 o -2 6 3 1 43.16 42.76 1.65 o -2 6 3 2 3.72 4.70 1.37 o 0 6 3 -2 6.12 6.19 1.21 o 0 6 3 -1 8.01 8.20 1.04 o 0 6 3 0 218.20 214.05 2.13 o 0 6 3 1 17.99 18.92 1.38 o 0 6 3 2 0.08 -0.30 2.15 < 2 6 3 -2 0.54 1.34 1.03 < 2 6 3 -1 73.70 74.42 2.40 o 2 6 3 0 414.87 413.83 4.85 o 2 6 3 1 0.80 1.57 1.98 < 2 6 3 2 0.15 0.45 1.84 < 4 6 3 -2 2.49 3.78 1.45 < 4 6 3 -1 10.32 9.10 1.48 o 4 6 3 0 498.19 512.93 3.71 o 4 6 3 1 1.74 1.01 2.13 < 4 6 3 2 2.72 1.54 3.61 < 6 6 3 -2 0.33 0.08 1.74 < 6 6 3 -1 2.81 3.52 2.41 < 6 6 3 0 37.19 40.46 3.03 o 6 6 3 1 6.69 5.06 3.00 < 8 6 3 -2 5.89 7.79 2.27 o 8 6 3 -1 51.12 47.15 2.72 o -9 7 3 -2 0.07 0.86 4.68 < -9 7 3 -1 52.36 54.64 3.87 o -9 7 3 0 13.87 14.81 3.28 o -9 7 3 1 148.06 155.37 4.23 o -9 7 3 2 3.23 6.27 4.34 < -7 7 3 -2 2.18 3.00 2.63 < -7 7 3 -1 111.65 114.57 3.56 o -7 7 3 0 194.73 196.66 2.99 o -7 7 3 1 43.75 44.69 2.07 o -7 7 3 2 1.85 3.52 3.31 < -5 7 3 -2 0.63 0.65 1.07 < -5 7 3 -1 7.92 7.78 1.09 o -5 7 3 0 342.28 334.56 2.57 o -5 7 3 1 256.16 262.35 2.73 o -5 7 3 2 3.42 4.78 1.57 o -3 7 3 -2 7.58 5.99 1.54 o -3 7 3 -1 128.02 120.76 2.30 o -3 7 3 0 741.73 732.95 3.95 o -3 7 3 1 195.22 186.25 3.05 o -3 7 3 2 1.63 0.26 1.54 < -1 7 3 -2 2.37 1.06 1.32 < -1 7 3 -1 3.38 3.10 2.38 < -1 7 3 0 1296.50 1268.95 5.94 o -1 7 3 1 35.96 32.51 1.57 o -1 7 3 2 0.67 0.12 1.48 < 1 7 3 -2 0.50 0.20 0.89 < 1 7 3 -1 9.43 8.11 1.20 o 1 7 3 0 108.99 102.64 3.07 o 1 7 3 1 76.92 73.32 3.02 o 1 7 3 2 0.13 -1.15 2.02 < 3 7 3 -2 0.13 -0.25 1.98 < 3 7 3 -1 2.16 1.80 1.82 < 3 7 3 0 585.52 599.87 4.43 o 3 7 3 1 1.91 0.98 2.15 < 3 7 3 2 1.24 0.47 2.41 < 5 7 3 -2 1.27 0.90 1.70 < 5 7 3 -1 0.04 1.10 1.73 < 5 7 3 0 172.16 176.44 3.33 o 5 7 3 1 1.29 -0.58 3.69 < 7 7 3 -2 1.41 1.84 2.15 < 7 7 3 -1 44.62 41.36 3.05 o 7 7 3 0 59.97 64.79 5.98 o -8 8 3 -2 11.15 12.18 3.21 o -8 8 3 -1 15.26 13.37 3.22 o -8 8 3 0 175.03 180.23 4.39 o -8 8 3 1 60.83 58.86 3.35 o -8 8 3 2 7.15 5.62 3.97 < -6 8 3 -2 9.04 7.62 1.91 o -6 8 3 -1 173.59 177.69 3.78 o -6 8 3 0 6.34 7.19 2.30 o -6 8 3 1 50.98 51.03 3.89 o -6 8 3 2 0.02 -0.65 3.38 < -4 8 3 -2 3.42 3.98 1.20 o -4 8 3 -1 49.40 50.95 2.10 o -4 8 3 0 764.06 734.59 5.47 o -4 8 3 1 63.24 63.26 3.98 o -4 8 3 2 0.60 0.61 3.34 < -2 8 3 -2 4.30 5.71 2.52 < -2 8 3 -1 165.95 172.23 4.70 o -2 8 3 0 522.35 488.20 5.04 o -2 8 3 1 146.95 145.41 2.24 o -2 8 3 2 0.74 -0.31 1.91 < 0 8 3 -2 0.20 -0.59 1.03 < 0 8 3 -1 95.80 100.98 1.54 o 0 8 3 0 673.04 657.07 4.84 o 0 8 3 1 12.20 11.78 2.60 o 0 8 3 2 0.08 -0.22 2.71 < 2 8 3 -2 5.35 3.27 2.01 < 2 8 3 -1 8.46 8.21 2.21 o 2 8 3 0 774.12 720.65 6.72 o 2 8 3 1 4.11 4.00 2.40 < 2 8 3 2 0.32 -0.58 2.26 < 4 8 3 -2 0.72 0.47 1.48 < 4 8 3 -1 25.19 28.33 2.05 o 4 8 3 0 363.14 358.19 3.91 o 4 8 3 1 8.11 8.96 2.44 o 6 8 3 -2 3.44 2.49 1.93 < 6 8 3 -1 19.68 19.06 2.77 o 6 8 3 0 1137.51 1093.83 7.93 o 8 8 3 -2 9.60 6.74 2.94 < -7 9 3 -2 2.17 3.81 2.96 < -7 9 3 -1 3.24 2.91 2.78 < -7 9 3 0 113.59 100.27 3.55 o -7 9 3 1 253.95 245.54 6.48 o -7 9 3 2 20.26 20.31 4.37 o -5 9 3 -2 10.53 14.13 2.40 o -5 9 3 -1 3.14 4.45 3.22 < -5 9 3 0 0.81 0.42 3.02 < -5 9 3 1 47.78 52.99 4.53 o -5 9 3 2 8.08 8.87 4.19 < -3 9 3 -2 0.83 1.51 2.61 < -3 9 3 -1 53.52 47.87 3.86 o -3 9 3 0 208.56 204.02 5.47 o -3 9 3 1 9.27 9.29 1.90 o -3 9 3 2 2.12 2.13 2.21 < -1 9 3 -2 6.87 9.90 1.94 o -1 9 3 -1 1.00 2.21 1.52 < -1 9 3 0 254.97 265.90 2.85 o -1 9 3 1 179.02 185.14 3.32 o -1 9 3 2 5.57 6.19 2.30 < 1 9 3 -2 0.02 -1.60 1.29 < 1 9 3 -1 45.01 45.89 2.12 o 1 9 3 0 440.88 425.40 5.40 o 1 9 3 1 21.22 17.24 3.07 o 1 9 3 2 0.13 0.76 2.64 < 3 9 3 -2 0.57 1.42 2.38 < 3 9 3 -1 0.68 0.90 1.77 < 3 9 3 0 196.70 204.06 3.38 o 3 9 3 1 30.07 31.26 2.57 o 3 9 3 2 0.01 -0.36 3.80 < 5 9 3 -2 5.24 5.93 2.07 < 5 9 3 -1 22.98 21.67 2.23 o 5 9 3 0 31.92 33.33 2.85 o 7 9 3 -2 0.22 -0.17 2.47 < -6 10 3 -2 1.79 4.17 2.72 < -6 10 3 -1 30.77 27.14 2.86 o -6 10 3 0 768.08 727.86 10.32 o -6 10 3 1 0.41 -1.73 4.03 < -6 10 3 2 0.01 0.54 4.68 < -4 10 3 -2 0.03 0.16 2.24 < -4 10 3 -1 141.36 146.79 5.54 o -4 10 3 0 75.51 76.87 5.00 o -4 10 3 1 219.18 221.68 3.55 o -4 10 3 2 0.86 0.95 2.40 < -2 10 3 -2 1.17 0.89 2.18 < -2 10 3 -1 25.05 25.53 2.65 o -2 10 3 0 483.12 477.91 3.77 o -2 10 3 1 1.74 1.42 2.29 < -2 10 3 2 0.18 0.09 2.46 < 0 10 3 -2 2.62 3.83 1.43 < 0 10 3 -1 1.05 2.22 1.56 < 0 10 3 0 987.52 1001.74 6.54 o 0 10 3 1 92.29 85.44 3.77 o 0 10 3 2 0.28 -0.92 3.20 < 2 10 3 -2 2.38 1.56 2.35 < 2 10 3 -1 102.31 89.85 3.49 o 2 10 3 0 211.15 198.92 3.78 o 2 10 3 1 22.46 19.33 2.52 o 2 10 3 2 0.08 0.34 3.86 < 4 10 3 -2 5.48 6.61 1.68 o 4 10 3 -1 33.48 34.30 2.49 o 4 10 3 0 1069.99 1061.82 6.55 o 6 10 3 -2 0.24 -1.07 2.38 < 6 10 3 -1 8.37 8.29 3.98 < -5 11 3 -2 0.86 0.14 3.86 < -5 11 3 -1 125.54 130.49 6.16 o -5 11 3 0 0.26 -1.01 3.00 < -5 11 3 1 4.34 4.15 3.19 < -5 11 3 2 4.08 3.19 3.41 < -3 11 3 -2 17.05 21.08 2.83 o -3 11 3 -1 3.11 4.54 2.12 < -3 11 3 0 307.02 295.53 3.91 o -3 11 3 1 51.79 49.88 2.86 o -3 11 3 2 1.31 1.17 2.74 < -1 11 3 -2 0.08 -0.61 1.66 < -1 11 3 -1 130.62 133.09 2.58 o -1 11 3 0 24.48 23.18 2.55 o -1 11 3 1 54.23 57.72 3.03 o -1 11 3 2 0.37 -0.37 3.48 < 1 11 3 -2 1.64 0.30 1.71 < 1 11 3 -1 1.74 2.64 2.86 < 1 11 3 0 1010.95 948.28 8.38 o 1 11 3 1 24.73 22.44 3.05 o 3 11 3 -2 2.75 0.81 1.87 < 3 11 3 -1 18.54 19.32 2.19 o 3 11 3 0 123.64 118.24 3.21 o 5 11 3 -2 0.30 -0.36 2.43 < -4 12 3 -2 3.37 2.80 3.10 < -4 12 3 -1 1.88 3.08 3.22 < -4 12 3 0 348.73 339.77 4.54 o -4 12 3 1 42.69 42.50 3.83 o -2 12 3 -2 0.09 -0.65 2.22 < -2 12 3 -1 0.00 0.02 2.08 < -2 12 3 0 91.22 95.55 3.27 o -2 12 3 1 113.50 115.32 3.67 o 0 12 3 -2 5.56 7.00 1.93 o 0 12 3 -1 18.44 18.00 2.71 o 0 12 3 0 74.19 70.97 3.88 o 0 12 3 1 3.51 3.06 5.09 < 2 12 3 -2 2.02 1.31 2.99 < 2 12 3 -1 35.17 35.46 2.30 o 2 12 3 0 63.25 60.12 3.64 o 4 12 3 -2 1.03 2.21 2.97 < -3 13 3 -2 0.05 0.72 2.60 < -3 13 3 -1 117.36 117.19 3.49 o -1 13 3 -2 1.51 0.67 2.13 < -1 13 3 -1 15.75 16.24 2.97 o -1 13 3 0 427.48 407.96 6.38 o 1 13 3 -2 0.62 -0.19 3.24 < 1 13 3 -1 25.26 25.35 3.77 o 3 13 3 -2 0.28 2.21 3.81 < 0 -12 4 -2 0.48 0.86 4.34 < -5 -11 4 2 0.46 -1.17 4.78 < -3 -11 4 -2 2.51 1.37 2.40 < -3 -11 4 -1 6.66 7.50 4.40 < -3 -11 4 0 110.82 115.79 5.73 o -3 -11 4 1 0.54 1.37 4.11 < -3 -11 4 2 0.25 -1.00 4.64 < -1 -11 4 -2 3.13 3.63 3.10 < -1 -11 4 -1 6.37 4.39 3.05 < -1 -11 4 0 884.75 849.88 11.28 o -1 -11 4 1 25.68 27.77 4.71 o -1 -11 4 2 1.68 2.46 4.23 < 1 -11 4 -2 0.11 0.12 2.82 < 1 -11 4 -1 0.27 -0.53 4.23 < 1 -11 4 0 287.82 277.85 7.29 o 1 -11 4 1 1.99 0.12 4.39 < 3 -11 4 -2 0.40 2.02 3.05 < 3 -11 4 -1 6.33 6.11 4.40 < -6 -10 4 0 14.98 15.79 3.64 o -6 -10 4 1 62.36 59.06 3.72 o -6 -10 4 2 0.70 0.86 3.34 < -4 -10 4 -2 0.03 0.31 1.91 < -4 -10 4 -1 3.17 2.68 1.88 < -4 -10 4 0 0.87 1.70 2.36 < -4 -10 4 1 0.69 -0.19 2.38 < -4 -10 4 2 0.27 1.54 3.08 < -2 -10 4 -2 4.69 4.06 2.15 < -2 -10 4 -1 67.28 65.07 2.63 o -2 -10 4 0 391.80 416.52 7.45 o -2 -10 4 1 5.87 4.42 4.19 < -2 -10 4 2 1.02 -0.22 4.09 < 0 -10 4 -2 0.07 0.36 2.12 < 0 -10 4 -1 31.27 33.44 2.93 o 0 -10 4 0 7.80 7.69 4.05 < 0 -10 4 1 2.33 1.82 4.17 < 0 -10 4 2 0.72 1.51 3.92 < 2 -10 4 -2 0.88 0.39 2.80 < 2 -10 4 -1 34.92 31.53 3.10 o 2 -10 4 0 460.74 478.84 5.80 o 2 -10 4 1 17.59 19.70 4.56 o 4 -10 4 -2 0.75 0.87 2.36 < 4 -10 4 -1 35.27 36.66 3.25 o 4 -10 4 0 1.64 0.79 4.36 < -7 -9 4 0 348.79 299.68 5.35 o -7 -9 4 1 58.83 54.31 2.96 o -7 -9 4 2 7.27 7.03 2.36 < -5 -9 4 -2 6.25 5.31 1.90 < -5 -9 4 -1 6.74 5.15 1.70 o -5 -9 4 0 41.69 37.28 1.84 o -5 -9 4 1 2.31 1.42 2.13 < -5 -9 4 2 0.58 1.46 2.02 < -3 -9 4 -2 0.88 0.34 1.62 < -3 -9 4 -1 74.91 68.23 2.13 o -3 -9 4 0 742.38 749.26 4.72 o -3 -9 4 1 186.82 185.61 3.30 o -3 -9 4 2 7.18 7.64 4.12 < -1 -9 4 -2 0.09 -0.95 1.65 < -1 -9 4 -1 4.89 5.99 1.65 o -1 -9 4 0 5.99 4.95 2.44 < -1 -9 4 1 10.88 11.47 3.83 < -1 -9 4 2 0.51 0.61 3.62 < 1 -9 4 -2 2.47 2.54 1.80 < 1 -9 4 -1 3.17 4.22 2.33 < 1 -9 4 0 366.73 368.76 6.98 o 1 -9 4 1 14.88 13.38 3.81 o 1 -9 4 2 0.28 1.09 3.53 < 3 -9 4 -2 0.09 -0.33 2.12 < 3 -9 4 -1 7.54 6.30 2.16 < 3 -9 4 0 210.98 211.25 4.28 o 3 -9 4 1 16.71 15.34 2.89 o 5 -9 4 -2 0.17 -1.20 2.66 < 5 -9 4 -1 9.16 10.78 2.91 o -8 -8 4 1 72.46 65.32 3.64 o -8 -8 4 2 8.93 6.10 2.21 < -6 -8 4 -2 1.20 1.43 2.26 < -6 -8 4 -1 90.72 80.44 2.37 o -6 -8 4 0 624.78 560.74 3.62 o -6 -8 4 1 33.28 30.58 1.73 o -6 -8 4 2 1.39 -0.05 1.54 < -4 -8 4 -2 2.18 2.50 1.32 < -4 -8 4 -1 29.25 28.93 1.29 o -4 -8 4 0 265.76 246.39 2.09 o -4 -8 4 1 11.26 11.30 1.28 o -4 -8 4 2 0.17 1.03 1.38 < -2 -8 4 -2 5.59 5.20 1.04 o -2 -8 4 -1 0.43 0.78 1.14 < -2 -8 4 0 287.27 299.79 2.57 o -2 -8 4 1 16.46 16.71 1.57 o -2 -8 4 2 0.35 0.42 2.40 < 0 -8 4 -2 0.19 0.34 1.42 < 0 -8 4 -1 83.64 85.70 2.85 o 0 -8 4 0 937.12 913.28 9.90 o 0 -8 4 1 1.07 -0.59 3.20 < 0 -8 4 2 0.19 -0.98 3.16 < 2 -8 4 -2 2.34 2.91 1.66 < 2 -8 4 -1 48.40 53.27 2.24 o 2 -8 4 0 292.07 300.86 3.54 o 2 -8 4 1 13.10 12.17 2.50 o 2 -8 4 2 0.46 2.61 3.55 < 4 -8 4 -2 0.09 -0.87 1.88 < 4 -8 4 -1 0.39 0.79 2.46 < 4 -8 4 0 1206.21 1170.68 8.14 o 4 -8 4 1 0.89 0.42 3.80 < 6 -8 4 -2 0.20 0.34 1.85 < 6 -8 4 -1 18.16 17.32 2.86 o -9 -7 4 2 1.75 2.55 4.28 < -7 -7 4 -2 14.28 14.05 2.51 o -7 -7 4 -1 34.77 29.80 2.19 o -7 -7 4 0 1.65 2.08 2.10 < -7 -7 4 1 58.21 57.33 1.98 o -7 -7 4 2 3.80 3.78 1.48 < -5 -7 4 -2 5.38 5.52 1.73 o -5 -7 4 -1 25.39 24.12 1.45 o -5 -7 4 0 156.71 157.29 1.71 o -5 -7 4 1 97.47 92.79 1.76 o -5 -7 4 2 0.85 0.92 1.20 < -3 -7 4 -2 10.76 9.82 0.95 o -3 -7 4 -1 108.78 102.59 1.32 o -3 -7 4 0 135.05 140.44 1.51 o -3 -7 4 1 0.92 1.49 1.00 < -3 -7 4 2 1.16 2.32 1.09 < -1 -7 4 -2 4.52 5.01 0.75 o -1 -7 4 -1 1.51 1.66 0.79 < -1 -7 4 0 616.66 654.78 3.17 o -1 -7 4 1 48.21 51.04 2.57 o -1 -7 4 2 0.02 -2.21 2.16 < 1 -7 4 -2 0.35 0.17 1.10 < 1 -7 4 -1 27.21 28.26 1.87 o 1 -7 4 0 449.90 481.18 4.91 o 1 -7 4 1 18.62 20.63 3.13 o 1 -7 4 2 3.98 3.58 3.39 < 3 -7 4 -2 2.48 3.47 1.68 < 3 -7 4 -1 0.13 0.64 1.66 < 3 -7 4 0 1.89 1.94 1.73 < 3 -7 4 1 0.54 -0.23 2.40 < 3 -7 4 2 0.06 -0.23 3.47 < 5 -7 4 -2 1.60 1.10 1.57 < 5 -7 4 -1 24.04 23.54 1.85 o 5 -7 4 0 70.79 69.29 3.13 o 5 -7 4 1 4.64 4.84 4.01 < 7 -7 4 -2 3.05 3.59 2.33 < 7 -7 4 -1 1.80 1.56 4.51 < -8 -6 4 -2 1.29 2.05 2.72 < -8 -6 4 -1 127.58 121.24 3.14 o -8 -6 4 0 800.93 725.47 5.56 o -8 -6 4 1 62.93 59.09 2.69 o -8 -6 4 2 2.70 2.91 1.76 < -6 -6 4 -2 0.08 -0.59 2.33 < -6 -6 4 -1 58.83 54.34 2.05 o -6 -6 4 0 2.77 1.24 2.05 < -6 -6 4 1 39.92 37.80 1.46 o -6 -6 4 2 4.35 5.65 1.29 o -4 -6 4 -2 1.01 0.33 1.37 < -4 -6 4 -1 97.23 95.87 1.43 o -4 -6 4 0 1086.42 1074.54 3.69 o -4 -6 4 1 107.37 107.68 1.53 o -4 -6 4 2 3.56 3.10 1.17 < -2 -6 4 -2 2.38 1.94 0.79 < -2 -6 4 -1 72.99 69.37 1.06 o -2 -6 4 0 849.34 862.16 2.86 o -2 -6 4 1 19.92 18.81 1.00 o -2 -6 4 2 1.69 2.18 2.04 < 0 -6 4 -2 0.96 1.62 0.92 < 0 -6 4 -1 0.13 0.84 1.12 < 0 -6 4 0 715.14 757.59 5.72 o 0 -6 4 1 17.38 17.94 1.74 o 0 -6 4 2 0.49 -1.88 2.86 < 2 -6 4 -2 0.01 -1.09 1.45 < 2 -6 4 -1 28.22 29.78 1.74 o 2 -6 4 0 953.11 962.94 5.10 o 2 -6 4 1 17.17 16.35 1.79 o 2 -6 4 2 0.20 0.34 2.29 < 4 -6 4 -2 0.17 0.64 1.10 < 4 -6 4 -1 9.87 9.88 1.45 o 4 -6 4 0 15.56 16.18 1.43 o 4 -6 4 1 47.16 44.44 2.96 o 4 -6 4 2 1.46 -0.08 2.60 < 6 -6 4 -2 0.09 0.14 1.46 < 6 -6 4 -1 20.71 17.41 1.93 o 6 -6 4 0 648.73 616.43 6.34 o 8 -6 4 -2 0.15 0.44 2.46 < -9 -5 4 0 64.51 61.99 2.99 o -9 -5 4 1 80.03 80.50 2.96 o -9 -5 4 2 5.81 6.88 2.30 < -7 -5 4 -2 6.19 6.41 2.26 < -7 -5 4 -1 13.29 10.70 2.54 o -7 -5 4 0 3.09 5.74 1.99 < -7 -5 4 1 3.79 4.26 1.74 < -7 -5 4 2 4.43 3.77 1.42 < -5 -5 4 -2 2.82 3.20 1.71 < -5 -5 4 -1 52.41 51.57 1.73 o -5 -5 4 0 404.45 414.65 2.81 o -5 -5 4 1 51.46 49.49 1.37 o -5 -5 4 2 2.94 2.38 1.12 < -3 -5 4 -2 0.01 -0.11 0.95 < -3 -5 4 -1 50.10 50.75 1.03 o -3 -5 4 0 5.79 7.58 0.89 o -3 -5 4 1 4.51 4.17 0.96 o -3 -5 4 2 0.16 0.45 0.98 < -1 -5 4 -2 0.01 0.59 0.72 < -1 -5 4 -1 16.21 17.12 0.82 o -1 -5 4 0 2162.05 2145.01 4.79 o -1 -5 4 1 0.07 2.13 1.76 < -1 -5 4 2 0.52 1.20 1.90 < 1 -5 4 -2 0.00 -0.54 0.95 < 1 -5 4 -1 0.27 0.67 1.32 < 1 -5 4 0 141.01 141.79 1.98 o 1 -5 4 1 1.63 1.17 1.77 < 1 -5 4 2 0.00 -0.16 1.63 < 3 -5 4 -2 0.15 0.42 0.92 < 3 -5 4 -1 3.74 3.78 0.96 o 3 -5 4 0 342.18 315.68 2.17 o 3 -5 4 1 0.35 0.36 1.49 < 3 -5 4 2 0.00 -0.67 2.12 < 5 -5 4 -2 0.01 0.75 1.09 < 5 -5 4 -1 7.15 6.50 1.21 o 5 -5 4 0 768.86 725.34 5.23 o 5 -5 4 1 1.37 1.32 2.71 < 5 -5 4 2 0.16 0.56 4.25 < 7 -5 4 -2 5.46 5.10 1.59 o 7 -5 4 -1 73.37 68.88 2.15 o -10 -4 4 2 1.70 1.49 3.45 < -8 -4 4 -2 3.63 3.87 2.40 < -8 -4 4 -1 31.54 29.04 2.46 o -8 -4 4 0 27.15 27.29 2.40 o -8 -4 4 1 83.46 84.61 2.68 o -8 -4 4 2 13.01 13.63 1.93 o -6 -4 4 -2 15.61 16.13 1.84 o -6 -4 4 -1 0.51 -0.17 1.65 < -6 -4 4 0 597.06 570.17 4.81 o -6 -4 4 1 101.06 103.10 2.01 o -6 -4 4 2 0.35 1.23 1.26 < -4 -4 4 -2 4.89 5.76 1.20 o -4 -4 4 -1 6.70 8.00 1.38 o -4 -4 4 0 369.96 370.32 2.26 o -4 -4 4 1 66.02 68.96 1.31 o -4 -4 4 2 7.26 7.16 1.07 o -2 -4 4 -2 14.43 14.89 0.78 o -2 -4 4 -1 19.21 18.64 0.84 o -2 -4 4 0 26.91 24.76 0.96 o -2 -4 4 1 55.02 52.37 1.28 o -2 -4 4 2 0.05 -0.30 1.17 < 0 -4 4 -2 3.23 4.50 0.96 o 0 -4 4 -1 0.49 0.86 0.81 < 0 -4 4 0 943.26 956.92 3.60 o 0 -4 4 1 9.83 10.86 1.21 o 0 -4 4 2 0.44 0.90 1.17 < 2 -4 4 -2 1.21 1.91 0.93 < 2 -4 4 -1 28.04 27.96 1.07 o 2 -4 4 0 126.79 131.31 1.65 o 2 -4 4 1 10.68 11.23 1.20 o 2 -4 4 2 0.90 1.49 1.57 < 4 -4 4 -2 1.82 1.06 0.86 < 4 -4 4 -1 18.29 17.05 1.03 o 4 -4 4 0 487.10 462.43 2.73 o 4 -4 4 1 0.69 0.72 2.02 < 4 -4 4 2 0.20 -0.20 2.33 < 6 -4 4 -2 1.16 0.17 1.12 < 6 -4 4 -1 1.10 1.54 1.43 < 6 -4 4 0 218.86 217.04 2.82 o 6 -4 4 1 15.85 13.61 2.77 o 8 -4 4 -2 1.72 3.41 2.01 < 8 -4 4 -1 29.44 24.97 3.41 o -9 -3 4 -2 0.28 1.59 2.69 < -9 -3 4 -1 58.12 57.89 2.96 o -9 -3 4 0 36.17 37.42 3.13 o -9 -3 4 1 11.14 9.91 2.35 o -9 -3 4 2 9.29 9.20 2.21 o -7 -3 4 -2 9.34 7.79 1.76 o -7 -3 4 -1 213.75 208.21 3.61 o -7 -3 4 0 903.33 875.17 5.41 o -7 -3 4 1 18.07 18.95 2.04 o -7 -3 4 2 2.48 3.55 1.46 < -5 -3 4 -2 0.54 -1.01 1.62 < -5 -3 4 -1 121.23 121.78 1.88 o -5 -3 4 0 154.17 155.78 2.09 o -5 -3 4 1 14.59 14.44 1.12 o -5 -3 4 2 0.06 -0.48 1.09 < -3 -3 4 -2 0.01 1.07 1.15 < -3 -3 4 -1 186.34 191.36 1.43 o -3 -3 4 0 3126.36 3066.72 5.24 o -3 -3 4 1 140.88 134.00 1.53 o -3 -3 4 2 2.90 2.60 1.48 < -1 -3 4 -2 0.03 -0.11 0.50 < -1 -3 4 -1 62.45 59.15 0.78 o -1 -3 4 0 271.92 290.84 1.68 o -1 -3 4 1 7.44 7.36 1.40 o -1 -3 4 2 0.60 1.99 1.21 < 1 -3 4 -2 2.53 2.36 0.79 < 1 -3 4 -1 33.99 32.26 1.37 o 1 -3 4 0 1919.22 1877.21 5.53 o 1 -3 4 1 21.91 21.50 1.23 o 1 -3 4 2 0.28 -0.02 1.42 < 3 -3 4 -2 0.09 0.22 0.79 < 3 -3 4 -1 2.21 2.60 0.82 o 3 -3 4 0 2099.53 2060.21 4.25 o 3 -3 4 1 0.03 -0.53 1.15 < 3 -3 4 2 0.00 -0.26 1.79 < 5 -3 4 -2 1.18 1.21 1.00 < 5 -3 4 -1 9.76 8.64 1.31 o 5 -3 4 0 129.56 120.78 2.10 o 5 -3 4 1 6.08 7.25 2.43 < 5 -3 4 2 0.89 2.01 3.13 < 7 -3 4 -2 0.81 0.51 1.62 < 7 -3 4 -1 0.14 0.36 1.74 < 7 -3 4 0 702.73 684.78 6.17 o 9 -3 4 -2 0.02 -1.35 2.55 < -10 -2 4 -1 2.69 2.69 5.76 < -10 -2 4 0 43.27 49.11 3.52 o -10 -2 4 1 24.51 27.29 3.16 o -10 -2 4 2 8.77 11.11 2.85 o -8 -2 4 -2 11.47 14.66 2.33 o -8 -2 4 -1 0.09 -0.31 2.18 < -8 -2 4 0 347.16 351.79 3.88 o -8 -2 4 1 214.24 228.57 4.50 o -8 -2 4 2 13.31 14.02 1.94 o -6 -2 4 -2 1.48 0.53 1.43 < -6 -2 4 -1 18.68 19.22 1.48 o -6 -2 4 0 188.56 194.04 2.68 o -6 -2 4 1 28.33 32.04 1.66 o -6 -2 4 2 8.96 8.62 1.31 o -4 -2 4 -2 34.42 34.38 1.29 o -4 -2 4 -1 30.20 31.20 1.21 o -4 -2 4 0 19.00 16.79 1.17 o -4 -2 4 1 108.26 106.60 1.46 o -4 -2 4 2 0.05 1.03 1.14 < -2 -2 4 -2 0.02 -0.53 0.75 < -2 -2 4 -1 12.73 12.95 0.65 o -2 -2 4 0 161.85 150.00 1.37 o -2 -2 4 1 26.46 27.01 1.43 o -2 -2 4 2 0.86 1.09 0.95 < 0 -2 4 -2 4.01 2.22 0.75 < 0 -2 4 -1 72.02 69.64 1.29 o 0 -2 4 0 708.14 724.85 4.10 o 0 -2 4 1 0.54 0.31 0.96 < 0 -2 4 2 2.87 2.83 1.07 < 2 -2 4 -2 0.01 -0.93 1.07 < 2 -2 4 -1 3.32 2.92 1.00 < 2 -2 4 0 2.57 3.66 1.26 < 2 -2 4 1 0.04 -0.36 1.17 < 2 -2 4 2 0.49 0.36 1.62 < 4 -2 4 -2 2.02 0.70 1.04 < 4 -2 4 -1 4.73 3.92 1.03 o 4 -2 4 0 1460.66 1440.90 4.66 o 4 -2 4 1 0.02 -0.58 2.04 < 4 -2 4 2 0.01 -0.44 2.08 < 6 -2 4 -2 1.09 1.56 1.34 < 6 -2 4 -1 14.74 13.94 1.54 o 6 -2 4 0 7.15 9.30 2.01 o 6 -2 4 1 0.19 1.63 3.34 < 8 -2 4 -2 5.58 4.71 1.85 < 8 -2 4 -1 52.77 50.67 2.69 o -9 -1 4 -2 2.23 2.04 2.41 < -9 -1 4 -1 84.17 91.78 2.99 o -9 -1 4 0 165.46 155.40 3.71 o -9 -1 4 1 81.57 85.79 3.05 o -9 -1 4 2 6.17 8.21 1.93 o -7 -1 4 -2 8.52 8.35 1.71 o -7 -1 4 -1 16.82 18.70 1.66 o -7 -1 4 0 13.97 15.68 1.82 o -7 -1 4 1 52.49 53.22 2.37 o -7 -1 4 2 3.11 3.38 1.40 < -5 -1 4 -2 1.01 0.87 1.57 < -5 -1 4 -1 183.66 189.00 2.06 o -5 -1 4 0 1071.06 1047.43 5.53 o -5 -1 4 1 292.84 278.36 2.65 o -5 -1 4 2 12.22 12.68 1.38 o -3 -1 4 -2 9.78 9.02 0.79 o -3 -1 4 -1 0.50 0.53 0.76 < -3 -1 4 0 3.59 20.21 0.82 o -3 -1 4 1 46.46 46.08 1.39 o -3 -1 4 2 2.20 1.88 0.96 < -1 -1 4 -2 12.93 11.83 0.53 o -1 -1 4 -1 65.14 62.61 1.28 o -1 -1 4 0 3981.57 3777.34 7.02 o -1 -1 4 1 127.78 127.39 1.46 o -1 -1 4 2 0.22 -0.86 1.03 < 1 -1 4 -2 0.34 0.26 0.61 < 1 -1 4 -1 0.86 0.34 0.64 < 1 -1 4 0 6.51 13.88 0.82 o 1 -1 4 1 8.32 10.38 1.10 o 1 -1 4 2 0.27 0.17 1.38 < 3 -1 4 -2 1.13 1.57 1.00 < 3 -1 4 -1 0.66 0.72 1.52 < 3 -1 4 0 431.30 433.46 2.90 o 3 -1 4 1 0.98 1.80 1.63 < 3 -1 4 2 0.94 2.88 2.35 < 5 -1 4 -2 0.16 0.37 1.23 < 5 -1 4 -1 0.83 0.81 1.54 < 5 -1 4 0 128.79 125.54 2.16 o 5 -1 4 1 4.18 5.01 2.41 < 5 -1 4 2 0.08 -1.07 3.56 < 7 -1 4 -2 1.29 0.65 1.76 < 7 -1 4 -1 10.42 8.59 2.12 o 7 -1 4 0 13.83 17.78 2.88 o 9 -1 4 -2 0.73 0.96 2.13 < -10 0 4 -2 3.87 3.94 5.76 < -10 0 4 -1 19.24 18.33 3.19 o -10 0 4 0 5.80 9.79 2.97 o -10 0 4 1 14.35 17.22 2.86 o -10 0 4 2 12.64 10.46 2.83 o -8 0 4 -2 15.08 18.34 2.04 o -8 0 4 -1 130.45 129.81 2.72 o -8 0 4 0 1132.73 1150.49 7.04 o -8 0 4 1 5.39 5.63 2.13 < -8 0 4 2 5.71 5.21 2.02 < -6 0 4 -2 9.49 10.60 1.46 o -6 0 4 -1 82.58 84.30 1.95 o -6 0 4 0 34.85 35.88 1.93 o -6 0 4 1 0.07 0.12 1.60 < -6 0 4 2 1.02 0.44 1.43 < -4 0 4 -2 2.94 3.39 1.15 < -4 0 4 -1 224.30 222.92 2.10 o -4 0 4 0 1527.89 1552.44 4.06 o -4 0 4 1 0.89 1.57 1.10 < -4 0 4 2 2.95 1.14 1.62 < -2 0 4 -2 0.81 0.67 0.82 < -2 0 4 -1 164.32 161.05 1.78 o -2 0 4 0 1126.31 1132.25 8.57 o -2 0 4 1 23.93 24.46 1.20 o -2 0 4 2 1.65 2.13 1.18 < 0 0 4 -1 61.55 62.76 1.32 o 0 0 4 0 1799.92 1821.69 4.87 o 0 0 4 1 2.41 2.74 1.04 < 0 0 4 2 0.13 0.68 1.20 < 2 0 4 -2 1.66 0.51 0.87 < 2 0 4 -1 3.83 2.96 0.98 o 2 0 4 0 2071.10 2205.26 6.29 o 2 0 4 1 3.46 4.39 1.65 < 2 0 4 2 0.10 0.40 1.91 < 4 0 4 -2 1.02 0.68 1.62 < 4 0 4 -1 1.31 3.17 1.70 < 4 0 4 0 107.36 110.06 2.35 o 4 0 4 1 6.37 5.99 1.96 o 4 0 4 2 1.21 1.71 2.64 < 6 0 4 -2 2.00 1.23 1.73 < 6 0 4 -1 7.22 5.24 2.26 < 6 0 4 0 1805.77 1773.72 7.88 o 6 0 4 1 3.39 2.46 2.33 < 8 0 4 -2 2.82 1.32 2.57 < 8 0 4 -1 16.21 15.75 2.38 o -9 1 4 -2 3.71 5.83 2.40 < -9 1 4 -1 10.53 13.07 2.36 o -9 1 4 0 8.60 8.49 2.21 o -9 1 4 1 96.19 105.46 4.08 o -9 1 4 2 8.32 8.35 2.43 o -7 1 4 -2 8.35 12.48 1.77 o -7 1 4 -1 0.17 0.62 1.65 < -7 1 4 0 261.83 269.57 2.56 o -7 1 4 1 80.77 81.76 2.52 o -7 1 4 2 11.62 10.42 1.74 o -5 1 4 -2 15.76 17.24 1.34 o -5 1 4 -1 1.68 3.25 1.40 < -5 1 4 0 8.24 20.71 1.09 o -5 1 4 1 275.00 263.34 2.93 o -5 1 4 2 8.46 8.76 1.54 o -3 1 4 -2 5.45 7.02 0.84 o -3 1 4 -1 39.43 37.05 0.68 o -3 1 4 0 1201.92 1138.96 4.44 o -3 1 4 1 8.02 8.98 1.32 o -3 1 4 2 0.04 -0.06 1.04 < -1 1 4 -1 7.06 7.37 0.96 o -1 1 4 0 777.01 775.19 2.99 o -1 1 4 1 96.81 97.41 1.51 o -1 1 4 2 0.23 0.86 1.15 < 1 1 4 -2 0.84 1.12 0.65 < 1 1 4 -1 20.57 19.00 0.75 o 1 1 4 0 595.25 578.05 2.89 o 1 1 4 1 2.54 2.05 1.21 < 1 1 4 2 1.84 0.36 1.57 < 3 1 4 -2 0.14 1.23 0.86 < 3 1 4 -1 3.84 3.42 1.14 o 3 1 4 0 30.85 33.92 1.87 o 3 1 4 1 3.02 3.13 1.84 < 3 1 4 2 0.43 2.07 2.41 < 5 1 4 -2 0.57 -0.98 2.24 < 5 1 4 -1 19.08 22.20 2.26 o 5 1 4 0 69.66 77.29 2.83 o 5 1 4 1 24.20 22.44 2.85 o 5 1 4 2 0.18 1.49 2.96 < 7 1 4 -2 5.50 6.94 2.75 < 7 1 4 -1 7.97 8.62 2.29 o 7 1 4 0 17.65 14.49 2.55 o 9 1 4 -2 0.55 -0.47 2.91 < -10 2 4 -2 3.52 4.26 3.81 < -10 2 4 -1 32.84 36.10 3.28 o -10 2 4 0 204.03 206.50 5.25 o -10 2 4 1 0.18 1.93 3.34 < -10 2 4 2 1.10 -1.73 3.10 < -8 2 4 -2 0.35 -0.08 1.77 < -8 2 4 -1 190.68 197.76 3.04 o -8 2 4 0 22.60 25.22 1.99 o -8 2 4 1 185.53 191.36 3.96 o -8 2 4 2 4.84 6.75 2.02 o -6 2 4 -2 0.01 0.11 1.28 < -6 2 4 -1 90.16 94.52 1.93 o -6 2 4 0 1193.94 1150.13 4.31 o -6 2 4 1 20.80 19.14 1.70 o -6 2 4 2 0.46 1.18 1.56 < -4 2 4 -2 0.93 0.42 1.31 < -4 2 4 -1 215.35 211.37 1.65 o -4 2 4 0 715.39 682.82 2.69 o -4 2 4 1 242.45 233.16 2.76 o -4 2 4 2 11.54 10.98 1.51 o -2 2 4 -2 5.36 4.45 0.61 o -2 2 4 -1 165.07 154.21 1.64 o -2 2 4 0 452.36 429.07 3.28 o -2 2 4 1 105.72 104.17 1.35 o -2 2 4 2 0.81 0.33 1.23 < 0 2 4 -2 0.14 0.44 1.12 < 0 2 4 -1 2.76 3.10 0.70 o 0 2 4 0 2193.51 2198.33 5.56 o 0 2 4 1 52.49 53.21 1.63 o 0 2 4 2 0.00 0.06 1.56 < 2 2 4 -2 0.95 1.06 1.01 < 2 2 4 -1 33.58 34.83 1.43 o 2 2 4 0 207.24 209.88 2.68 o 2 2 4 1 33.37 36.18 1.81 o 2 2 4 2 0.01 2.30 2.01 < 4 2 4 -2 0.06 0.45 0.98 < 4 2 4 -1 4.11 4.39 1.60 < 4 2 4 0 2160.86 2169.06 8.26 o 4 2 4 1 0.90 -0.50 2.50 < 4 2 4 2 1.51 3.33 2.72 < 6 2 4 -2 1.40 1.98 1.65 < 6 2 4 -1 6.89 4.62 2.99 < 6 2 4 0 4.09 5.35 2.61 < 6 2 4 1 3.93 4.90 3.44 < 8 2 4 -2 0.00 -0.89 2.44 < 8 2 4 -1 12.11 13.60 3.58 o -9 3 4 -2 7.42 10.42 2.15 o -9 3 4 -1 14.46 16.76 2.10 o -9 3 4 0 1.27 2.27 2.47 < -9 3 4 1 66.47 68.79 3.44 o -9 3 4 2 39.91 39.98 2.49 o -7 3 4 -2 25.90 28.51 2.21 o -7 3 4 -1 12.72 13.51 1.52 o -7 3 4 0 262.71 259.93 2.74 o -7 3 4 1 95.08 95.65 2.37 o -7 3 4 2 4.20 4.08 1.74 < -5 3 4 -2 5.90 8.00 1.14 o -5 3 4 -1 205.11 197.09 2.52 o -5 3 4 0 0.40 -0.96 1.09 < -5 3 4 1 2.75 3.70 1.65 < -5 3 4 2 4.00 2.60 1.59 < -3 3 4 -2 21.34 20.32 0.92 o -3 3 4 -1 21.96 21.82 1.17 o -3 3 4 0 1389.76 1339.32 5.64 o -3 3 4 1 105.14 101.44 2.06 o -3 3 4 2 2.95 1.03 1.26 < -1 3 4 -2 4.89 5.41 1.01 o -1 3 4 -1 134.29 131.07 1.96 o -1 3 4 0 1.68 2.08 0.95 < -1 3 4 1 3.52 4.12 1.20 o -1 3 4 2 1.00 3.10 1.65 < 1 3 4 -2 0.23 -0.09 0.54 < 1 3 4 -1 32.26 33.53 1.57 o 1 3 4 0 907.37 880.09 4.43 o 1 3 4 1 8.81 10.04 1.63 o 1 3 4 2 0.06 1.06 1.84 < 3 3 4 -2 4.58 2.83 1.48 < 3 3 4 -1 3.60 4.45 1.49 < 3 3 4 0 1521.53 1601.00 8.14 o 3 3 4 1 7.01 7.56 2.02 o 3 3 4 2 0.06 -1.09 2.18 < 5 3 4 -2 2.61 0.96 2.44 < 5 3 4 -1 1.05 1.15 2.12 < 5 3 4 0 97.69 90.31 3.89 o 5 3 4 1 5.22 8.45 3.50 < 7 3 4 -2 3.82 3.47 3.10 < 7 3 4 -1 41.38 41.86 2.93 o -10 4 4 -1 41.64 46.92 4.15 o -10 4 4 0 0.22 1.40 3.33 < -10 4 4 1 69.49 67.25 3.16 o -10 4 4 2 7.14 7.00 2.43 < -8 4 4 -2 1.53 3.72 2.05 < -8 4 4 -1 7.87 11.03 1.96 o -8 4 4 0 552.15 527.87 4.67 o -8 4 4 1 54.79 53.66 2.37 o -8 4 4 2 2.30 2.58 2.33 < -6 4 4 -2 0.15 1.20 1.45 < -6 4 4 -1 46.07 48.07 1.65 o -6 4 4 0 12.78 11.00 1.23 o -6 4 4 1 146.87 140.91 2.96 o -6 4 4 2 25.90 27.12 1.95 o -4 4 4 -2 23.73 25.36 1.23 o -4 4 4 -1 5.03 5.48 1.20 o -4 4 4 0 115.24 108.24 2.43 o -4 4 4 1 91.66 89.94 2.10 o -4 4 4 2 0.77 -0.31 1.54 < -2 4 4 -2 0.17 0.03 0.93 < -2 4 4 -1 6.07 5.69 1.21 o -2 4 4 0 1621.72 1487.99 4.87 o -2 4 4 1 114.93 112.48 1.87 o -2 4 4 2 4.95 4.47 1.42 o 0 4 4 -2 9.38 8.95 0.75 o 0 4 4 -1 15.77 15.64 1.31 o 0 4 4 0 1.18 3.06 1.49 < 0 4 4 1 37.78 35.71 1.96 o 0 4 4 2 0.01 0.93 1.68 < 2 4 4 -2 0.16 -1.26 1.23 < 2 4 4 -1 23.44 22.62 1.43 o 2 4 4 0 875.80 850.19 5.66 o 2 4 4 1 11.19 10.92 2.60 o 2 4 4 2 1.31 -0.28 2.26 < 4 4 4 -2 0.05 0.12 1.34 < 4 4 4 -1 0.71 0.47 1.77 < 4 4 4 0 178.93 180.46 4.47 o 4 4 4 1 10.83 10.32 2.29 o 4 4 4 2 0.06 0.14 2.94 < 6 4 4 -2 0.01 -1.82 2.77 < 6 4 4 -1 0.25 1.10 2.41 < 6 4 4 0 212.12 201.89 4.19 o 8 4 4 -2 0.78 0.17 2.80 < -9 5 4 -2 16.75 18.36 2.86 o -9 5 4 -1 102.77 110.14 3.25 o -9 5 4 0 175.97 164.13 3.46 o -9 5 4 1 31.41 29.19 2.79 o -9 5 4 2 0.44 1.63 2.61 < -7 5 4 -2 0.06 0.02 1.77 < -7 5 4 -1 124.88 126.47 2.30 o -7 5 4 0 12.61 12.04 1.56 o -7 5 4 1 0.10 -0.47 2.07 < -7 5 4 2 4.37 2.75 2.29 < -5 5 4 -2 8.53 8.96 1.29 o -5 5 4 -1 152.62 149.41 1.92 o -5 5 4 0 934.12 877.86 4.57 o -5 5 4 1 59.72 61.10 2.02 o -5 5 4 2 0.04 -0.26 1.63 < -3 5 4 -2 0.01 0.73 1.32 < -3 5 4 -1 152.01 154.22 2.23 o -3 5 4 0 28.21 26.34 1.51 o -3 5 4 1 68.33 69.84 1.90 o -3 5 4 2 0.80 1.28 1.43 < -1 5 4 -2 1.81 0.50 1.06 < -1 5 4 -1 147.04 137.15 2.04 o -1 5 4 0 3145.92 3141.95 7.71 o -1 5 4 1 33.70 30.81 1.60 o -1 5 4 2 0.92 -0.65 2.44 < 1 5 4 -2 1.53 1.03 0.95 < 1 5 4 -1 39.16 36.21 1.76 o 1 5 4 0 492.98 469.85 4.07 o 1 5 4 1 75.04 79.07 2.61 o 1 5 4 2 0.25 1.51 2.22 < 3 5 4 -2 0.43 -0.03 1.51 < 3 5 4 -1 8.25 9.71 1.99 o 3 5 4 0 686.35 730.11 4.90 o 3 5 4 1 1.30 1.60 2.74 < 3 5 4 2 1.87 1.77 3.06 < 5 5 4 -2 5.29 6.04 2.02 < 5 5 4 -1 12.20 13.40 2.89 o 5 5 4 0 739.61 708.38 6.51 o 5 5 4 1 0.89 0.51 3.62 < 7 5 4 -2 0.06 -0.81 2.21 < 7 5 4 -1 11.79 9.96 2.93 o -8 6 4 -2 13.30 16.65 2.15 o -8 6 4 -1 4.01 3.19 1.91 < -8 6 4 0 259.87 259.79 3.54 o -8 6 4 1 128.49 131.66 4.90 o -8 6 4 2 14.67 17.74 4.03 o -6 6 4 -2 19.72 22.89 1.45 o -6 6 4 -1 3.80 4.73 1.38 o -6 6 4 0 324.10 315.85 3.19 o -6 6 4 1 53.43 52.69 2.19 o -6 6 4 2 4.79 4.82 1.93 < -4 6 4 -2 6.24 8.57 1.12 o -4 6 4 -1 29.39 29.64 1.48 o -4 6 4 0 32.78 37.81 1.74 o -4 6 4 1 202.98 203.99 2.73 o -4 6 4 2 7.42 7.00 3.50 < -2 6 4 -2 18.14 19.28 1.32 o -2 6 4 -1 15.51 16.23 1.37 o -2 6 4 0 20.91 20.48 1.63 o -2 6 4 1 0.29 0.23 1.48 < -2 6 4 2 0.29 1.04 1.63 < 0 6 4 -2 1.16 -0.78 1.17 < 0 6 4 -1 91.26 93.31 1.96 o 0 6 4 0 50.85 52.60 1.71 o 0 6 4 1 25.15 23.20 1.95 o 0 6 4 2 0.00 1.43 2.82 < 2 6 4 -2 5.63 6.43 2.55 < 2 6 4 -1 1.09 -0.78 3.22 < 2 6 4 0 297.49 290.22 4.83 o 2 6 4 1 13.26 13.88 2.60 o 2 6 4 2 0.00 0.25 2.52 < 4 6 4 -2 0.11 -0.42 1.84 < 4 6 4 -1 9.85 11.34 2.33 o 4 6 4 0 10.73 13.29 2.89 o 4 6 4 1 8.63 11.12 3.05 o 6 6 4 -2 3.41 2.96 3.13 < 6 6 4 -1 31.45 24.57 3.84 o 8 6 4 -2 5.24 2.63 3.66 < -9 7 4 -1 58.37 60.23 5.98 o -7 7 4 -2 0.89 -0.59 2.07 < -7 7 4 -1 25.07 26.44 2.19 o -7 7 4 0 229.28 219.67 3.91 o -7 7 4 1 82.12 81.78 4.42 o -7 7 4 2 3.82 3.91 3.89 < -5 7 4 -2 1.79 1.54 1.28 < -5 7 4 -1 116.68 116.91 2.21 o -5 7 4 0 104.90 94.24 2.29 o -5 7 4 1 161.83 158.34 2.29 o -5 7 4 2 6.44 7.09 2.41 < -3 7 4 -2 0.03 -0.08 1.48 < -3 7 4 -1 17.28 15.98 1.24 o -3 7 4 0 1383.51 1338.36 7.35 o -3 7 4 1 8.40 5.87 2.16 < -3 7 4 2 1.08 1.48 1.90 < -1 7 4 -2 1.52 0.53 1.54 < -1 7 4 -1 38.89 40.37 1.54 o -1 7 4 0 8.03 10.92 1.48 o -1 7 4 1 207.05 214.78 3.12 o -1 7 4 2 3.72 2.08 4.09 < 1 7 4 -2 0.09 -0.47 1.28 < 1 7 4 -1 2.39 2.68 2.15 < 1 7 4 0 1402.10 1299.73 8.86 o 1 7 4 1 2.14 1.71 2.83 < 1 7 4 2 0.04 1.14 2.69 < 3 7 4 -2 1.52 1.73 1.87 < 3 7 4 -1 0.34 1.21 2.19 < 3 7 4 0 125.25 117.46 2.86 o 3 7 4 1 51.07 51.14 4.33 o 5 7 4 -2 0.05 -0.42 1.91 < 5 7 4 -1 18.06 19.15 2.86 o 5 7 4 0 225.80 212.41 4.53 o 7 7 4 -2 0.58 -0.33 2.89 < -8 8 4 -2 4.82 6.85 3.19 < -8 8 4 -1 69.50 71.68 5.56 o -6 8 4 -2 8.74 11.26 2.50 o -6 8 4 -1 46.99 43.60 3.98 o -6 8 4 0 446.84 477.83 7.89 o -6 8 4 1 57.98 56.68 4.34 o -6 8 4 2 7.37 7.65 4.54 < -4 8 4 -2 5.15 5.04 1.84 < -4 8 4 -1 122.37 120.51 2.76 o -4 8 4 0 101.85 107.62 2.97 o -4 8 4 1 55.52 57.66 4.40 o -4 8 4 2 1.13 0.48 2.24 < -2 8 4 -2 0.43 -1.23 1.74 < -2 8 4 -1 155.36 151.71 2.62 o -2 8 4 0 307.48 297.55 3.65 o -2 8 4 1 3.58 2.97 2.19 < -2 8 4 2 0.42 -0.96 2.38 < 0 8 4 -2 4.49 5.40 1.14 o 0 8 4 -1 1.57 2.26 1.52 < 0 8 4 0 529.73 547.95 4.90 o 0 8 4 1 6.46 5.94 2.88 < 0 8 4 2 0.60 0.79 3.27 < 2 8 4 -2 0.23 -2.15 2.22 < 2 8 4 -1 82.02 79.43 3.28 o 2 8 4 0 247.79 244.29 4.05 o 2 8 4 1 38.56 38.96 2.71 o 4 8 4 -2 1.61 2.26 1.96 < 4 8 4 -1 0.59 2.18 2.68 < 4 8 4 0 1361.34 1360.75 9.12 o 6 8 4 -2 4.70 3.70 3.00 < 6 8 4 -1 1.27 1.56 5.41 < -7 9 4 -2 7.74 9.43 3.11 o -7 9 4 -1 38.75 40.60 4.86 o -7 9 4 1 125.52 115.51 5.82 o -5 9 4 -2 1.65 0.61 3.39 < -5 9 4 -1 35.14 33.42 3.98 o -5 9 4 0 97.04 94.08 4.93 o -5 9 4 1 6.57 7.59 4.31 < -5 9 4 2 4.45 0.96 3.14 < -3 9 4 -2 15.30 20.38 3.53 o -3 9 4 -1 16.19 12.07 3.66 o -3 9 4 0 9.19 5.49 2.72 < -3 9 4 1 306.63 302.03 4.11 o -3 9 4 2 4.66 4.33 2.64 < -1 9 4 -2 1.72 0.19 1.66 < -1 9 4 -1 34.87 38.61 2.24 o -1 9 4 0 379.12 376.82 4.41 o -1 9 4 1 0.62 1.70 2.44 < -1 9 4 2 0.01 -0.65 3.36 < 1 9 4 -2 0.20 -0.47 1.91 < 1 9 4 -1 1.09 -0.81 2.52 < 1 9 4 0 0.82 -0.68 2.99 < 1 9 4 1 61.42 55.00 3.14 o 3 9 4 -2 3.32 1.21 2.26 < 3 9 4 -1 1.31 1.28 2.21 < 3 9 4 0 28.95 29.74 2.79 o 5 9 4 -2 0.04 -0.22 2.78 < 5 9 4 -1 24.36 25.39 3.38 o -6 10 4 -2 3.12 0.72 4.09 < -6 10 4 -1 119.18 115.32 5.70 o -6 10 4 0 50.12 43.40 5.07 o -6 10 4 1 83.68 86.35 5.95 o -4 10 4 -2 0.48 -1.28 3.94 < -4 10 4 -1 58.56 70.48 5.07 o -4 10 4 0 93.00 88.33 3.72 o -4 10 4 1 13.57 15.70 2.77 o -4 10 4 2 0.53 2.52 4.89 < -2 10 4 -2 4.00 3.22 1.87 < -2 10 4 -1 8.04 7.65 2.21 o -2 10 4 0 808.37 777.29 6.14 o -2 10 4 1 65.71 65.46 3.17 o 0 10 4 -2 2.62 3.80 2.02 < 0 10 4 -1 144.60 147.18 3.39 o 0 10 4 0 148.63 136.23 4.23 o 0 10 4 1 73.41 73.10 4.08 o 2 10 4 -2 2.42 1.07 2.88 < 2 10 4 -1 4.48 2.69 2.32 < 2 10 4 0 870.19 811.42 6.99 o 4 10 4 -2 0.70 0.54 2.04 < 4 10 4 -1 3.69 4.67 3.14 < -5 11 4 -2 15.05 19.31 4.87 o -5 11 4 -1 3.84 3.78 4.93 < -3 11 4 -2 2.30 1.88 2.74 < -3 11 4 -1 64.02 61.29 3.55 o -3 11 4 0 9.39 8.76 2.68 o -3 11 4 1 1.48 0.78 5.23 < -1 11 4 -2 0.92 2.99 2.22 < -1 11 4 -1 29.33 27.42 2.61 o -1 11 4 0 340.69 333.17 4.68 o 1 11 4 -2 5.92 7.36 3.03 < 1 11 4 -1 21.37 18.53 3.44 o 1 11 4 0 126.89 123.53 4.75 o 3 11 4 -2 0.36 0.48 2.38 < 3 11 4 -1 18.59 17.41 3.17 o -4 12 4 -2 0.02 0.58 3.19 < -2 12 4 -2 5.81 6.94 2.60 < -2 12 4 -1 19.28 19.70 2.91 o 0 12 4 -2 0.16 -0.86 2.58 < 0 12 4 -1 21.03 17.54 3.63 o 2 12 4 -2 1.33 1.42 3.42 < -1 13 4 -2 0.70 0.14 2.92 < 1 13 4 -2 0.04 5.01 5.46 < -4 -10 5 -2 3.06 2.35 4.73 < -4 -10 5 -1 17.24 14.97 3.44 o -4 -10 5 0 70.82 65.51 5.51 o -2 -10 5 -2 0.22 0.09 3.19 < -2 -10 5 -1 2.04 3.05 4.53 < -2 -10 5 0 0.30 0.72 4.64 < 0 -10 5 -2 0.14 0.31 4.31 < 0 -10 5 -1 28.53 26.86 4.51 o 0 -10 5 0 68.62 73.40 5.04 o 2 -10 5 -2 0.03 -0.54 4.03 < -5 -9 5 -2 6.62 4.56 2.82 < -5 -9 5 -1 39.01 36.49 2.96 o -5 -9 5 0 339.57 344.86 5.74 o -5 -9 5 1 115.82 110.18 5.57 o -3 -9 5 -2 0.68 0.70 2.38 < -3 -9 5 -1 3.55 3.69 2.49 < -3 -9 5 0 49.25 49.77 5.15 o -1 -9 5 -2 11.28 11.51 2.89 o -1 -9 5 -1 0.10 1.45 3.95 < -1 -9 5 0 355.77 347.41 7.51 o 1 -9 5 -2 0.37 0.79 3.77 < 1 -9 5 -1 4.22 5.09 3.72 < 1 -9 5 0 349.81 375.55 7.31 o 3 -9 5 -2 1.23 -0.31 4.05 < 3 -9 5 -1 17.25 21.05 4.54 o -6 -8 5 -2 13.48 12.79 3.35 o -6 -8 5 -1 101.76 93.24 2.93 o -6 -8 5 0 75.08 65.24 2.32 o -6 -8 5 1 0.47 1.28 2.22 < -6 -8 5 2 0.68 -0.16 2.92 < -4 -8 5 -2 0.01 -0.89 1.62 < -4 -8 5 -1 1.47 1.43 1.91 < -4 -8 5 0 29.01 29.55 2.46 o -4 -8 5 1 0.35 -0.34 2.50 < -2 -8 5 -2 0.71 -0.96 1.73 < -2 -8 5 -1 195.33 190.17 3.29 o -2 -8 5 0 634.23 664.76 9.71 o 0 -8 5 -2 0.04 3.70 3.62 < 0 -8 5 -1 5.61 6.35 3.97 < 0 -8 5 0 80.73 77.03 4.51 o 2 -8 5 -2 0.00 -0.62 3.56 < 2 -8 5 -1 17.55 18.25 2.65 o 2 -8 5 0 1106.60 1224.07 12.20 o 2 -8 5 1 31.93 33.05 4.47 o 4 -8 5 -2 1.68 2.19 2.60 < 4 -8 5 -1 6.44 8.17 4.06 < -7 -7 5 -2 0.56 1.32 4.53 < -7 -7 5 -1 64.32 58.02 2.66 o -7 -7 5 0 185.97 174.18 2.82 o -7 -7 5 1 118.49 108.50 2.37 o -7 -7 5 2 12.99 13.32 1.96 o -5 -7 5 -2 7.19 6.01 1.60 o -5 -7 5 -1 15.44 13.18 1.62 o -5 -7 5 0 91.59 92.89 1.82 o -5 -7 5 1 9.96 10.67 1.56 o -5 -7 5 2 0.54 0.45 1.48 < -3 -7 5 -2 3.00 3.41 1.15 < -3 -7 5 -1 4.69 4.61 1.15 o -3 -7 5 0 659.63 687.02 3.68 o -3 -7 5 1 111.08 116.03 2.68 o -3 -7 5 2 2.97 2.26 2.54 < -1 -7 5 -2 0.03 -0.51 1.14 < -1 -7 5 -1 3.76 3.61 1.49 < -1 -7 5 0 160.17 176.07 3.81 o -1 -7 5 1 0.45 1.57 3.56 < -1 -7 5 2 0.08 -0.96 3.81 < 1 -7 5 -2 1.68 0.50 3.10 < 1 -7 5 -1 1.51 2.68 3.13 < 1 -7 5 1 8.29 8.32 3.91 < 1 -7 5 2 0.24 0.73 4.06 < 3 -7 5 -2 0.00 -0.95 1.80 < 3 -7 5 -1 14.93 15.40 3.55 o 3 -7 5 0 9.59 11.23 3.64 o 3 -7 5 1 0.08 1.45 3.67 < 5 -7 5 -2 0.37 0.45 3.58 < 5 -7 5 -1 0.71 -0.50 3.78 < -8 -6 5 0 1.03 1.00 3.17 < -8 -6 5 1 0.14 -0.33 2.55 < -8 -6 5 2 0.62 -0.12 2.29 < -6 -6 5 -2 2.32 2.80 1.70 < -6 -6 5 -1 44.80 44.65 1.76 o -6 -6 5 0 272.14 251.50 2.49 o -6 -6 5 1 67.77 64.09 1.84 o -6 -6 5 2 0.64 -0.39 1.52 < -4 -6 5 -2 0.27 0.44 1.18 < -4 -6 5 -1 67.25 66.89 1.53 o -4 -6 5 0 765.06 767.07 3.39 o -4 -6 5 1 1.87 2.44 1.34 < -4 -6 5 2 0.32 0.05 2.07 < -2 -6 5 -2 8.95 9.15 1.03 o -2 -6 5 -1 0.29 0.09 1.03 < -2 -6 5 0 98.41 102.50 1.98 o -2 -6 5 1 34.51 38.70 2.66 o -2 -6 5 2 0.29 -4.03 3.73 < 0 -6 5 -2 0.29 0.72 1.26 < 0 -6 5 -1 37.01 34.79 2.46 o 0 -6 5 0 1373.36 1458.44 12.40 o 0 -6 5 1 21.12 22.70 3.89 o 2 -6 5 -2 1.89 1.66 1.90 < 2 -6 5 -1 15.17 12.91 3.00 o 2 -6 5 0 2.98 2.83 3.38 < 2 -6 5 1 8.51 9.06 2.55 o 2 -6 5 2 1.75 -1.23 4.06 < 4 -6 5 -2 0.34 1.32 2.22 < 4 -6 5 -1 3.27 2.77 3.30 < 4 -6 5 0 1133.22 1093.30 8.15 o 4 -6 5 1 0.29 -0.53 3.86 < 6 -6 5 -2 0.17 1.84 3.73 < -7 -5 5 -2 19.34 21.08 2.49 o -7 -5 5 -1 65.02 59.65 2.33 o -7 -5 5 0 191.81 187.50 2.41 o -7 -5 5 1 28.69 29.64 1.93 o -7 -5 5 2 4.46 2.88 1.62 < -5 -5 5 -2 1.38 2.92 1.59 < -5 -5 5 -1 32.79 30.76 1.42 o -5 -5 5 0 39.78 38.81 1.45 o -5 -5 5 1 18.70 19.03 1.48 o -5 -5 5 2 0.18 0.96 1.51 < -3 -5 5 -2 6.71 7.17 1.09 o -3 -5 5 -1 107.25 105.50 1.54 o -3 -5 5 0 1015.22 1008.10 3.86 o -3 -5 5 1 5.44 4.03 1.77 < -3 -5 5 2 0.62 0.30 2.40 < -1 -5 5 -2 2.57 3.28 0.93 o -1 -5 5 -1 15.48 15.23 1.32 o -1 -5 5 0 14.28 17.86 2.21 o -1 -5 5 2 0.41 1.63 2.50 < 1 -5 5 -2 0.09 -0.26 1.46 < 1 -5 5 -1 26.16 25.81 2.24 o 1 -5 5 0 208.44 221.49 3.57 o 1 -5 5 1 6.28 5.73 2.21 < 1 -5 5 2 0.60 -0.12 3.67 < 3 -5 5 -2 0.29 0.73 1.59 < 3 -5 5 -1 12.16 11.47 2.18 o 3 -5 5 0 672.13 648.58 6.06 o 3 -5 5 1 2.24 0.93 2.54 < 5 -5 5 -2 1.61 0.23 1.87 < 5 -5 5 -1 31.51 33.17 2.93 o 5 -5 5 0 154.64 156.06 4.11 o 7 -5 5 -2 1.92 3.38 3.98 < -8 -4 5 -2 1.74 2.86 2.86 < -8 -4 5 -1 57.19 58.17 2.85 o -8 -4 5 0 383.72 354.23 4.07 o -8 -4 5 1 162.26 156.97 2.57 o -8 -4 5 2 2.02 2.86 1.71 < -6 -4 5 -2 0.69 0.90 2.02 < -6 -4 5 -1 10.85 10.88 1.77 o -6 -4 5 0 132.70 130.90 2.13 o -6 -4 5 1 45.59 46.50 1.68 o -6 -4 5 2 9.72 10.72 1.68 o -4 -4 5 -2 9.38 9.69 1.20 o -4 -4 5 -1 35.65 34.05 1.28 o -4 -4 5 0 38.09 43.49 1.42 o -4 -4 5 1 178.58 179.23 2.23 o -4 -4 5 2 2.04 2.72 1.91 < -2 -4 5 -2 1.91 2.41 0.92 < -2 -4 5 -1 7.46 7.97 1.06 o -2 -4 5 0 571.00 581.16 4.28 o -2 -4 5 1 45.92 51.03 2.66 o -2 -4 5 2 0.53 1.60 1.80 < 0 -4 5 -2 3.96 4.29 1.34 o 0 -4 5 -1 0.49 1.06 1.38 < 0 -4 5 0 64.77 72.60 2.65 o 0 -4 5 1 14.11 15.26 1.84 o 0 -4 5 2 0.16 0.45 2.52 < 2 -4 5 -2 0.25 0.31 1.23 < 2 -4 5 -1 7.51 7.62 1.57 o 2 -4 5 0 406.08 393.61 3.65 o 2 -4 5 1 9.22 10.52 2.33 o 2 -4 5 2 0.16 1.71 3.97 < 4 -4 5 -2 0.40 -0.33 1.26 < 4 -4 5 -1 0.40 -0.81 1.91 < 4 -4 5 0 9.62 9.43 2.33 o 4 -4 5 1 3.49 3.70 2.49 < 6 -4 5 -2 0.02 -1.17 2.24 < 6 -4 5 -1 6.25 6.88 2.54 < -9 -3 5 0 164.95 157.45 6.87 o -9 -3 5 1 0.12 0.31 2.07 < -9 -3 5 2 1.81 0.73 1.80 < -7 -3 5 -2 2.31 3.97 2.24 < -7 -3 5 -1 61.44 61.26 2.21 o -7 -3 5 0 25.96 21.91 1.80 o -7 -3 5 1 0.12 0.92 1.56 < -7 -3 5 2 0.01 0.59 1.68 < -5 -3 5 -2 0.01 -0.30 1.60 < -5 -3 5 -1 78.91 79.39 1.71 o -5 -3 5 0 635.60 621.62 3.68 o -5 -3 5 1 26.33 24.24 1.52 o -5 -3 5 2 0.01 0.03 1.56 < -3 -3 5 -2 1.39 1.34 0.96 < -3 -3 5 -1 68.30 69.00 1.42 o -3 -3 5 0 69.95 71.44 1.59 o -3 -3 5 1 3.37 3.94 1.66 < -3 -3 5 2 1.93 2.38 1.76 < -1 -3 5 -2 5.61 5.12 0.78 o -1 -3 5 -1 44.38 43.98 1.45 o -1 -3 5 0 868.42 929.18 4.32 o -1 -3 5 1 18.91 20.82 1.84 o -1 -3 5 2 0.01 1.06 2.30 < 1 -3 5 -2 0.03 1.12 1.34 < 1 -3 5 -1 13.25 13.23 1.15 o 1 -3 5 0 1274.10 1306.81 4.68 o 1 -3 5 1 4.64 4.78 1.45 o 1 -3 5 2 0.64 0.28 2.77 < 3 -3 5 -2 0.02 -0.59 1.07 < 3 -3 5 -1 3.73 4.85 1.49 o 3 -3 5 0 173.31 168.94 2.57 o 3 -3 5 1 0.27 -1.46 2.32 < 3 -3 5 2 0.03 1.40 2.64 < 5 -3 5 -2 0.44 0.53 1.56 < 5 -3 5 -1 0.12 0.76 2.24 < 5 -3 5 0 573.67 568.68 5.31 o 5 -3 5 1 5.44 2.78 5.85 < 7 -3 5 -2 0.22 0.19 2.52 < 7 -3 5 -1 5.31 4.29 4.31 < -8 -2 5 -2 1.51 2.68 2.77 < -8 -2 5 -1 0.07 1.56 3.08 < -8 -2 5 0 140.40 146.71 3.02 o -8 -2 5 1 91.16 92.11 2.35 o -8 -2 5 2 23.98 23.42 1.96 o -6 -2 5 -2 30.65 32.02 2.13 o -6 -2 5 -1 39.87 39.81 2.26 o -6 -2 5 0 3.49 2.96 1.45 < -6 -2 5 1 18.93 19.25 1.59 o -6 -2 5 2 0.42 0.08 1.65 < -4 -2 5 -2 5.59 7.56 1.17 o -4 -2 5 -1 1.66 0.62 1.09 < -4 -2 5 0 73.19 69.48 1.63 o -4 -2 5 1 125.74 126.65 1.68 o -4 -2 5 2 10.08 11.59 1.94 o -2 -2 5 -2 7.38 8.45 0.95 o -2 -2 5 -1 114.72 112.14 1.65 o -2 -2 5 0 258.20 276.98 2.24 o -2 -2 5 1 0.20 0.76 1.09 < -2 -2 5 2 0.05 -0.11 1.54 < 0 -2 5 -2 3.48 3.44 0.95 o 0 -2 5 -1 6.10 6.94 1.24 o 0 -2 5 0 0.65 1.91 0.98 < 0 -2 5 1 16.81 18.20 1.66 o 0 -2 5 2 0.26 0.82 2.12 < 2 -2 5 -2 0.40 0.33 1.04 < 2 -2 5 -1 14.55 15.11 1.31 o 2 -2 5 0 830.59 877.09 4.66 o 2 -2 5 1 4.14 2.60 2.26 < 2 -2 5 2 0.01 0.34 2.46 < 4 -2 5 -2 2.29 2.41 1.10 < 4 -2 5 -1 0.83 1.49 1.65 < 4 -2 5 0 3.97 4.71 1.99 < 4 -2 5 1 0.51 1.52 2.61 < 4 -2 5 2 0.05 -2.82 5.68 < 6 -2 5 -2 0.37 -0.44 1.77 < 6 -2 5 -1 3.03 3.92 2.44 < 6 -2 5 0 226.25 238.92 8.08 o -9 -1 5 -2 0.11 -0.53 2.92 < -9 -1 5 -1 20.55 22.79 3.13 o -9 -1 5 0 1.57 2.07 2.85 < -9 -1 5 1 14.11 14.73 2.77 o -9 -1 5 2 0.65 -1.63 3.70 < -7 -1 5 -2 0.16 -1.60 2.40 < -7 -1 5 -1 144.23 145.12 3.24 o -7 -1 5 0 697.37 677.62 4.25 o -7 -1 5 1 124.70 120.32 2.51 o -7 -1 5 2 5.43 6.11 1.87 o -5 -1 5 -2 1.25 1.23 1.46 < -5 -1 5 -1 45.11 46.44 1.57 o -5 -1 5 0 4.68 14.20 1.42 o -5 -1 5 1 76.03 77.07 1.98 o -5 -1 5 2 1.56 4.19 2.32 < -3 -1 5 -2 6.76 7.19 1.04 o -3 -1 5 -1 56.02 54.25 1.57 o -3 -1 5 0 2650.58 2574.21 7.14 o -3 -1 5 1 85.54 87.77 1.70 o -3 -1 5 2 0.07 0.12 1.15 < -1 -1 5 -2 0.59 0.73 1.17 < -1 -1 5 -1 31.83 33.81 0.98 o -1 -1 5 0 90.22 106.80 1.49 o -1 -1 5 1 76.63 81.43 1.54 o -1 -1 5 2 2.31 1.98 1.48 < 1 -1 5 -2 3.39 3.95 1.38 < 1 -1 5 -1 0.25 0.25 0.96 < 1 -1 5 0 499.66 516.70 2.90 o 1 -1 5 1 5.21 5.24 1.51 o 1 -1 5 2 2.40 2.30 2.02 < 3 -1 5 -2 0.11 1.06 1.23 < 3 -1 5 -1 0.02 -0.26 1.52 < 3 -1 5 0 702.14 726.24 4.64 o 3 -1 5 1 3.12 2.71 2.50 < 3 -1 5 2 0.22 0.56 2.75 < 5 -1 5 -2 0.19 0.40 1.46 < 5 -1 5 -1 4.57 4.84 2.40 < 5 -1 5 0 30.77 28.82 2.99 o 5 -1 5 1 5.71 4.56 5.77 < 7 -1 5 -2 0.03 -1.26 2.55 < 7 -1 5 -1 0.02 1.52 5.40 < -8 0 5 -2 12.08 15.75 2.77 o -8 0 5 -1 58.81 58.64 2.51 o -8 0 5 0 56.52 55.28 2.85 o -8 0 5 1 1.63 2.47 2.10 < -8 0 5 2 3.19 3.17 2.24 < -6 0 5 -2 2.41 2.99 2.04 < -6 0 5 -1 50.96 47.90 2.23 o -6 0 5 0 102.46 92.51 2.19 o -6 0 5 1 8.41 9.09 1.82 o -6 0 5 2 5.67 5.03 1.96 < -4 0 5 -2 9.53 10.08 1.10 o -4 0 5 -1 182.37 175.70 2.10 o -4 0 5 0 653.49 636.18 4.45 o -4 0 5 1 2.89 2.05 1.52 < -4 0 5 2 1.15 0.23 1.34 < -2 0 5 -2 0.06 0.16 1.09 < -2 0 5 -1 73.81 74.18 1.93 o -2 0 5 0 17.84 17.58 1.18 o -2 0 5 1 6.17 5.38 1.14 o -2 0 5 2 0.16 -0.25 1.24 < 0 0 5 -2 2.37 3.75 0.79 o 0 0 5 -1 54.06 54.92 1.26 o 0 0 5 0 1948.37 2078.55 5.43 o 0 0 5 1 3.38 3.77 1.34 < 0 0 5 2 0.40 -0.58 1.51 < 2 0 5 -2 0.00 -1.07 1.18 < 2 0 5 -1 12.18 12.79 1.23 o 2 0 5 0 36.44 41.61 2.05 o 2 0 5 1 9.65 10.25 2.08 o 2 0 5 2 0.42 1.87 2.58 < 4 0 5 -2 0.10 -0.17 1.32 < 4 0 5 -1 1.11 1.57 1.93 < 4 0 5 0 2144.89 2157.83 9.97 o 4 0 5 1 0.12 -0.40 2.77 < 6 0 5 -2 2.16 2.72 2.04 < 6 0 5 -1 7.74 7.86 2.78 < 6 0 5 0 102.52 96.56 6.51 o 8 0 5 -2 2.46 3.25 4.90 < -9 1 5 -2 0.28 0.51 2.86 < -9 1 5 -1 13.41 12.84 2.86 o -9 1 5 0 122.59 111.92 3.53 o -9 1 5 1 57.39 54.08 2.91 o -9 1 5 2 17.16 18.36 2.43 o -7 1 5 -2 21.78 26.08 2.38 o -7 1 5 -1 5.10 7.36 2.15 o -7 1 5 0 49.99 65.61 2.57 o -7 1 5 1 212.22 204.86 3.36 o -7 1 5 2 9.99 10.80 1.80 o -5 1 5 -2 2.07 4.03 1.56 < -5 1 5 -1 1.49 2.50 1.40 < -5 1 5 0 735.02 699.32 4.30 o -5 1 5 1 68.14 68.70 2.16 o -5 1 5 2 7.55 9.01 1.99 o -3 1 5 -2 20.45 21.53 1.37 o -3 1 5 -1 1.83 1.99 1.17 < -3 1 5 0 546.28 574.12 4.31 o -3 1 5 1 149.41 154.09 1.82 o -3 1 5 2 5.59 6.63 1.40 o -1 1 5 -2 9.22 9.90 1.06 o -1 1 5 -1 0.75 0.40 1.04 < -1 1 5 0 591.87 576.94 3.20 o -1 1 5 1 36.61 39.91 1.45 o -1 1 5 2 0.01 0.61 1.59 < 1 1 5 -2 0.59 1.21 0.96 < 1 1 5 -1 13.67 14.30 1.21 o 1 1 5 0 7.18 13.60 1.38 o 1 1 5 1 31.08 32.15 2.09 o 1 1 5 2 0.09 -0.34 2.18 < 3 1 5 -2 2.38 1.91 1.51 < 3 1 5 -1 1.50 0.96 1.76 < 3 1 5 0 91.17 107.04 3.02 o 3 1 5 1 2.45 1.99 2.32 < 3 1 5 2 0.83 3.28 2.82 < 5 1 5 -2 0.81 0.14 1.98 < 5 1 5 -1 0.22 1.26 2.05 < 5 1 5 0 6.94 6.04 2.85 < 7 1 5 -2 0.89 0.45 2.33 < -8 2 5 -2 4.11 3.05 3.19 < -8 2 5 -1 106.95 105.42 3.10 o -8 2 5 0 591.79 540.36 5.09 o -8 2 5 1 21.60 19.78 2.27 o -8 2 5 2 2.89 1.96 2.35 < -6 2 5 -2 3.33 3.11 1.66 < -6 2 5 -1 53.85 55.50 2.19 o -6 2 5 0 218.96 186.38 2.96 o -6 2 5 1 7.45 6.01 1.82 o -6 2 5 2 2.29 3.24 1.90 < -4 2 5 -2 1.44 1.51 1.18 < -4 2 5 -1 221.64 218.55 2.54 o -4 2 5 0 221.93 210.08 2.88 o -4 2 5 1 100.04 98.69 2.44 o -4 2 5 2 0.03 0.42 1.42 < -2 2 5 -2 2.19 1.21 1.20 < -2 2 5 -1 8.86 8.54 1.40 o -2 2 5 0 1333.39 1275.17 4.19 o -2 2 5 1 11.02 11.67 1.32 o -2 2 5 2 0.73 1.38 1.63 < 0 2 5 -2 4.01 3.89 0.95 o 0 2 5 -1 76.79 77.00 1.99 o 0 2 5 0 338.22 341.92 2.77 o 0 2 5 1 75.03 75.13 1.81 o 0 2 5 2 0.03 0.45 1.66 < 2 2 5 -2 0.15 0.12 1.10 < 2 2 5 -1 5.49 6.52 1.34 o 2 2 5 0 1913.33 1931.18 6.90 o 2 2 5 1 0.08 -0.42 2.16 < 2 2 5 2 0.37 1.62 2.47 < 4 2 5 -2 0.19 0.78 1.76 < 4 2 5 -1 1.81 1.14 2.36 < 4 2 5 0 78.81 78.33 3.13 o 4 2 5 1 2.19 0.79 2.96 < 6 2 5 -2 1.53 2.07 3.24 < 6 2 5 -1 0.10 1.42 3.16 < 8 2 5 -2 0.01 -0.39 5.20 < -9 3 5 -2 9.84 15.56 3.55 o -9 3 5 -1 0.47 1.34 3.13 < -9 3 5 0 36.81 33.61 2.71 o -9 3 5 1 44.44 42.50 2.72 o -9 3 5 2 13.43 12.70 2.99 o -7 3 5 -2 6.57 11.87 2.72 o -7 3 5 -1 85.70 78.82 2.65 o -7 3 5 0 3.65 3.45 1.94 < -7 3 5 1 5.31 5.20 2.21 < -7 3 5 2 4.64 4.53 2.24 < -5 3 5 -2 13.61 14.33 1.45 o -5 3 5 -1 24.61 23.43 1.70 o -5 3 5 0 221.78 225.19 3.18 o -5 3 5 1 49.59 52.74 2.29 o -5 3 5 2 10.24 8.65 2.04 o -3 3 5 -2 11.38 11.98 1.49 o -3 3 5 -1 86.95 88.06 2.12 o -3 3 5 0 45.44 42.16 1.90 o -3 3 5 1 0.57 -0.47 1.51 < -3 3 5 2 0.02 0.09 2.46 < -1 3 5 -2 0.08 1.43 1.28 < -1 3 5 -1 104.82 101.83 1.90 o -1 3 5 0 292.03 306.33 3.46 o -1 3 5 1 0.75 2.18 1.88 < -1 3 5 2 0.34 0.86 1.88 < 1 3 5 -2 4.09 4.78 1.48 o 1 3 5 -1 19.23 20.32 1.59 o 1 3 5 0 625.33 630.78 4.37 o 1 3 5 1 9.35 9.24 1.84 o 1 3 5 2 0.57 0.28 2.05 < 3 3 5 -2 0.10 0.73 1.73 < 3 3 5 -1 23.33 25.16 2.01 o 3 3 5 0 73.82 81.59 2.71 o 3 3 5 1 0.75 0.73 2.78 < 3 3 5 2 0.00 0.75 3.62 < 5 3 5 -2 1.50 2.15 2.05 < 5 3 5 -1 3.30 2.83 2.61 < 5 3 5 0 419.58 411.87 5.44 o 7 3 5 -2 1.59 -0.09 2.85 < -8 4 5 -2 0.07 -0.44 2.94 < -8 4 5 -1 60.13 63.70 2.79 o -8 4 5 0 6.28 10.21 2.26 o -8 4 5 1 175.63 174.56 4.10 o -8 4 5 2 18.42 20.65 2.58 o -6 4 5 -2 11.07 12.23 1.59 o -6 4 5 -1 33.54 31.26 2.02 o -6 4 5 0 93.86 87.43 2.94 o -6 4 5 1 61.62 63.29 2.51 o -6 4 5 2 0.58 0.09 2.12 < -4 4 5 -2 1.49 2.83 1.63 < -4 4 5 -1 14.87 14.38 1.66 o -4 4 5 0 526.56 507.26 4.23 o -4 4 5 1 272.61 268.59 3.21 o -4 4 5 2 8.38 9.97 1.82 o -2 4 5 -2 10.13 12.49 1.42 o -2 4 5 -1 37.49 34.22 1.42 o -2 4 5 0 105.68 102.06 1.76 o -2 4 5 1 72.36 73.17 2.41 o -2 4 5 2 0.87 0.75 2.08 < 0 4 5 -2 3.48 4.25 1.40 o 0 4 5 -1 0.38 0.62 1.68 < 0 4 5 0 386.75 399.67 4.07 o 0 4 5 1 35.22 36.91 1.95 o 0 4 5 2 0.28 1.98 2.57 < 2 4 5 -2 0.53 -1.26 1.38 < 2 4 5 -1 0.00 0.42 2.05 < 2 4 5 0 1.76 0.67 2.10 < 2 4 5 1 33.73 35.49 2.32 o 2 4 5 2 0.06 0.39 2.52 < 4 4 5 -2 0.68 0.05 2.24 < 4 4 5 -1 0.32 0.73 2.26 < 4 4 5 0 257.51 264.49 3.97 o 6 4 5 -2 0.11 -1.62 3.14 < 6 4 5 -1 1.47 3.36 3.64 < -9 5 5 -2 5.55 8.26 2.75 < -9 5 5 -1 45.55 43.81 2.91 o -9 5 5 0 0.34 -1.01 3.17 < -9 5 5 1 16.47 18.86 3.14 o -7 5 5 -2 9.88 12.54 2.18 o -7 5 5 -1 47.45 45.50 2.71 o -7 5 5 0 271.10 264.46 4.30 o -7 5 5 1 0.14 0.72 2.22 < -7 5 5 2 1.91 0.53 2.33 < -5 5 5 -2 6.85 5.96 1.57 o -5 5 5 -1 130.80 127.60 3.04 o -5 5 5 0 5.18 2.69 1.84 < -5 5 5 1 23.79 22.83 2.10 o -5 5 5 2 0.48 0.23 2.05 < -3 5 5 -2 0.29 0.03 1.52 < -3 5 5 -1 84.05 82.34 2.15 o -3 5 5 0 1288.84 1247.42 5.98 o -3 5 5 1 1.14 2.78 1.82 < -3 5 5 2 1.01 1.76 2.26 < -1 5 5 -2 3.75 4.39 1.17 o -1 5 5 -1 97.55 99.22 1.98 o -1 5 5 0 233.62 215.05 3.21 o -1 5 5 1 73.29 72.18 2.58 o -1 5 5 2 3.03 4.70 2.01 < 1 5 5 -2 0.09 -0.09 1.54 < 1 5 5 -1 24.40 25.50 2.02 o 1 5 5 0 425.61 408.42 4.32 o 1 5 5 1 1.09 1.82 2.60 < 1 5 5 2 0.18 0.06 2.54 < 3 5 5 -2 3.42 2.89 2.58 < 3 5 5 -1 1.92 1.66 2.10 < 3 5 5 0 805.57 810.35 6.98 o 3 5 5 1 10.88 10.60 3.05 o 5 5 5 -2 0.07 2.27 2.64 < 5 5 5 -1 23.67 25.24 2.68 o 7 5 5 -2 3.52 0.84 3.55 < -8 6 5 -2 10.27 12.93 3.97 o -8 6 5 -1 7.36 4.37 3.83 < -8 6 5 0 87.44 71.72 4.81 o -8 6 5 1 4.64 5.77 3.47 < -8 6 5 2 9.98 9.77 3.39 < -6 6 5 -2 3.00 5.63 2.24 < -6 6 5 -1 0.40 0.50 2.36 < -6 6 5 0 8.44 7.34 2.27 o -6 6 5 1 192.64 200.35 3.38 o -6 6 5 2 17.83 16.14 2.89 o -4 6 5 -2 15.16 17.04 1.79 o -4 6 5 -1 22.50 18.44 1.84 o -4 6 5 0 72.05 78.36 1.98 o -4 6 5 1 1.60 2.44 2.02 < -4 6 5 2 3.25 4.89 3.89 < -2 6 5 -2 2.43 4.11 1.35 o -2 6 5 -1 54.01 57.10 2.61 o -2 6 5 0 81.25 79.04 2.10 o -2 6 5 1 34.41 31.21 2.46 o -2 6 5 2 1.48 2.21 2.97 < 0 6 5 -2 5.95 7.28 1.42 o 0 6 5 -1 2.15 1.57 1.52 < 0 6 5 0 292.33 302.94 3.91 o 0 6 5 1 39.24 37.53 2.74 o 0 6 5 2 1.84 1.76 2.88 < 2 6 5 -2 0.22 2.08 2.26 < 2 6 5 -1 36.51 37.83 4.09 o 2 6 5 0 207.85 204.15 4.91 o 2 6 5 1 18.27 19.82 2.69 o 4 6 5 -2 0.06 -0.67 2.18 < 4 6 5 -1 0.19 0.03 2.85 < 4 6 5 0 694.78 716.09 7.01 o 6 6 5 -2 4.15 3.66 3.83 < -7 7 5 -2 1.23 0.51 3.52 < -7 7 5 -1 83.87 86.35 4.86 o -7 7 5 0 2.46 4.39 4.48 < -7 7 5 1 122.32 135.70 5.81 o -7 7 5 2 0.04 -1.23 4.57 < -5 7 5 -2 0.85 0.89 2.02 < -5 7 5 -1 42.88 42.95 2.26 o -5 7 5 0 860.34 792.35 4.56 o -5 7 5 1 6.36 5.96 2.75 < -5 7 5 2 0.61 -0.16 4.42 < -3 7 5 -2 2.49 3.08 1.57 < -3 7 5 -1 69.53 64.82 2.68 o -3 7 5 0 22.75 22.79 2.18 o -3 7 5 1 249.79 257.87 3.85 o -3 7 5 2 2.85 3.91 3.31 < -1 7 5 -2 1.99 1.82 1.37 < -1 7 5 -1 9.64 8.64 1.54 o -1 7 5 0 1095.32 1068.42 6.63 o -1 7 5 1 7.22 4.75 3.11 < -1 7 5 2 0.01 -1.06 3.24 < 1 7 5 -2 0.28 0.64 1.79 < 1 7 5 -1 3.34 1.62 2.40 < 1 7 5 0 322.51 303.29 4.47 o 1 7 5 1 113.39 101.70 3.56 o 3 7 5 -2 1.97 -0.96 2.77 < 3 7 5 -1 31.56 31.45 2.96 o 3 7 5 0 148.13 147.60 4.22 o 5 7 5 -2 1.32 1.62 2.92 < -6 8 5 -1 35.10 37.30 4.71 o -6 8 5 0 22.11 20.12 4.12 o -6 8 5 1 2.31 1.65 4.48 < -4 8 5 -2 1.79 0.61 2.19 < -4 8 5 -1 139.01 140.56 3.44 o -4 8 5 0 18.17 15.84 3.02 o -4 8 5 1 0.44 -0.68 3.02 < -4 8 5 2 1.69 1.18 3.08 < -2 8 5 -2 15.36 15.59 1.84 o -2 8 5 -1 2.97 2.69 1.96 < -2 8 5 0 324.11 301.82 4.77 o -2 8 5 1 8.23 6.16 3.36 < 0 8 5 -2 0.19 0.36 1.65 < 0 8 5 -1 151.38 155.65 3.91 o 0 8 5 0 35.88 34.67 4.92 o 0 8 5 1 61.00 59.92 3.83 o 2 8 5 -2 3.15 1.31 2.74 < 2 8 5 -1 3.85 4.26 3.20 < 2 8 5 0 1064.06 1015.30 9.57 o 4 8 5 -2 1.68 -1.79 2.85 < 4 8 5 -1 4.99 5.73 4.09 < -5 9 5 -1 16.58 16.17 4.31 o -5 9 5 0 2.30 4.06 4.64 < -5 9 5 1 192.30 213.95 7.33 o -3 9 5 -2 3.79 4.05 3.80 < -3 9 5 -1 0.62 1.10 2.94 < -3 9 5 0 304.92 285.68 4.25 o -3 9 5 1 19.85 21.97 3.72 o -1 9 5 -2 0.31 0.89 2.05 < -1 9 5 -1 1.78 1.23 2.33 < -1 9 5 0 2.84 3.59 3.34 < 1 9 5 -2 5.74 6.88 2.86 < 1 9 5 -1 0.12 -0.89 3.00 < 1 9 5 0 0.37 0.47 2.92 < 3 9 5 -2 0.22 -0.61 2.68 < 3 9 5 -1 27.62 25.50 3.31 o -4 10 5 -2 3.94 3.53 4.42 < -4 10 5 -1 18.47 16.51 3.33 o -4 10 5 0 244.05 242.82 7.57 o -2 10 5 -2 0.63 0.61 2.38 < -2 10 5 -1 142.38 138.13 3.43 o -2 10 5 0 228.78 219.03 5.26 o 0 10 5 -2 0.55 0.81 2.36 < 0 10 5 -1 3.73 2.33 3.22 < 2 10 5 -2 0.16 2.15 3.31 < -3 11 5 -2 2.71 3.58 3.19 < -3 11 5 -1 21.86 19.95 5.09 o -1 11 5 -2 7.81 6.08 2.72 < -1 11 5 -1 36.08 31.25 5.40 o 1 11 5 -2 0.05 -2.15 3.36 < -1 -9 6 -2 0.46 2.58 4.62 < 1 -9 6 -2 0.35 -1.06 4.50 < -4 -8 6 -2 0.17 1.23 3.28 < -4 -8 6 -1 75.72 69.68 5.25 o 0 -8 6 -2 0.24 0.82 4.06 < -5 -7 6 -2 9.97 11.92 2.02 o -5 -7 6 -1 1.74 2.21 2.47 < -5 -7 6 0 238.40 225.80 4.49 o -5 -7 6 1 64.36 74.24 5.23 o -3 -7 6 -2 1.06 2.02 2.58 < -3 -7 6 -1 0.45 1.14 2.52 < -3 -7 6 0 0.20 -1.21 2.99 < -3 -7 6 1 12.23 14.89 3.27 o -3 -7 6 2 0.18 -1.18 4.56 < -1 -7 6 -2 9.38 8.00 3.94 < -1 -7 6 -1 17.76 20.15 4.14 o -1 -7 6 0 11.18 12.15 4.26 < -1 -7 6 1 9.47 8.31 4.59 < 3 -7 6 -2 0.90 2.08 3.70 < 3 -7 6 -1 22.12 23.40 4.68 o -6 -6 6 -2 6.96 6.52 1.90 o -6 -6 6 -1 120.19 120.44 2.34 o -6 -6 6 0 464.54 447.70 3.42 o -6 -6 6 1 11.01 11.58 2.33 o -4 -6 6 -2 3.27 3.10 1.38 < -4 -6 6 -1 7.59 7.69 1.54 o -4 -6 6 0 5.00 5.45 2.01 < -4 -6 6 1 22.21 23.12 2.51 o -4 -6 6 2 0.25 0.92 3.14 < -2 -6 6 -2 0.45 0.81 1.59 < -2 -6 6 -1 109.21 118.15 2.76 o -2 -6 6 0 899.80 989.54 7.72 o -2 -6 6 1 65.19 79.01 5.52 o -2 -6 6 2 2.47 0.36 5.04 < 0 -6 6 -2 0.89 -0.73 3.52 < 0 -6 6 -1 0.33 -1.62 3.75 < 0 -6 6 0 10.99 12.32 4.42 < 2 -6 6 -1 14.72 15.95 4.01 o 4 -6 6 -2 0.13 0.36 3.50 < 4 -6 6 -1 0.01 -0.53 3.75 < -7 -5 6 -2 1.05 0.53 4.73 < -7 -5 6 -1 1.55 1.43 2.50 < -7 -5 6 0 43.65 46.03 5.18 o -5 -5 6 -2 3.43 3.33 1.49 < -5 -5 6 -1 51.28 49.77 1.79 o -5 -5 6 0 296.86 287.62 3.04 o -5 -5 6 1 2.41 1.34 2.30 < -5 -5 6 2 0.28 0.81 2.44 < -3 -5 6 -2 7.86 8.68 1.34 o -3 -5 6 -1 1.84 1.48 1.49 < -3 -5 6 0 5.95 6.57 2.15 o -3 -5 6 1 58.21 68.10 3.44 o -3 -5 6 2 0.22 0.19 4.51 < -1 -5 6 -2 0.49 0.12 1.79 < -1 -5 6 -1 23.32 25.52 2.66 o -1 -5 6 0 25.08 38.84 4.53 o -1 -5 6 1 1.52 1.24 4.36 < -1 -5 6 2 0.01 -0.44 4.71 < 1 -5 6 -2 1.33 0.95 3.44 < 1 -5 6 -1 21.19 21.99 4.14 o 1 -5 6 0 397.71 392.68 7.12 o 1 -5 6 1 1.12 -0.92 4.14 < 3 -5 6 -2 0.13 0.23 2.32 < 3 -5 6 -1 8.52 8.40 2.63 o 3 -5 6 0 45.91 49.61 4.82 o 5 -5 6 -2 1.49 1.77 2.88 < -6 -4 6 -2 8.15 9.40 1.68 o -6 -4 6 -1 12.71 14.25 1.73 o -6 -4 6 0 6.55 7.78 1.82 o -6 -4 6 1 72.50 73.30 2.49 o -6 -4 6 2 2.87 1.38 2.52 < -4 -4 6 -2 2.23 3.48 1.37 < -4 -4 6 -1 24.95 24.69 1.49 o -4 -4 6 0 295.89 297.28 3.27 o -4 -4 6 1 56.24 64.54 2.69 o -4 -4 6 2 1.73 1.74 2.69 < -2 -4 6 -2 8.54 8.67 1.54 o -2 -4 6 -1 5.58 5.20 1.87 < -2 -4 6 0 35.09 35.90 2.93 o -2 -4 6 1 14.48 19.78 3.95 o -2 -4 6 2 0.19 1.31 4.45 < 0 -4 6 -2 2.49 3.11 2.19 < 0 -4 6 -1 7.40 7.03 2.33 o 0 -4 6 0 457.83 481.07 5.57 o 0 -4 6 1 35.72 35.60 3.08 o 2 -4 6 -2 0.87 1.88 1.99 < 2 -4 6 -1 6.76 5.52 2.36 < 2 -4 6 0 18.75 18.70 4.14 o 2 -4 6 1 0.39 -1.00 4.12 < 4 -4 6 -2 0.63 0.70 2.41 < 4 -4 6 -1 0.05 0.93 3.81 < 6 -4 6 -2 0.25 -0.64 3.92 < -7 -3 6 -2 5.52 5.13 2.18 < -7 -3 6 -1 90.40 86.65 2.23 o -7 -3 6 0 384.64 380.14 3.59 o -7 -3 6 1 4.03 3.14 2.15 < -7 -3 6 2 2.62 -0.39 2.92 < -5 -3 6 -2 3.35 3.91 1.49 < -5 -3 6 -1 60.01 60.41 1.77 o -5 -3 6 0 2.33 3.73 1.82 < -5 -3 6 1 4.80 4.98 2.19 < -5 -3 6 2 0.23 0.37 2.30 < -3 -3 6 -2 0.01 0.05 1.20 < -3 -3 6 -1 104.55 110.10 2.23 o -3 -3 6 0 863.26 928.41 6.03 o -3 -3 6 1 9.29 9.85 2.71 o -3 -3 6 2 0.14 -2.57 4.23 < -1 -3 6 -2 0.11 -1.49 1.60 < -1 -3 6 -1 49.36 51.82 2.12 o -1 -3 6 0 392.67 428.73 7.75 o -1 -3 6 1 21.44 24.07 4.48 o -1 -3 6 2 1.35 3.81 4.54 < 1 -3 6 -2 0.02 -0.82 2.01 < 1 -3 6 -1 9.32 9.07 2.33 o 1 -3 6 0 336.42 353.65 5.10 o 1 -3 6 1 4.33 4.62 3.72 < 1 -3 6 2 0.00 -0.96 4.15 < 3 -3 6 -2 0.16 0.02 1.84 < 3 -3 6 -1 7.41 8.06 2.88 < 3 -3 6 0 419.41 419.21 8.20 o 5 -3 6 -2 0.13 -0.05 2.33 < -6 -2 6 -2 7.47 9.49 1.77 o -6 -2 6 -1 0.02 -0.33 1.71 < -6 -2 6 0 96.62 97.83 2.62 o -6 -2 6 1 86.51 84.98 2.51 o -6 -2 6 2 8.68 9.16 2.50 o -4 -2 6 -2 5.11 5.26 1.24 o -4 -2 6 -1 8.23 7.28 1.62 o -4 -2 6 0 23.74 26.62 2.18 o -4 -2 6 1 41.68 44.10 2.54 o -4 -2 6 2 1.51 1.35 2.78 < -2 -2 6 -2 5.11 5.23 1.66 o -2 -2 6 -1 11.78 14.07 1.91 o -2 -2 6 0 59.45 62.25 2.93 o -2 -2 6 1 18.25 19.92 4.25 o -2 -2 6 2 0.11 2.96 4.42 < 0 -2 6 -2 1.98 2.71 1.42 < 0 -2 6 -1 6.56 7.11 1.85 o 0 -2 6 0 234.72 250.15 4.31 o 0 -2 6 1 6.88 8.29 2.78 < 0 -2 6 2 0.01 0.39 4.06 < 2 -2 6 -2 1.37 1.82 1.34 < 2 -2 6 -1 2.86 4.79 2.77 < 2 -2 6 0 84.97 81.42 3.58 o 2 -2 6 1 0.68 3.84 4.19 < 4 -2 6 -2 0.06 -1.23 1.87 < 4 -2 6 -1 1.32 1.46 2.52 < 4 -2 6 0 102.10 103.12 6.12 o 6 -2 6 -2 1.19 1.31 3.24 < -7 -1 6 -2 0.02 1.43 2.02 < -7 -1 6 -1 87.82 84.80 2.96 o -7 -1 6 0 1.49 7.92 2.44 o -7 -1 6 1 94.74 94.14 2.63 o -7 -1 6 2 2.93 5.29 2.40 < -5 -1 6 -2 2.06 2.74 1.48 < -5 -1 6 -1 16.91 17.82 1.87 o -5 -1 6 0 702.48 670.57 4.62 o -5 -1 6 1 17.47 20.91 2.24 o -5 -1 6 2 0.26 -1.56 2.26 < -3 -1 6 -2 0.39 -0.22 1.38 < -3 -1 6 -1 81.94 84.39 1.90 o -3 -1 6 0 61.94 75.11 2.46 o -3 -1 6 1 120.13 127.78 3.81 o -3 -1 6 2 6.95 7.30 4.29 < -1 -1 6 -2 4.99 4.99 0.96 o -1 -1 6 -1 4.52 4.54 1.17 o -1 -1 6 0 101.96 107.44 2.66 o -1 -1 6 1 17.71 21.46 2.33 o 1 -1 6 -2 0.52 1.18 1.23 < 1 -1 6 -1 5.11 6.77 2.04 o 1 -1 6 0 929.50 981.11 6.44 o 1 -1 6 1 31.60 34.48 3.47 o 1 -1 6 2 0.06 -0.19 3.50 < 3 -1 6 -2 0.37 1.65 2.46 < 3 -1 6 -1 1.19 2.27 2.38 < 3 -1 6 0 9.38 8.84 2.63 o 3 -1 6 1 0.89 -0.36 5.26 < 5 -1 6 -2 0.21 0.68 2.52 < 5 -1 6 -1 0.12 -0.19 2.77 < -8 0 6 -2 1.69 3.72 2.36 < -8 0 6 -1 9.89 8.18 2.58 o -8 0 6 0 20.32 16.12 2.69 o -6 0 6 -2 22.02 24.58 2.40 o -6 0 6 -1 84.72 80.20 2.41 o -6 0 6 0 458.13 445.51 3.99 o -6 0 6 1 5.35 6.10 2.69 < -6 0 6 2 0.08 0.33 2.43 < -4 0 6 -2 0.79 3.05 1.71 < -4 0 6 -1 57.70 57.52 2.26 o -4 0 6 0 11.42 13.16 1.66 o -4 0 6 1 0.30 1.09 1.85 < -4 0 6 2 2.45 2.96 2.91 < -2 0 6 -2 8.38 9.38 1.21 o -2 0 6 -1 55.90 58.95 1.65 o -2 0 6 0 1004.65 1064.58 4.68 o -2 0 6 1 1.40 1.00 2.22 < -2 0 6 2 0.13 0.30 3.03 < 0 0 6 -2 0.40 0.73 1.00 < 0 0 6 -1 40.84 43.67 1.62 o 0 0 6 0 8.06 6.78 1.63 o 0 0 6 1 6.45 6.61 2.24 < 0 0 6 2 0.44 2.97 2.66 < 2 0 6 -2 0.01 0.92 1.65 < 2 0 6 -1 21.89 24.58 1.82 o 2 0 6 0 1260.22 1318.08 7.72 o 2 0 6 1 0.10 -1.31 3.36 < 4 0 6 -2 1.74 2.04 2.38 < 4 0 6 -1 0.27 -0.05 2.58 < 4 0 6 0 263.96 271.84 5.83 o 6 0 6 -2 0.86 0.30 2.83 < -7 1 6 -2 0.66 2.27 2.04 < -7 1 6 -1 13.36 15.53 2.30 o -7 1 6 0 307.56 283.99 3.57 o -7 1 6 1 81.49 86.90 3.04 o -7 1 6 2 6.02 5.66 2.60 < -5 1 6 -2 4.30 6.91 1.82 o -5 1 6 -1 0.48 0.19 1.70 < -5 1 6 0 61.72 72.13 2.55 o -5 1 6 1 48.13 51.07 2.18 o -5 1 6 2 6.67 7.28 1.84 o -3 1 6 -2 17.73 19.93 2.29 o -3 1 6 -1 2.48 3.20 1.79 < -3 1 6 0 302.76 305.20 3.16 o -3 1 6 1 89.79 91.99 2.33 o -3 1 6 2 0.06 0.67 1.98 < -1 1 6 -2 0.05 1.79 1.09 < -1 1 6 -1 7.67 8.12 1.18 o -1 1 6 0 262.53 262.37 2.46 o -1 1 6 1 22.91 23.90 1.87 o -1 1 6 2 1.47 1.10 2.21 < 1 1 6 -2 7.62 7.64 1.29 o 1 1 6 -1 0.11 -0.31 1.46 < 1 1 6 0 74.28 93.04 2.18 o 1 1 6 1 7.29 10.04 2.43 o 1 1 6 2 1.32 1.88 3.91 < 3 1 6 -2 0.01 -0.36 1.88 < 3 1 6 -1 5.81 5.62 2.19 < 3 1 6 0 166.77 166.74 3.91 o 5 1 6 -2 0.93 1.09 2.68 < 5 1 6 -1 0.02 0.47 2.97 < -8 2 6 -2 9.61 11.05 2.63 o -8 2 6 -1 51.54 48.83 2.86 o -8 2 6 0 36.24 28.01 2.44 o -6 2 6 -2 0.46 -0.37 1.91 < -6 2 6 -1 99.69 96.27 2.49 o -6 2 6 0 7.34 6.46 2.30 < -6 2 6 1 31.37 33.19 2.57 o -6 2 6 2 0.27 0.61 2.02 < -4 2 6 -2 4.49 4.50 1.85 < -4 2 6 -1 76.09 76.58 2.43 o -4 2 6 0 583.00 572.36 4.23 o -4 2 6 1 44.89 47.28 2.18 o -4 2 6 2 1.23 1.00 2.12 < -2 2 6 -2 1.85 2.12 1.23 < -2 2 6 -1 68.53 70.32 1.57 o -2 2 6 0 75.75 76.95 2.61 o -2 2 6 1 52.87 54.58 2.33 o -2 2 6 2 0.58 0.17 2.24 < 0 2 6 -2 0.28 1.06 1.43 < 0 2 6 -1 57.64 59.11 1.68 o 0 2 6 0 1250.32 1287.56 5.14 o 0 2 6 1 26.42 26.72 1.93 o 0 2 6 2 0.06 -0.12 2.58 < 2 2 6 -2 0.07 -0.09 1.38 < 2 2 6 -1 2.34 2.16 1.87 < 2 2 6 0 37.97 38.20 2.60 o 2 2 6 1 21.14 21.24 2.80 o 4 2 6 -2 0.01 -0.89 2.07 < 4 2 6 -1 0.89 0.65 2.78 < 6 2 6 -2 0.56 1.49 2.99 < -7 3 6 -2 15.19 19.39 2.32 o -7 3 6 -1 14.20 10.47 2.61 o -7 3 6 0 171.31 176.36 3.63 o -7 3 6 1 56.07 63.25 3.02 o -5 3 6 -2 13.01 15.54 2.10 o -5 3 6 -1 5.43 6.05 2.12 < -5 3 6 0 159.02 164.15 3.29 o -5 3 6 1 31.39 29.11 2.13 o -5 3 6 2 1.51 -0.28 2.15 < -3 3 6 -2 3.59 4.71 1.80 < -3 3 6 -1 66.07 61.49 1.99 o -3 3 6 0 304.02 310.29 3.37 o -3 3 6 1 30.39 33.45 2.54 o -3 3 6 2 4.29 4.96 2.49 < -1 3 6 -2 9.69 9.85 1.54 o -1 3 6 -1 19.41 19.43 1.68 o -1 3 6 0 63.68 61.57 1.99 o -1 3 6 1 0.08 0.68 1.74 < -1 3 6 2 0.51 0.23 2.16 < 1 3 6 -2 0.49 -0.16 1.43 < 1 3 6 -1 34.20 37.10 1.71 o 1 3 6 0 77.51 81.94 2.21 o 1 3 6 1 7.55 10.14 2.35 o 3 3 6 -2 2.39 0.09 1.88 < 3 3 6 -1 0.40 1.45 2.35 < 3 3 6 0 139.30 140.60 3.44 o 5 3 6 -2 0.27 -1.35 2.75 < -8 4 6 -2 0.06 -1.60 2.50 < -8 4 6 -1 36.85 35.62 3.27 o -6 4 6 -2 0.38 1.15 2.44 < -6 4 6 -1 13.05 13.57 2.30 o -6 4 6 0 185.33 173.17 3.46 o -6 4 6 1 108.24 105.31 3.14 o -6 4 6 2 4.24 6.18 2.26 < -4 4 6 -2 2.19 2.86 1.88 < -4 4 6 -1 51.19 55.34 2.40 o -4 4 6 0 74.29 59.34 2.19 o -4 4 6 1 58.74 61.92 2.46 o -4 4 6 2 4.42 3.36 2.60 < -2 4 6 -2 2.16 2.72 1.29 < -2 4 6 -1 0.25 0.54 1.98 < -2 4 6 0 285.11 280.13 3.91 o -2 4 6 1 24.84 24.01 2.60 o -2 4 6 2 0.26 -0.02 2.36 < 0 4 6 -2 1.88 2.01 1.87 < 0 4 6 -1 3.71 5.26 2.07 < 0 4 6 0 7.74 4.45 1.82 < 0 4 6 1 72.72 74.94 2.35 o 2 4 6 -2 0.71 0.76 1.85 < 2 4 6 -1 0.24 0.48 2.02 < 2 4 6 0 541.39 542.19 4.62 o 4 4 6 -2 0.09 0.34 2.32 < 4 4 6 -1 0.01 1.21 2.64 < -7 5 6 -2 6.22 7.41 2.83 < -7 5 6 -1 113.07 108.44 3.24 o -7 5 6 0 0.32 0.70 2.54 < -7 5 6 1 54.37 55.14 5.38 o -5 5 6 -2 3.40 3.77 2.08 < -5 5 6 -1 40.53 37.70 2.44 o -5 5 6 0 472.68 457.21 4.65 o -5 5 6 1 23.47 25.60 2.58 o -5 5 6 2 3.84 3.22 3.17 < -3 5 6 -2 3.11 3.87 1.80 < -3 5 6 -1 131.55 122.18 2.85 o -3 5 6 0 44.83 47.38 2.63 o -3 5 6 1 89.70 92.91 3.19 o -3 5 6 2 0.23 -1.34 2.78 < -1 5 6 -2 0.13 0.75 1.85 < -1 5 6 -1 48.48 48.86 2.51 o -1 5 6 0 180.45 178.32 3.60 o -1 5 6 1 0.65 1.31 2.32 < -1 5 6 2 0.01 0.03 5.01 < 1 5 6 -2 0.83 1.17 2.04 < 1 5 6 -1 10.86 9.68 2.13 o 1 5 6 0 601.83 645.38 5.46 o 3 5 6 -2 0.00 -1.18 2.35 < 3 5 6 -1 46.34 48.04 2.85 o 5 5 6 -2 0.52 -0.47 2.50 < -6 6 6 -2 12.64 14.55 2.43 o -6 6 6 -1 0.00 1.20 2.29 < -6 6 6 0 46.22 46.33 2.85 o -6 6 6 1 37.21 42.79 3.49 o -4 6 6 -2 3.75 6.63 1.99 o -4 6 6 -1 22.95 23.73 2.74 o -4 6 6 0 117.81 119.18 3.18 o -4 6 6 1 33.83 35.66 2.91 o -4 6 6 2 3.75 1.10 4.59 < -2 6 6 -2 12.94 15.05 2.01 o -2 6 6 -1 2.09 2.78 2.29 < -2 6 6 0 65.17 70.14 2.91 o -2 6 6 1 133.55 132.25 3.61 o 0 6 6 -2 1.91 2.15 2.04 < 0 6 6 -1 32.29 30.83 2.58 o 0 6 6 0 201.11 192.18 3.35 o 2 6 6 -2 0.53 -0.03 2.41 < 2 6 6 -1 4.84 3.61 2.89 < 4 6 6 -2 3.55 4.00 3.16 < -7 7 6 -2 2.34 4.29 5.23 < -5 7 6 -2 0.33 -0.16 2.12 < -5 7 6 -1 66.36 67.33 2.72 o -5 7 6 0 0.93 0.65 3.08 < -3 7 6 -2 1.73 2.68 1.93 < -3 7 6 -1 30.22 31.67 2.46 o -3 7 6 0 288.04 263.25 4.18 o -1 7 6 -2 1.43 1.88 2.10 < -1 7 6 -1 11.57 10.97 2.46 o -1 7 6 0 510.29 485.17 6.77 o 1 7 6 -2 3.39 5.49 2.24 < 1 7 6 -1 51.28 52.40 3.14 o 3 7 6 -2 1.02 0.96 3.52 < -6 8 6 -1 42.23 35.90 5.04 o -4 8 6 -2 16.35 18.28 2.89 o -4 8 6 -1 10.84 8.78 4.62 < -2 8 6 -2 0.50 1.09 1.98 < -2 8 6 -1 94.98 94.01 4.05 o 0 8 6 -2 1.72 2.66 3.05 < 0 8 6 -1 31.21 28.57 3.55 o 2 8 6 -2 2.65 2.13 2.77 < -5 9 6 -2 3.60 5.66 4.68 < -3 9 6 -2 0.41 0.82 4.54 < -1 9 6 -2 9.33 7.97 4.36 < 1 9 6 -2 0.01 0.76 3.28 < -4 10 6 -2 0.46 -0.34 5.43 < -2 10 6 -2 1.06 1.45 4.15 < -4 -6 7 -2 0.07 0.64 3.16 < -2 -6 7 -2 0.05 -1.09 3.13 < -2 -6 7 -1 7.83 8.96 5.15 < 0 -6 7 -2 3.69 4.39 4.71 < -5 -5 7 -2 19.14 21.83 2.08 o -5 -5 7 -1 19.28 17.43 4.39 o -3 -5 7 -2 0.09 0.95 2.32 < -3 -5 7 -1 6.38 6.38 3.07 < -1 -5 7 -2 5.17 7.75 4.57 < -1 -5 7 -1 64.66 70.38 5.54 o 1 -5 7 -2 0.19 1.34 4.22 < -4 -4 7 -2 3.83 4.70 2.02 < -4 -4 7 -1 0.17 0.65 2.33 < -4 -4 7 0 2.29 2.30 3.06 < -2 -4 7 -2 1.50 0.95 2.18 < -2 -4 7 -1 35.12 40.24 3.24 o -2 -4 7 0 544.81 618.87 10.23 o 0 -4 7 -2 0.54 -0.84 4.11 < 0 -4 7 -1 0.07 -0.64 4.11 < 2 -4 7 -2 2.17 2.75 3.66 < 2 -4 7 -1 0.68 0.86 4.23 < -5 -3 7 -2 1.12 1.63 1.85 < -5 -3 7 -1 53.04 57.81 2.85 o -3 -3 7 -2 1.16 0.06 2.19 < -3 -3 7 -1 38.21 40.79 2.63 o -3 -3 7 0 111.43 113.75 4.09 o -1 -3 7 -2 0.11 0.54 2.71 < -1 -3 7 -1 16.92 19.42 4.14 o -1 -3 7 0 51.90 57.86 5.48 o 1 -3 7 -2 0.23 0.12 2.66 < 1 -3 7 -1 19.23 21.49 4.82 o 3 -3 7 -2 0.19 0.67 3.87 < -6 -2 7 -2 8.65 11.70 2.04 o -6 -2 7 -1 0.03 -0.47 2.49 < -4 -2 7 -2 2.83 3.98 2.18 < -4 -2 7 -1 5.23 4.19 2.32 < -4 -2 7 0 71.72 74.60 2.97 o -2 -2 7 -2 9.26 12.59 2.15 o -2 -2 7 -1 4.46 5.76 4.06 < -2 -2 7 0 148.11 153.19 6.09 o 0 -2 7 -2 2.14 0.73 4.03 < 0 -2 7 -1 5.38 5.34 4.43 < 0 -2 7 0 154.24 151.05 6.24 o 2 -2 7 -2 0.55 -0.34 3.45 < 2 -2 7 -1 9.72 9.88 4.29 < 4 -2 7 -2 0.58 -0.62 4.43 < -5 -1 7 -2 0.33 1.04 1.94 < -5 -1 7 -1 43.32 43.31 2.65 o -5 -1 7 0 30.47 33.49 2.72 o -3 -1 7 -2 2.03 3.25 2.10 < -3 -1 7 -1 48.14 50.45 2.60 o -3 -1 7 0 78.58 89.63 3.78 o -1 -1 7 -2 0.05 1.20 2.49 < -1 -1 7 -1 8.62 9.16 4.31 < -1 -1 7 0 662.67 697.05 10.79 o 1 -1 7 -2 1.61 3.81 2.61 < 1 -1 7 -1 11.87 15.45 2.97 o 3 -1 7 -2 0.06 1.93 3.22 < -6 0 7 -2 3.84 5.06 2.08 < -6 0 7 -1 39.21 35.95 3.49 o -4 0 7 -2 5.95 7.28 2.80 < -4 0 7 -1 20.11 19.93 3.08 o -4 0 7 0 130.41 124.97 5.22 o -2 0 7 -2 3.51 5.37 2.04 < -2 0 7 -1 48.68 48.93 4.22 o -2 0 7 0 0.94 0.30 4.40 < 0 0 7 -2 0.01 -0.25 2.07 < 0 0 7 -1 37.37 37.58 4.85 o 0 0 7 0 305.47 327.83 8.20 o 2 0 7 -2 1.93 2.41 3.08 < 2 0 7 -1 6.12 6.24 3.35 < 4 0 7 -2 0.08 0.37 3.56 < -5 1 7 -2 16.06 16.18 2.46 o -5 1 7 -1 3.47 3.70 2.46 < -5 1 7 0 82.41 81.39 3.18 o -3 1 7 -2 0.14 -0.26 1.59 < -3 1 7 -1 4.08 5.04 2.83 < -3 1 7 0 180.79 176.73 4.48 o -1 1 7 -2 8.68 7.97 1.84 o -1 1 7 -1 0.19 1.14 3.00 < -1 1 7 0 35.46 42.39 4.76 o 1 1 7 -2 1.09 1.82 1.80 < 1 1 7 -1 0.50 0.23 2.61 < 1 1 7 0 148.77 164.71 4.97 o 3 1 7 -2 0.68 -0.03 2.68 < 3 1 7 -1 0.96 -0.14 5.66 < -6 2 7 -2 6.80 5.88 2.40 < -6 2 7 -1 77.83 77.85 3.02 o -4 2 7 -2 0.35 0.62 2.16 < -4 2 7 -1 35.65 38.47 2.01 o -4 2 7 0 13.25 9.66 3.22 < -2 2 7 -2 0.02 1.03 1.87 < -2 2 7 -1 69.41 71.67 2.47 o -2 2 7 0 700.03 731.70 6.12 o 0 2 7 -2 0.82 0.73 1.74 < 0 2 7 -1 13.09 15.33 2.02 o 0 2 7 0 12.74 14.13 3.72 o 2 2 7 -2 0.90 -0.56 1.88 < 2 2 7 -1 7.94 9.72 3.73 < 4 2 7 -2 1.04 1.71 3.00 < -5 3 7 -2 3.55 6.88 2.41 < -5 3 7 -1 14.89 14.45 2.60 o -5 3 7 0 96.62 95.23 3.98 o -3 3 7 -2 10.64 13.33 1.70 o -3 3 7 -1 24.23 23.99 2.15 o -3 3 7 0 12.52 14.58 2.72 o -3 3 7 1 0.30 1.00 3.73 < -1 3 7 -2 1.49 1.07 2.16 < -1 3 7 -1 23.81 25.42 2.23 o -1 3 7 0 3.04 3.45 2.43 < 1 3 7 -2 3.31 2.19 1.74 < 1 3 7 -1 7.58 7.53 1.98 o 3 3 7 -2 0.13 -1.03 2.50 < -6 4 7 -2 1.54 1.42 2.58 < -4 4 7 -2 0.01 1.63 2.26 < -4 4 7 -1 11.03 11.00 2.19 o -4 4 7 0 262.46 280.65 4.38 o -2 4 7 -2 4.37 5.91 2.29 < -2 4 7 -1 20.21 22.06 2.65 o -2 4 7 0 8.27 8.43 2.43 o 0 4 7 -2 1.16 1.65 1.80 < 0 4 7 -1 3.27 3.22 1.91 < 2 4 7 -2 0.11 -0.14 2.15 < 2 4 7 -1 0.85 1.73 3.91 < -5 5 7 -2 5.91 8.85 2.49 o -5 5 7 -1 36.02 33.28 2.40 o -3 5 7 -2 1.30 0.19 1.99 < -3 5 7 -1 66.49 69.07 3.07 o -1 5 7 -2 4.10 3.49 2.40 < -1 5 7 -1 9.60 11.90 2.32 o 1 5 7 -2 0.07 -0.79 2.01 < 1 5 7 -1 76.48 79.06 3.18 o 3 5 7 -2 1.05 -2.18 3.91 < -4 6 7 -2 8.34 10.74 2.58 o -4 6 7 -1 10.86 11.87 4.56 < -2 6 7 -2 3.11 4.45 2.50 < -2 6 7 -1 13.83 12.82 2.82 o 0 6 7 -2 1.06 2.01 2.58 < 0 6 7 -1 7.91 8.84 3.36 < 2 6 7 -2 3.74 5.09 2.43 < -5 7 7 -2 0.58 0.79 4.54 < -3 7 7 -2 2.05 0.78 2.57 < -1 7 7 -2 1.94 0.67 2.69 < -1 -1 8 -2 1.70 0.95 3.97 < -2 0 8 -2 0.71 0.26 4.26 < -1 1 8 -2 2.91 2.07 4.71 < -2 2 8 -2 1.39 2.27 4.17 < -1 3 8 -2 6.12 7.62 5.17 < -2 4 8 -2 1.18 1.56 2.97 < #======================================================================= data_alpha3_single #======================================================================= # start Validation Reply Form #_vrf_PLAT213_alpha3_single #; #PROBLEM: Atom O4 has ADP max/min Ratio ..... 5.5 prolat #RESPONSE: This atom is disordered about the center of inversion. The #distribution of the displacement is not well described by a normal #distribution. #; # end Validation Reply Form # # 5. CHEMICAL DATA _chemical_name_systematic ? _chemical_name_common ? _chemical_formula_moiety ? _chemical_formula_structural ? _chemical_formula_analytical ? _chemical_formula_iupac ? _chemical_formula_sum 'Fe2 O7 P2' _chemical_formula_weight 285.6 _chemical_melting_point ? _chemical_compound_source ? _chemical_absolute_configuration . #======================================================================= # 6. CRYSTAL DATA _space_group_crystal_system triclinic _space_group_name_H-M_alt 'C-1' _space_group_name_Hall '-C 1' _space_group_IT_number 2 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,-y,-z 3 x+1/2,y+1/2,z 4 -x+1/2,-y+1/2,-z _cell_length_a 6.6161(5) _cell_length_b 8.4673(4) _cell_length_c 4.4825(3) _cell_angle_alpha 90.135(5) _cell_angle_beta 103.645(7) _cell_angle_gamma 91.616(7) _cell_volume 243.92(3) _cell_formula_units_Z 2 _cell_measurement_reflns_used 11950 _cell_measurement_theta_min 3.92 _cell_measurement_theta_max 41.04 _cell_measurement_temperature 400 _cell_special_details ? _exptl_crystal_density_diffrn 3.8891 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_F_000 276 _exptl_crystal_type_of_structure cryst _exptl_absorpt_coefficient_mu 6.582 _exptl_crystal_description 'plate' _exptl_crystal_colour 'light brown' _exptl_crystal_size_max 0.060 _exptl_crystal_size_mid 0.037 _exptl_crystal_size_min 0.010 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; STOE LANA, absorption correction by scaling of reflection intensities. J. Koziskova, F. Hahn, J. Richter, J. Kozisek, "Comparison of different absorption corrections on the model structure of tetrakis(\m~2~-acetato)- diaqua-di-copper(II)", Acta Chimica Slovaca, vol. 9, no. 2, 2016, pp. 136 - 140. Afterwards a spherical absorption correction was performed within STOE LANA. ; _exptl_absorpt_correction_T_min 0.5683 _exptl_absorpt_correction_T_max 0.6892 #======================================================================= # 7. EXPERIMENTAL DATA _exptl_special_details ? _diffrn_measurement_device 'Eulerian 4-circle diffractometer' _diffrn_measurement_device_type 'STOE STADIVARI' _diffrn_detector 'EIGER2 1M CDTE' _diffrn_detector_type ? _diffrn_detector_area_resol_mean 13.33 _diffrn_source 'Axo_Mo' _diffrn_source_type ? _diffrn_radiation_probe x-ray _diffrn_source_target ? _diffrn_source_voltage 60 _diffrn_source_current 0.830 _diffrn_source_power 0.050 _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_monochromator 'Graded multilayer mirror' _diffrn_radiation_polarisn_norm -90 _diffrn_radiation_collimation '1.2 0.6 mm diameter' _diffrn_ambient_temperature 400 _diffrn_measurement_method 'rotation method, \w scans' _diffrn_measurement_details ; 1960 frames, detector distance = 45 mm ; _diffrn_reflns_number 7257 _diffrn_reflns_theta_min 3.92 _diffrn_reflns_theta_max 41.04 _diffrn_reflns_theta_full 40.94 _diffrn_measured_fraction_theta_max 0.97 _diffrn_measured_fraction_theta_full 0.98 _diffrn_reflns_av_R_equivalents 0.0158 _diffrn_reflns_av_unetI/netI 0.0111 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_k_min -9 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_l_min -8 _diffrn_reflns_limit_l_max 8 _diffrn_reflns_reduction_process ? _diffrn_standards_number ? _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% ? loop_ _diffrn_standard_refln_index_h _diffrn_standard_refln_index_k _diffrn_standard_refln_index_l ? ? ? #_diffrn_reflns_av_sigmaI/netI 0.0111 #======================================================================= # 8. REFINEMENT DATA _refine_special_details ? _reflns_number_total 1563 _reflns_number_gt 1341 _reflns_threshold_expression 'I>3\s(I)' _refine_ls_structure_factor_coef Fsqd _refine_ls_R_factor_gt 0.0224 _refine_ls_wR_factor_gt 0.0634 _refine_ls_R_factor_all 0.0264 _refine_ls_wR_factor_ref 0.0645 _refine_ls_goodness_of_fit_ref 1.2014 _refine_ls_goodness_of_fit_gt 1.2778 _refine_ls_restrained_S_gt ? _refine_ls_restrained_S_all ? _refine_ls_number_reflns 1563 _refine_ls_number_parameters 53 _refine_ls_number_restraints 0 _refine_ls_number_constraints 0 _refine_ls_weighting_scheme sigma _refine_ls_weighting_details 'w=1/(\s^2^(I)+0.0016I^2^)' _refine_ls_hydrogen_treatment ? _refine_ls_shift/su_max 0.0094 _refine_ls_shift/su_mean 0.0010 _refine_diff_density_max 0.34 _refine_diff_density_min -0.18 _refine_ls_extinction_method 'B-C type 1 Gaussian isotropic (Becker & Coppens, 1974)' _refine_ls_extinction_coef 540(60) _refine_ls_extinction_expression ? _refine_ls_abs_structure_details ? _refine_ls_abs_structure_Flack ? _refine_ls_abs_structure_Rogers ? loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Fe 0.3463 0.8444 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' O 0.0106 0.0060 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' P 0.1023 0.0942 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' _computing_data_collection ; X-Area Pilatus3_SV 1.31.194.0 (STOE, 2023) ; _computing_cell_refinement ; X-Area Recipe 2.0.2 (STOE, 2024) ; _computing_data_reduction ; X-Area Integrate 2.5.18.0 (STOE, 2024) X-Area LANA 2.8.4 (STOE, 2024) ; _computing_publication_material ; STOE & Cie GmbH, X-Area, software package for collecting single-crystal or multi-domain crystal data on STOE area-detector diffractometers, for image processing, for the correction and scaling of reflection intensities and for outlier rejection, version 2.4, Darmstadt 2024 ; _computing_structure_solution SHELXT _computing_structure_refinement Jana2020 #======================================================================= # 9. ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_adp_type _atom_site_U_iso_or_equiv _atom_site_site_symmetry_multiplicity _atom_site_occupancy _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_disorder_assembly _atom_site_disorder_group Fe1 Fe 0.49493(3) 0.190859(18) 0.50929(4) Uani 0.01288(5) 4 1 d . . . P1 P 0.21345(4) 0.00054(3) -0.09088(6) Uani 0.00889(7) 4 1 d . . . O1 O 0.37354(13) 0.00275(10) 0.21365(18) Uani 0.01153(18) 4 1 d . . . O2 O 0.22526(16) 0.14811(10) -0.2778(2) Uani 0.0151(2) 4 1 d . . . O3 O 0.21855(18) -0.14925(11) -0.2769(2) Uani 0.0193(2) 4 1 d . . . O4 O 0 0 0 Uani 0.0513(9) 2 1 d . . . loop_ _atom_site_aniso_label _atom_site_aniso_type_symbol _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Fe1 Fe 0.01281(8) 0.00944(8) 0.01400(9) -0.00045(5) -0.00155(5) -0.00023(5) P1 P 0.00697(11) 0.01237(12) 0.00713(11) -0.00035(8) 0.00129(8) 0.00088(8) O1 O 0.0116(3) 0.0134(3) 0.0082(3) 0.0010(2) -0.0004(2) -0.0004(2) O2 O 0.0196(4) 0.0125(3) 0.0131(3) 0.0039(3) 0.0034(3) 0.0035(3) O3 O 0.0276(5) 0.0125(3) 0.0144(4) -0.0052(3) -0.0011(3) -0.0028(3) O4 O 0.0086(6) 0.114(2) 0.0357(10) 0.0056(9) 0.0132(7) 0.0186(12) #======================================================================= # 10. MOLECULAR GEOMETRY loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_1 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Fe1 O1 . . 2.0866(8) ? Fe1 O1 . 2_656 2.1371(9) ? Fe1 O2 . 1_556 2.2347(12) ? Fe1 O2 . 4_555 2.1128(10) ? Fe1 O3 . 3_556 2.0377(10) ? Fe1 O3 . 2_655 2.4021(13) ? P1 O1 . . 1.5173(8) ? P1 O2 . . 1.5164(10) ? P1 O3 . . 1.5218(10) ? P1 O4 . . 1.5593(4) ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_2 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag O1 Fe1 O1 . . 2_656 79.99(3) ? O1 Fe1 O2 . . 1_556 86.54(4) ? O1 Fe1 O2 . . 4_555 94.07(3) ? O1 Fe1 O3 . . 3_556 155.39(4) ? O1 Fe1 O3 . . 2_655 79.81(3) ? O1 Fe1 O2 2_656 . 1_556 84.18(3) ? O1 Fe1 O2 2_656 . 4_555 160.67(4) ? O1 Fe1 O3 2_656 . 3_556 94.44(3) ? O1 Fe1 O3 2_656 . 2_655 82.33(3) ? O2 Fe1 O2 1_556 . 4_555 77.08(4) ? O2 Fe1 O3 1_556 . 3_556 116.95(4) ? O2 Fe1 O3 1_556 . 2_655 162.25(3) ? O2 Fe1 O3 4_555 . 3_556 98.19(4) ? O2 Fe1 O3 4_555 . 2_655 114.94(4) ? O3 Fe1 O3 3_556 . 2_655 75.68(4) ? O1 P1 O2 . . . 112.88(5) ? O1 P1 O3 . . . 112.59(5) ? O1 P1 O4 . . . 104.34(4) ? O2 P1 O3 . . . 111.88(6) ? O2 P1 O4 . . . 107.10(4) ? O3 P1 O4 . . . 107.46(5) ? Fe1 O1 Fe1 . . 2_656 100.01(3) ? Fe1 O1 P1 . . . 130.27(5) ? Fe1 O1 P1 2_656 . . 129.20(5) ? Fe1 O2 Fe1 1_554 . 4_555 102.92(4) ? Fe1 O2 P1 1_554 . . 120.14(6) ? Fe1 O2 P1 4_555 . . 134.47(7) ? Fe1 O3 Fe1 3_444 . 2_655 104.32(4) ? Fe1 O3 P1 3_444 . . 133.27(7) ? Fe1 O3 P1 2_655 . . 119.95(6) ? P1 O4 P1 . . 2_555 180 ? #------------------------------------------------------------------------------- # STOE DATA #------------------------------------------------------------------------------- #_STOE_detector_size_x '8.0 cm' #_STOE_detector_size_y '7.7 cm' #_STOE_detector_pixelsize_x '0.075 mm' #_STOE_detector_pixelsize_y '0.075 mm' #_STOE_detector_distance '45.0 mm' #_STOE_measurement_tube_power '49.8 W' #_STOE_measurement_total_run_number 29 #_STOE_measurement_total_frame_number 1960 #_STOE_measurement_min_exposure_per_frame '30.0 s' #_STOE_measurement_max_exposure_per_frame '30.0 s' #_STOE_measurement_mean_exposure_per_frame '30.0 s' #_STOE_measurement_total_exposure_time '16.3 h' #_STOE_evaluation_integration_A 15.1 #_STOE_evaluation_integration_B -1.0 #_STOE_evaluation_integration_EMS 0.037 #_STOE_evaluation_LANA_point_group '-1' #_STOE_evaluation_LANA_FS_max_order 3 #_STOE_evaluation_LANA_DXS_max_order - #_STOE_evaluation_LANA_DYS_max_order - #_STOE_evaluation_LANA_BIS_l_even_max 4 #_STOE_evaluation_LANA_BIS_l_odd_max 1 #_STOE_evaluation_LANA_BOS_l_even_max 4 #_STOE_evaluation_LANA_BOS_l_odd_max 1 #_STOE_evaluation_LANA_OR_c1 0.035 #_STOE_evaluation_LANA_OR_c2 0 #_STOE_evaluation_LANA_OR_c3 0 #_STOE_evaluation_LANA_OR_c4 0.7 #_STOE_evaluation_LANA_max_2theta_available 82.1 #_STOE_evaluation_LANA_max_2theta_desired 82.1 #_STOE_evaluation_LANA_number_refls_total 8369 #_STOE_evaluation_LANA_number_refls_outliers 1112 #_STOE_evaluation_LANA_number_refls_after_OR 7257 #_STOE_evaluation_LANA_number_refls_unique 1567 #_STOE_evaluation_LANA_number_refls_written 7257 #_STOE_evaluation_LANA_completeness 97.5 #_STOE_evaluation_LANA_mean_redundancy 4.6 #_STOE_evaluation_LANA_table #; #---------------------------------------------------------------------------- #2Theta 11.4 19.8 28.2 36.6 45.0 53.4 61.8 70.2 78.6 #---------------------------------------------------------------------------- #<Resolution> 3.53 2.03 1.42 1.13 0.91 0.79 0.69 0.62 0.57 #N(total) 108 353 490 792 907 1403 1571 1547 1198 #<Redundancy> 7.3 7.2 5.3 5.8 4.5 5.3 4.9 4.1 3.5 #Complet. [%%] 100.0 100.0 100.0 99.2 98.8 100.0 100.0 100.0 89.5 #<I/sigma> 265.9 169.9 149.1 76.8 43.7 33.2 19.3 13.4 6.8 #R(int) 0.010 0.013 0.014 0.014 0.015 0.016 0.021 0.026 0.039 #---------------------------------------------------------------------------- #; #======================================================================= # 11. STRUCTURE-FACTOR LIST loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_include_status 0 0 1 1551.47 1567.17 2.96 o 0 0 2 1851.37 1618.74 3.94 o 0 0 3 2473.54 2551.13 6.14 o 0 0 4 1917.09 1928.63 8.12 o 0 0 5 2368.34 2363.71 16.75 o 0 0 6 2.58 1.51 3.35 < 0 0 7 405.81 421.27 9.89 o 0 0 8 86.92 91.08 14.90 o 0 2 -7 44.14 40.84 6.19 o 0 2 -6 514.21 518.40 11.40 o 0 2 -5 25.54 30.97 2.68 o 0 2 -4 1179.71 1235.62 7.08 o 0 2 -3 460.73 458.97 3.36 o 0 2 -2 800.97 779.58 2.87 o 0 2 -1 13334.70 14333.00 8.47 o 0 2 0 36.58 39.70 0.50 o 0 2 1 14342.30 14942.40 8.37 o 0 2 2 1681.33 1662.41 4.26 o 0 2 3 1145.25 1142.76 4.39 o 0 2 4 2097.81 2066.90 7.45 o 0 2 5 254.12 254.52 6.20 o 0 2 6 1109.17 1146.37 7.40 o 0 2 7 4.28 6.86 6.36 < 0 4 -7 110.04 104.48 7.37 o 0 4 -6 252.18 261.02 7.87 o 0 4 -5 0.76 5.52 3.51 < 0 4 -4 513.58 509.11 7.89 o 0 4 -3 138.62 117.09 1.68 o 0 4 -2 589.17 629.50 2.02 o 0 4 -1 1848.15 1917.20 2.73 o 0 4 0 1320.26 1233.72 2.38 o 0 4 1 1067.74 1052.02 3.22 o 0 4 2 1291.98 1359.69 4.57 o 0 4 3 748.42 717.17 3.53 o 0 4 4 31.00 35.15 3.35 o 0 4 5 205.62 215.42 3.69 o 0 4 6 9.81 8.03 4.02 < 0 4 7 493.05 499.57 7.88 o 0 6 -7 299.96 313.86 9.05 o 0 6 -6 2.09 5.19 5.52 < 0 6 -5 1132.73 1150.94 8.07 o 0 6 -4 490.02 506.07 5.54 o 0 6 -3 958.29 921.99 5.55 o 0 6 -2 515.04 535.62 2.69 o 0 6 -1 73.87 65.47 2.01 o 0 6 0 9278.07 8880.08 10.21 o 0 6 1 46.66 37.84 1.34 o 0 6 2 186.59 201.24 2.18 o 0 6 3 348.15 340.04 7.88 o 0 6 4 147.38 138.84 3.35 o 0 6 5 530.87 524.15 4.86 o 0 6 6 102.96 108.16 5.02 o 0 6 7 86.10 82.71 4.86 o 0 8 -6 659.63 662.33 10.40 o 0 8 -5 72.07 71.82 4.85 o 0 8 -4 947.71 968.49 6.38 o 0 8 -3 712.91 692.94 5.88 o 0 8 -2 1411.02 1374.27 6.24 o 0 8 -1 3710.54 3664.21 6.49 o 0 8 0 26.68 30.30 1.67 o 0 8 1 3354.77 3241.89 9.71 o 0 8 2 1339.79 1308.70 6.91 o 0 8 3 731.22 711.45 5.54 o 0 8 4 723.47 725.35 5.88 o 0 8 5 54.93 51.73 3.68 o 0 8 6 609.62 608.68 8.39 o 0 10 -6 7.96 4.85 6.53 < 0 10 -5 168.53 157.26 6.70 o 0 10 -4 3.66 2.68 3.35 < 0 10 -3 762.07 786.04 9.57 o 0 10 -2 1126.23 1110.74 8.41 o 0 10 -1 52.92 57.42 5.36 o 0 10 0 1447.41 1450.66 8.09 o 0 10 1 100.62 107.33 3.18 o 0 10 2 1336.21 1310.98 7.41 o 0 10 3 945.88 922.20 6.38 o 0 10 4 97.32 92.42 5.69 o 0 10 5 315.43 317.39 5.70 o 0 10 6 53.63 54.41 6.70 o 0 12 -5 32.42 40.01 11.55 o 0 12 -4 13.30 11.38 7.87 < 0 12 -3 9.62 13.22 7.03 < 0 12 -2 10.48 9.04 5.69 < 0 12 -1 269.01 287.84 8.88 o 0 12 0 145.52 133.97 6.20 o 0 12 1 310.35 310.68 6.03 o 0 12 2 68.51 72.82 4.02 o 0 12 3 32.48 31.64 4.02 o 0 12 4 87.21 102.13 5.52 o 0 12 5 7.88 11.21 10.54 < 0 14 -3 73.27 70.98 11.22 o 0 14 -2 188.92 203.17 10.55 o 0 14 -1 293.05 310.99 10.72 o 0 14 0 67.56 74.00 9.21 o 0 14 1 184.86 178.04 7.70 o 0 14 2 103.11 105.82 8.20 o 0 14 3 33.98 27.62 9.37 < 1 -15 -2 196.85 211.38 11.39 o 1 -15 -1 116.36 123.74 8.71 o 1 -15 0 102.16 112.01 10.05 o 1 -15 1 184.15 189.93 11.39 o 1 -13 -4 13.12 9.88 5.19 < 1 -13 -3 471.14 478.90 8.22 o 1 -13 -2 263.19 254.49 5.86 o 1 -13 -1 748.74 765.62 10.58 o 1 -13 0 514.37 533.14 9.56 o 1 -13 1 98.72 96.11 9.21 o 1 -13 2 686.42 734.56 13.76 o 1 -13 3 105.67 106.99 11.22 o 1 -13 4 509.60 479.66 13.25 o 1 -11 -5 43.55 46.03 5.86 o 1 -11 -4 469.68 481.90 8.38 o 1 -11 -3 9.36 14.06 3.18 o 1 -11 -2 637.32 649.22 5.54 o 1 -11 -1 641.01 628.45 5.37 o 1 -11 0 458.69 477.74 5.87 o 1 -11 1 508.15 473.63 7.21 o 1 -11 2 16.40 17.74 3.51 o 1 -11 3 1419.40 1409.59 10.94 o 1 -11 4 182.04 185.24 9.55 o 1 -11 5 111.51 113.86 7.03 o 1 -9 -6 1.09 0.33 5.52 < 1 -9 -5 2.02 3.01 4.52 < 1 -9 -4 264.17 268.41 4.86 o 1 -9 -3 460.84 453.11 5.70 o 1 -9 -2 56.76 61.61 2.34 o 1 -9 -1 1.34 -0.67 2.18 < 1 -9 0 50.81 47.04 2.51 o 1 -9 1 28.64 29.80 1.84 o 1 -9 2 887.93 868.39 6.05 o 1 -9 3 244.32 247.96 4.02 o 1 -9 4 244.45 251.63 4.36 o 1 -9 5 182.77 193.62 5.53 o 1 -9 6 6.73 12.05 6.03 < 1 -7 -7 2.60 3.01 4.85 < 1 -7 -6 485.14 488.31 6.71 o 1 -7 -5 921.90 954.51 6.38 o 1 -7 -4 38.82 39.17 2.51 o 1 -7 -3 1080.28 1061.49 5.55 o 1 -7 -2 381.09 376.87 5.20 o 1 -7 -1 2095.21 2015.48 6.10 o 1 -7 0 938.73 968.05 3.54 o 1 -7 1 28.38 25.44 1.17 o 1 -7 2 1264.71 1218.63 4.72 o 1 -7 3 15.59 18.24 3.35 o 1 -7 4 798.02 781.90 6.38 o 1 -7 5 24.43 26.95 4.85 o 1 -7 6 101.61 111.51 7.20 o 1 -7 7 74.83 66.63 12.89 o 1 -5 -7 493.18 482.96 7.88 o 1 -5 -6 211.02 223.96 4.86 o 1 -5 -5 244.30 249.80 4.36 o 1 -5 -4 3211.01 3218.39 11.05 o 1 -5 -3 275.89 264.20 3.02 o 1 -5 -2 3784.08 3561.30 7.74 o 1 -5 -1 3975.17 4079.34 8.31 o 1 -5 0 3592.98 3596.04 6.74 o 1 -5 1 4770.47 4606.16 11.83 o 1 -5 2 182.06 182.65 2.18 o 1 -5 3 4925.97 4831.25 16.16 o 1 -5 4 209.45 199.69 3.85 o 1 -5 5 329.09 322.45 6.37 o 1 -5 6 537.47 536.71 10.40 o 1 -5 7 14.46 10.71 6.36 < 1 -3 -8 275.69 245.30 12.90 o 1 -3 -7 6.83 5.86 5.36 < 1 -3 -6 180.70 202.49 4.52 o 1 -3 -5 503.36 531.58 5.20 o 1 -3 -4 57.52 67.47 2.01 o 1 -3 -3 7273.78 7093.98 9.32 o 1 -3 -2 1719.65 1791.21 5.10 o 1 -3 0 4636.75 4358.10 7.33 o 1 -3 1 6996.61 7215.72 8.90 o 1 -3 2 12366.10 12143.80 24.68 o 1 -3 3 82.70 81.05 2.01 o 1 -3 4 1771.21 1742.91 8.61 o 1 -3 5 1187.84 1204.29 8.41 o 1 -3 6 292.59 315.85 8.55 o 1 -3 7 418.09 422.47 10.90 o 1 -1 -8 34.29 30.80 10.88 < 1 -1 -7 137.91 140.16 7.70 o 1 -1 -6 102.91 109.84 4.69 o 1 -1 -5 227.55 237.74 4.19 o 1 -1 -4 1442.55 1476.71 5.40 o 1 -1 -3 12.81 20.25 1.17 o 1 -1 -2 227.44 215.32 1.34 o 1 -1 -1 14.37 21.09 0.50 o 1 -1 0 368.06 362.29 1.52 o 1 -1 1 6963.79 7147.62 9.77 o 1 -1 2 51.51 61.29 1.84 o 1 -1 3 3474.49 3451.26 8.58 o 1 -1 4 19.70 27.79 2.85 o 1 -1 5 273.16 278.33 6.20 o 1 -1 6 742.34 761.77 12.09 o 1 -1 7 9.22 17.57 6.19 < 1 1 -8 14.50 19.92 7.03 < 1 1 -7 564.65 562.43 8.05 o 1 1 -6 19.55 31.63 4.52 o 1 1 -5 11.35 25.44 3.51 o 1 1 -4 3293.10 3205.63 8.70 o 1 1 -3 290.94 305.14 2.52 o 1 1 -2 1166.73 1067.05 3.73 o 1 1 -1 392.39 385.75 1.86 o 1 1 0 687.36 698.94 2.22 o 1 1 1 5942.29 6513.10 6.65 o 1 1 2 316.95 327.27 2.35 o 1 1 3 2009.81 2003.44 6.11 o 1 1 4 313.88 310.48 4.53 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1.67 o 3 3 3 2974.09 2884.52 9.86 o 3 3 4 1539.44 1560.92 8.76 o 3 3 5 86.98 87.90 3.85 o 3 3 6 205.68 214.74 7.04 o 3 3 7 7.98 7.03 5.86 < 3 5 -7 22.41 20.25 5.69 o 3 5 -6 11.71 10.88 4.18 < 3 5 -5 1498.36 1490.88 9.60 o 3 5 -4 15.47 13.56 2.68 o 3 5 -3 2223.63 2080.41 6.27 o 3 5 -2 748.62 720.75 3.03 o 3 5 -1 3188.66 3103.11 6.67 o 3 5 0 3115.22 2994.82 8.38 o 3 5 1 280.71 304.48 3.02 o 3 5 2 5042.52 4709.25 26.14 o 3 5 3 535.57 533.07 6.54 o 3 5 4 596.22 575.84 6.54 o 3 5 5 761.45 768.02 8.06 o 3 5 6 138.35 141.34 5.86 o 3 7 -7 51.64 44.19 7.03 o 3 7 -6 32.41 27.79 5.69 o 3 7 -5 420.63 434.88 7.04 o 3 7 -4 584.09 542.78 6.04 o 3 7 -3 46.43 39.00 2.34 o 3 7 -2 578.16 541.19 4.36 o 3 7 -1 14.90 12.22 1.51 o 3 7 0 3.58 4.18 1.67 < 3 7 1 2777.04 2672.49 13.75 o 3 7 2 11.84 11.21 2.51 o 3 7 3 545.67 554.27 5.20 o 3 7 4 97.78 92.25 3.35 o 3 7 5 71.32 72.49 5.19 o 3 7 6 421.83 418.63 8.05 o 3 9 -6 210.29 225.30 8.21 o 3 9 -5 0.61 3.85 5.19 < 3 9 -4 575.87 590.83 7.55 o 3 9 -3 13.60 11.72 3.51 o 3 9 -2 310.15 310.72 6.20 o 3 9 -1 174.38 198.65 4.02 o 3 9 0 24.50 25.44 2.51 o 3 9 1 455.56 452.28 4.70 o 3 9 2 317.84 337.52 3.35 o 3 9 3 212.82 216.25 3.52 o 3 9 4 42.24 37.16 3.85 o 3 9 5 32.43 33.14 4.02 o 3 11 -5 432.45 428.20 14.59 o 3 11 -4 56.29 61.27 10.21 o 3 11 -3 915.27 912.10 13.10 o 3 11 -2 263.07 260.19 7.54 o 3 11 -1 396.40 416.40 8.55 o 3 11 0 570.56 578.41 6.71 o 3 11 1 78.31 76.68 4.35 o 3 11 2 1356.97 1395.10 9.25 o 3 11 3 70.46 62.61 3.68 o 3 11 4 55.38 52.40 4.19 o 3 13 -4 400.45 367.30 20.62 o 3 13 -2 502.59 529.43 11.40 o 3 13 -1 117.43 110.35 7.37 o 3 13 0 148.81 146.20 8.71 o 3 13 1 1168.69 1232.17 15.97 o 3 13 2 135.49 134.63 8.71 o 3 13 3 327.55 309.87 10.39 o 4 -14 -3 56.21 65.45 13.22 o 4 -14 -2 3.82 4.69 5.86 < 4 -14 -1 200.01 203.35 8.04 o 4 -14 0 0.79 0.33 7.36 < 4 -14 1 3.34 5.69 7.87 < 4 -12 -4 66.80 65.62 5.52 o 4 -12 -3 303.87 292.74 6.03 o 4 -12 -2 11.82 13.89 4.02 o 4 -12 -1 316.63 311.52 6.87 o 4 -12 0 12.56 15.06 4.52 o 4 -12 1 29.49 30.30 4.52 o 4 -12 2 76.12 91.07 5.19 o 4 -12 3 2.67 2.51 5.02 < 4 -10 -6 112.89 112.69 6.53 o 4 -10 -5 359.99 356.50 6.70 o 4 -10 -4 125.19 113.19 6.53 o 4 -10 -3 67.78 71.15 4.02 o 4 -10 -2 2262.68 2160.07 10.13 o 4 -10 -1 190.39 207.03 4.02 o 4 -10 0 423.36 433.40 4.36 o 4 -10 1 290.54 292.57 3.85 o 4 -10 2 423.04 402.02 5.36 o 4 -10 3 872.32 874.99 8.90 o 4 -10 4 2.27 1.84 4.18 < 4 -10 5 231.55 218.28 8.21 o 4 -8 -6 375.19 374.12 7.38 o 4 -8 -5 52.23 45.87 4.35 o 4 -8 -4 222.98 214.76 5.36 o 4 -8 -3 1305.11 1267.01 8.08 o 4 -8 -2 60.12 64.45 2.68 o 4 -8 -1 2651.24 2538.18 10.68 o 4 -8 0 516.58 559.85 4.36 o 4 -8 1 638.48 628.76 6.55 o 4 -8 2 1036.64 989.13 6.89 o 4 -8 3 366.90 343.95 5.53 o 4 -8 4 1227.70 1204.00 10.60 o 4 -8 5 11.09 9.88 4.52 < 4 -6 -7 30.45 30.46 5.69 o 4 -6 -6 79.27 80.03 4.35 o 4 -6 -5 213.03 224.46 4.69 o 4 -6 -4 215.10 201.70 3.69 o 4 -6 -3 52.85 56.92 2.18 o 4 -6 -2 1288.14 1271.66 6.24 o 4 -6 -1 75.87 73.00 3.01 o 4 -6 0 1404.07 1425.41 9.95 o 4 -6 1 797.39 778.99 12.27 o 4 -6 2 152.76 138.01 3.35 o 4 -6 3 533.24 505.77 5.70 o 4 -6 4 4.38 3.18 3.85 < 4 -6 5 1017.22 1012.95 11.43 o 4 -6 6 79.52 75.67 7.03 o 4 -4 -7 261.88 253.49 6.70 o 4 -4 -6 28.78 34.31 4.69 o 4 -4 -5 383.37 364.45 6.20 o 4 -4 -4 19.89 24.27 3.18 o 4 -4 -3 152.02 168.51 2.35 o 4 -4 -2 4466.13 4407.33 8.61 o 4 -4 -1 34.04 35.99 1.84 o 4 -4 0 53.66 60.78 2.18 o 4 -4 1 46.53 44.20 1.67 o 4 -4 2 59.35 56.42 5.86 o 4 -4 3 493.10 508.62 6.54 o 4 -4 4 421.12 430.21 6.20 o 4 -4 5 47.35 52.06 6.70 o 4 -4 6 38.67 41.51 7.03 o 4 -2 -8 286.34 273.12 12.23 o 4 -2 -7 19.78 24.27 5.02 o 4 -2 -6 695.88 677.72 6.55 o 4 -2 -5 202.11 185.44 3.35 o 4 -2 -4 908.98 835.39 5.89 o 4 -2 -3 4249.51 4101.09 8.08 o 4 -2 -1 6562.94 6522.29 9.01 o 4 -2 0 1647.82 1710.77 6.28 o 4 -2 1 2329.23 2191.42 6.13 o 4 -2 2 1006.85 1074.53 5.39 o 4 -2 3 126.16 126.94 4.02 o 4 -2 4 1619.34 1762.48 9.27 o 4 -2 5 1.29 2.68 3.68 < 4 -2 6 166.89 169.32 7.54 o 4 0 -8 18.97 24.10 7.36 o 4 0 -7 278.51 265.07 7.87 o 4 0 -6 2.52 1.84 3.51 < 4 0 -5 1193.27 1195.68 9.42 o 4 0 -4 2280.55 2173.66 9.82 o 4 0 -3 213.91 221.40 3.18 o 4 0 -2 6179.46 6176.42 10.36 o 4 0 -1 99.13 86.77 2.85 o 4 0 0 8652.06 8472.19 11.53 o 4 0 1 4590.34 4790.40 9.52 o 4 0 2 1470.93 1533.93 7.26 o 4 0 3 1447.42 1542.92 10.12 o 4 0 4 103.46 99.79 3.18 o 4 0 5 2161.08 2321.87 13.51 o 4 0 6 235.92 247.60 6.70 o 4 2 -8 117.84 108.84 7.54 o 4 2 -7 16.67 21.59 5.19 o 4 2 -6 182.90 191.61 5.69 o 4 2 -5 1.15 9.54 3.51 < 4 2 -4 253.05 268.80 5.36 o 4 2 -3 2727.31 2711.42 6.98 o 4 2 -2 596.18 620.64 3.87 o 4 2 -1 3823.63 3889.17 11.22 o 4 2 0 1032.32 1076.33 3.88 o 4 2 1 2164.79 2251.10 7.31 o 4 2 2 916.29 983.17 5.72 o 4 2 3 124.64 116.56 3.18 o 4 2 4 2046.93 2111.03 8.95 o 4 2 5 36.23 36.99 5.52 o 4 2 6 330.33 352.10 7.37 o 4 4 -7 18.07 21.59 5.52 o 4 4 -6 135.72 158.41 4.69 o 4 4 -5 0.70 9.54 3.01 o 4 4 -4 194.18 206.55 3.69 o 4 4 -3 1206.97 1251.48 6.40 o 4 4 -2 1899.16 1803.12 6.27 o 4 4 -1 602.98 617.42 3.70 o 4 4 0 11.35 10.21 1.51 o 4 4 1 171.47 178.10 3.02 o 4 4 2 34.16 30.63 2.68 o 4 4 3 643.80 657.50 6.88 o 4 4 4 223.65 224.48 5.70 o 4 4 5 205.22 218.26 6.03 o 4 4 6 1.13 -0.67 6.36 < 4 6 -7 255.41 256.17 8.04 o 4 6 -6 1.69 1.84 4.69 < 4 6 -5 715.12 746.44 6.88 o 4 6 -4 979.76 1033.70 8.07 o 4 6 -3 63.99 59.10 3.35 o 4 6 -2 2349.82 2203.07 11.35 o 4 6 -1 6.61 7.03 1.51 o 4 6 0 2174.77 2141.08 6.44 o 4 6 1 1023.83 1055.71 10.60 o 4 6 2 186.76 188.12 3.69 o 4 6 3 427.05 411.29 5.20 o 4 6 4 8.96 10.88 3.35 o 4 6 5 748.43 753.20 8.73 o 4 6 6 18.70 20.92 5.86 o 4 8 -6 485.83 491.17 8.89 o 4 8 -5 58.51 59.26 6.19 o 4 8 -4 312.97 307.17 6.20 o 4 8 -3 1680.24 1657.67 9.78 o 4 8 -2 85.99 84.38 4.19 o 4 8 -1 2598.36 2512.86 10.33 o 4 8 0 586.83 611.35 4.87 o 4 8 1 876.97 874.34 6.38 o 4 8 2 925.94 911.82 6.38 o 4 8 3 311.67 295.77 5.03 o 4 8 4 1264.62 1238.66 9.25 o 4 8 5 17.36 14.39 4.85 < 4 10 -6 11.28 10.21 9.04 < 4 10 -5 193.33 179.55 9.38 o 4 10 -4 21.61 15.23 7.36 < 4 10 -3 1.32 1.84 5.19 < 4 10 -2 1675.39 1562.87 12.97 o 4 10 -1 109.21 118.88 5.19 o 4 10 0 341.77 331.35 5.53 o 4 10 1 154.24 151.56 3.52 o 4 10 2 456.15 455.22 5.87 o 4 10 3 994.66 998.07 7.56 o 4 10 4 16.03 14.90 3.85 o 4 12 -4 11.48 17.41 10.04 < 4 12 -3 55.06 48.21 10.04 o 4 12 -2 115.68 109.34 10.38 o 4 12 -1 122.55 129.44 8.20 o 4 12 0 8.64 9.87 6.53 < 4 12 1 15.33 17.91 6.53 < 4 12 2 55.93 62.78 5.69 o 4 12 3 0.81 0.33 4.52 < 4 14 -2 23.02 30.80 10.88 < 4 14 -1 357.58 384.49 17.10 o 4 14 0 19.66 19.42 7.87 < 4 14 1 33.60 40.34 12.05 o 5 -13 -3 156.41 156.92 6.03 o 5 -13 -2 138.01 128.11 6.53 o 5 -13 -1 305.11 328.94 7.04 o 5 -13 0 820.46 834.88 14.44 o 5 -13 1 9.62 8.54 6.03 < 5 -13 2 289.49 288.54 8.04 o 5 -11 -5 3.11 4.85 5.69 < 5 -11 -4 184.22 187.25 6.87 o 5 -11 -3 5.66 3.85 4.18 < 5 -11 -2 134.52 146.19 6.20 o 5 -11 -1 428.90 423.15 5.87 o 5 -11 0 40.58 45.53 4.02 o 5 -11 1 782.41 811.05 7.55 o 5 -11 2 11.95 12.39 4.18 < 5 -11 3 162.32 156.42 5.86 o 5 -11 4 377.80 288.48 16.59 o 5 -9 -6 178.39 172.34 5.69 o 5 -9 -5 13.28 15.40 4.52 o 5 -9 -4 91.02 82.88 5.36 o 5 -9 -3 33.56 39.00 3.68 o 5 -9 -2 19.41 22.26 3.51 o 5 -9 -1 93.26 89.58 3.35 o 5 -9 0 271.13 268.26 4.19 o 5 -9 1 180.92 187.42 4.19 o 5 -9 2 243.29 228.34 4.52 o 5 -9 3 10.62 11.05 4.18 < 5 -9 4 3.39 6.53 4.85 < 5 -7 -7 93.46 85.89 6.36 o 5 -7 -6 2.63 4.52 4.18 < 5 -7 -5 1005.11 983.01 6.89 o 5 -7 -4 100.46 87.74 3.01 o 5 -7 -3 335.75 328.18 4.86 o 5 -7 -2 155.49 152.91 4.02 o 5 -7 -1 488.10 518.02 4.86 o 5 -7 0 2623.47 2789.26 9.15 o 5 -7 1 124.10 114.37 3.85 o 5 -7 2 370.11 348.16 5.53 o 5 -7 3 185.92 175.70 4.86 o 5 -7 4 117.09 107.67 7.70 o 5 -7 5 139.96 142.84 6.87 o 5 -5 -7 26.68 28.62 5.86 o 5 -5 -6 691.60 694.63 9.90 o 5 -5 -5 47.23 44.86 3.01 o 5 -5 -4 1268.32 1211.09 7.41 o 5 -5 -3 458.52 444.51 5.03 o 5 -5 -2 1397.06 1422.31 9.44 o 5 -5 -1 2428.49 2493.85 9.84 o 5 -5 0 172.21 195.66 4.02 o 5 -5 1 4486.49 4467.28 16.43 o 5 -5 2 211.86 191.99 4.19 o 5 -5 3 653.06 605.18 6.04 o 5 -5 4 730.17 718.41 9.23 o 5 -5 5 169.76 163.46 7.37 o 5 -5 6 370.51 331.89 13.24 o 5 -3 -7 229.98 249.10 9.55 o 5 -3 -6 33.48 33.98 5.02 o 5 -3 -5 418.75 409.77 7.04 o 5 -3 -4 46.90 50.39 3.68 o 5 -3 -3 1880.92 1942.30 7.10 o 5 -3 -2 1072.05 1119.33 5.56 o 5 -3 -1 104.80 127.62 2.18 o 5 -3 0 3673.82 3830.40 8.22 o 5 -3 1 54.41 49.89 2.34 o 5 -3 2 3610.33 3437.47 15.67 o 5 -3 3 621.30 634.88 6.55 o 5 -3 4 127.18 121.90 4.19 o 5 -3 5 544.08 554.00 9.22 o 5 -3 6 153.34 163.62 8.37 o 5 -1 -8 36.10 28.62 8.70 o 5 -1 -7 15.87 19.92 7.36 < 5 -1 -6 135.42 144.68 5.69 o 5 -1 -5 497.17 474.33 7.88 o 5 -1 -4 53.23 83.37 4.19 o 5 -1 -3 4.30 24.10 2.01 o 5 -1 -1 186.78 220.71 3.02 o 5 -1 0 1469.00 1480.91 5.58 o 5 -1 1 3143.76 3008.66 8.02 o 5 -1 2 5.54 7.70 4.35 < 5 -1 3 152.16 153.41 4.02 o 5 -1 4 107.41 112.18 4.19 o 5 -1 5 15.90 17.07 4.69 o 5 -1 6 382.59 383.02 10.90 o 5 1 -8 21.09 25.94 6.70 o 5 1 -7 52.19 60.43 6.19 o 5 1 -6 623.52 609.56 8.72 o 5 1 -5 6.90 25.27 3.51 o 5 1 -4 934.65 928.26 5.88 o 5 1 -3 526.51 470.03 5.04 o 5 1 -2 1146.73 1202.19 6.07 o 5 1 -1 1214.28 1233.22 7.93 o 5 1 0 413.36 428.30 3.69 o 5 1 1 3984.72 4098.49 9.43 o 5 1 2 15.34 19.75 2.68 o 5 1 3 132.37 139.33 3.18 o 5 1 4 62.94 72.15 3.35 o 5 1 5 1.49 -2.68 6.19 < 5 1 6 171.58 180.21 10.38 o 5 3 -7 447.59 445.82 9.22 o 5 3 -6 8.19 6.86 4.02 < 5 3 -5 734.44 725.76 7.72 o 5 3 -4 216.93 211.10 4.86 o 5 3 -2 1917.71 1898.64 8.97 o 5 3 -1 320.42 348.65 3.19 o 5 3 0 4204.45 4263.66 8.07 o 5 3 1 149.81 150.42 3.02 o 5 3 2 3692.69 3805.33 12.27 o 5 3 3 628.51 658.54 6.71 o 5 3 4 95.00 96.61 4.19 o 5 3 5 430.26 442.26 8.55 o 5 3 6 99.13 104.81 7.37 o 5 5 -7 13.17 11.72 6.69 < 5 5 -6 529.03 491.91 8.72 o 5 5 -5 2.00 2.68 3.18 < 5 5 -4 800.40 775.09 7.22 o 5 5 -3 247.64 234.76 6.03 o 5 5 -2 1242.79 1211.41 7.07 o 5 5 -1 1923.24 1845.95 7.44 o 5 5 0 45.11 42.35 3.52 o 5 5 1 4021.53 4017.78 20.99 o 5 5 2 307.06 312.57 5.70 o 5 5 3 661.80 651.50 6.88 o 5 5 4 672.96 662.03 10.91 o 5 5 5 232.20 225.65 6.53 o 5 7 -7 0.02 3.85 8.03 < 5 7 -6 79.15 85.89 7.37 o 5 7 -5 345.55 310.55 9.22 o 5 7 -4 25.90 37.16 3.68 o 5 7 -3 39.01 33.31 3.35 o 5 7 -2 4.45 7.70 2.85 < 5 7 -1 77.54 70.49 2.51 o 5 7 0 1787.18 1751.05 8.94 o 5 7 1 193.19 182.25 3.35 o 5 7 2 259.94 250.48 4.52 o 5 7 3 181.22 178.88 4.69 o 5 7 4 215.90 208.38 5.53 o 5 7 5 241.58 249.45 6.20 o 5 9 -6 0.97 -3.01 9.37 < 5 9 -5 214.95 220.11 10.39 o 5 9 -4 0.99 -2.85 9.21 < 5 9 -3 502.79 535.31 7.88 o 5 9 -2 88.63 94.26 4.35 o 5 9 -1 0.64 2.51 3.35 < 5 9 0 525.16 516.94 6.71 o 5 9 1 50.67 46.20 3.01 o 5 9 2 316.75 320.07 6.37 o 5 9 3 5.60 3.68 3.68 < 5 9 4 12.41 15.57 5.02 o 5 11 -5 57.59 55.24 11.55 o 5 11 -4 438.68 451.67 15.09 o 5 11 -3 54.15 52.56 8.70 o 5 11 -2 381.90 424.24 10.56 o 5 11 -1 683.50 699.47 9.57 o 5 11 0 88.15 98.11 7.37 o 5 11 1 918.20 926.55 10.75 o 5 11 2 43.41 42.69 4.18 o 5 11 3 169.05 162.79 5.36 o 5 13 -2 82.82 71.99 12.72 o 5 13 -1 261.57 280.80 14.58 o 5 13 0 891.82 938.60 14.61 o 5 13 1 19.78 18.24 8.03 < 6 -12 -4 204.52 189.62 8.88 o 6 -12 -3 8.48 12.89 5.52 < 6 -12 -2 217.17 219.27 6.37 o 6 -12 -1 33.81 32.14 4.69 o 6 -12 0 84.72 95.10 5.19 o 6 -12 1 46.62 48.55 4.85 o 6 -12 2 1.98 0.50 4.52 < 6 -10 -5 117.78 122.40 6.87 o 6 -10 -4 117.41 115.54 5.86 o 6 -10 -3 1040.01 1000.10 9.41 o 6 -10 -2 13.57 16.74 4.35 o 6 -10 -1 352.28 376.10 6.37 o 6 -10 0 474.13 485.27 7.38 o 6 -10 1 492.63 516.66 7.38 o 6 -10 2 462.74 465.13 6.87 o 6 -10 3 6.44 6.86 4.69 < 6 -8 -6 0.71 0.33 5.52 < 6 -8 -5 117.89 122.74 5.53 o 6 -8 -4 723.37 721.58 9.57 o 6 -8 -3 13.99 14.56 3.35 o 6 -8 -2 991.57 1003.62 7.23 o 6 -8 -1 188.10 202.67 4.19 o 6 -8 0 640.02 678.63 9.06 o 6 -8 1 841.68 832.98 7.56 o 6 -8 2 183.23 186.92 5.36 o 6 -8 3 965.00 962.17 12.60 o 6 -8 4 13.65 12.55 4.85 < 6 -6 -7 29.95 21.59 6.19 o 6 -6 -6 161.07 188.24 6.03 o 6 -6 -5 2.60 4.02 3.51 < 6 -6 -4 149.34 153.74 3.52 o 6 -6 -3 629.91 622.79 6.21 o 6 -6 -2 0.27 -1.51 3.01 < 6 -6 -1 480.09 492.81 4.70 o 6 -6 0 66.80 70.98 3.52 o 6 -6 1 38.08 36.16 4.02 o 6 -6 2 778.45 711.92 9.23 o 6 -6 3 1.25 2.34 3.85 < 6 -6 4 701.50 652.36 8.90 o 6 -6 5 15.71 15.73 5.69 < 6 -4 -7 4.44 15.40 6.36 < 6 -4 -6 170.57 163.96 6.53 o 6 -4 -5 41.90 46.54 3.35 o 6 -4 -4 17.84 23.60 3.18 o 6 -4 -3 1547.02 1491.58 7.92 o 6 -4 -2 123.64 150.39 4.86 o 6 -4 -1 72.05 78.36 3.18 o 6 -4 0 184.70 192.65 4.02 o 6 -4 1 145.78 151.90 5.02 o 6 -4 2 313.95 296.31 5.70 o 6 -4 3 640.97 596.54 6.38 o 6 -4 4 255.53 243.09 5.53 o 6 -4 5 0.15 -1.34 5.86 < 6 -2 -7 469.94 462.96 9.56 o 6 -2 -6 20.34 20.25 4.69 o 6 -2 -5 396.65 392.11 6.04 o 6 -2 -4 1267.82 1223.71 8.92 o 6 -2 -3 33.99 37.33 2.85 o 6 -2 -2 2662.49 2771.85 9.51 o 6 -2 -1 913.98 930.78 6.73 o 6 -2 0 947.43 1003.50 6.06 o 6 -2 1 1101.12 1103.17 8.08 o 6 -2 2 113.96 106.50 3.85 o 6 -2 3 2023.35 2134.71 11.14 o 6 -2 4 5.92 7.36 4.18 < 6 -2 5 248.84 252.80 6.37 o 6 -2 6 168.03 143.87 15.07 o 6 0 -7 0.89 1.84 6.03 < 6 0 -6 917.14 950.25 10.41 o 6 0 -5 256.05 257.52 7.37 o 6 0 -4 3.35 4.35 2.51 < 6 0 -3 2223.54 2284.03 9.82 o 6 0 -2 827.37 840.35 7.40 o 6 0 -1 2920.53 3112.70 11.40 o 6 0 0 1089.57 1064.03 5.39 o 6 0 1 451.94 450.25 4.86 o 6 0 2 2597.76 2778.72 14.40 o 6 0 3 161.01 163.29 5.36 o 6 0 4 1773.61 1942.87 11.46 o 6 0 5 82.37 91.91 6.70 o 6 0 6 75.42 68.98 9.04 o 6 2 -7 155.36 159.26 7.03 o 6 2 -6 26.96 25.94 5.02 o 6 2 -5 119.76 113.19 4.52 o 6 2 -4 404.60 431.08 6.87 o 6 2 -3 151.57 163.30 6.03 o 6 2 -1 413.88 426.25 4.36 o 6 2 0 482.97 520.68 5.03 o 6 2 1 520.01 564.47 5.54 o 6 2 2 57.51 56.75 4.35 o 6 2 3 2090.14 2262.32 10.47 o 6 2 4 2.33 -1.67 4.52 < 6 2 5 281.68 296.40 7.54 o 6 4 -7 265.65 290.19 8.04 o 6 4 -6 0.71 3.85 4.18 < 6 4 -5 88.56 88.23 4.19 o 6 4 -4 214.02 226.49 4.19 o 6 4 -3 280.64 258.58 4.52 o 6 4 -2 863.03 863.23 7.06 o 6 4 -1 31.50 34.32 4.18 o 6 4 0 5.28 3.18 4.52 < 6 4 1 9.42 8.87 3.18 < 6 4 2 171.99 178.71 4.52 o 6 4 3 588.92 595.40 7.21 o 6 4 4 270.65 280.14 7.37 o 6 4 5 10.35 7.20 5.86 < 6 6 -7 0.75 1.17 8.37 < 6 6 -6 635.90 674.01 10.57 o 6 6 -5 224.99 231.84 6.03 o 6 6 -4 2.32 1.00 3.51 < 6 6 -3 1261.79 1274.79 9.42 o 6 6 -2 189.24 200.51 4.86 o 6 6 -1 1377.41 1386.47 6.90 o 6 6 0 236.65 250.98 5.19 o 6 6 1 140.77 144.19 4.19 o 6 6 2 914.02 885.48 9.24 o 6 6 3 9.27 13.06 3.85 o 6 6 4 609.60 607.84 8.56 o 6 6 5 3.96 3.18 5.02 < 6 8 -6 4.04 6.69 8.87 < 6 8 -5 216.25 214.75 9.88 o 6 8 -4 817.99 818.05 8.56 o 6 8 -3 25.18 23.60 4.35 o 6 8 -2 1158.02 1177.12 8.58 o 6 8 -1 272.40 277.64 5.70 o 6 8 0 841.40 833.50 6.38 o 6 8 1 755.03 724.04 7.39 o 6 8 2 212.31 216.59 5.36 o 6 8 3 1066.53 1044.58 9.92 o 6 8 4 26.18 25.44 4.85 o 6 10 -5 21.33 17.07 9.54 < 6 10 -4 18.16 11.38 10.38 < 6 10 -3 663.99 677.43 11.08 o 6 10 -2 5.57 8.87 6.03 < 6 10 -1 201.69 209.37 6.20 o 6 10 0 225.21 219.78 9.21 o 6 10 1 440.93 468.27 7.88 o 6 10 2 461.36 453.05 6.20 o 6 10 3 5.71 5.02 4.35 < 6 12 -3 104.16 109.84 12.89 o 6 12 -2 25.33 17.41 10.71 < 6 12 -1 24.82 31.13 8.70 o 6 12 0 25.07 23.77 8.20 < 6 12 1 11.25 13.56 8.54 < 7 -11 -4 0.66 0.50 6.03 < 7 -11 -3 154.27 177.85 7.20 o 7 -11 -2 207.90 213.07 7.20 o 7 -11 -1 2.69 5.19 5.36 < 7 -11 0 356.54 371.41 9.05 o 7 -11 1 26.05 24.27 4.69 o 7 -11 2 206.35 200.84 7.87 o 7 -9 -5 50.26 36.16 7.70 o 7 -9 -4 4.58 3.68 5.52 < 7 -9 -3 97.39 97.11 5.86 o 7 -9 -2 44.37 50.05 4.35 o 7 -9 -1 200.74 220.93 5.53 o 7 -9 0 191.54 192.78 7.20 o 7 -9 1 41.41 39.67 4.69 o 7 -9 2 0.05 -0.33 4.69 < 7 -9 3 1.14 2.01 4.85 < 7 -7 -6 322.49 284.72 8.04 o 7 -7 -5 1.15 3.68 5.52 < 7 -7 -4 348.05 336.54 6.70 o 7 -7 -3 209.32 210.56 4.19 o 7 -7 -2 316.69 315.06 4.86 o 7 -7 -1 885.48 935.81 6.55 o 7 -7 0 74.27 76.51 3.85 o 7 -7 1 620.67 628.18 7.21 o 7 -7 2 350.03 359.67 7.54 o 7 -7 3 68.10 71.48 5.86 o 7 -7 4 58.98 51.90 6.36 o 7 -5 -7 303.66 286.88 8.55 o 7 -5 -6 10.75 10.21 5.19 < 7 -5 -5 532.04 549.45 8.55 o 7 -5 -4 44.00 49.38 3.85 o 7 -5 -3 872.01 852.85 7.56 o 7 -5 -2 1011.20 1019.22 7.56 o 7 -5 -1 88.26 94.77 3.18 o 7 -5 0 2119.74 2194.59 9.46 o 7 -5 1 211.65 218.77 4.86 o 7 -5 2 592.05 577.96 7.89 o 7 -5 3 640.84 590.46 9.40 o 7 -5 4 145.10 138.49 7.87 o 7 -3 -7 65.94 59.26 8.87 o 7 -3 -6 294.22 323.73 7.71 o 7 -3 -5 10.18 15.40 4.18 o 7 -3 -4 742.34 765.56 7.55 o 7 -3 -3 2.26 6.86 3.01 < 7 -3 -2 104.60 122.07 4.35 o 7 -3 -1 2228.03 2444.01 16.24 o 7 -3 0 79.73 88.40 3.85 o 7 -3 1 1046.36 1026.96 7.57 o 7 -3 2 260.24 237.24 4.69 o 7 -3 3 232.27 211.75 5.70 o 7 -3 4 739.90 667.91 8.73 o 7 -3 5 66.23 64.79 6.36 o 7 -1 -7 22.79 34.15 7.70 o 7 -1 -6 260.31 227.85 7.87 o 7 -1 -5 189.04 207.02 6.03 o 7 -1 -4 151.93 159.94 5.19 o 7 -1 -3 40.68 59.26 4.85 o 7 -1 -2 2.59 16.07 3.01 o 7 -1 -1 224.33 245.63 5.70 o 7 -1 0 1204.12 1270.88 12.12 o 7 -1 1 25.34 26.45 3.85 o 7 -1 2 1.59 2.34 3.18 < 7 -1 3 111.59 116.04 5.36 o 7 -1 4 31.77 34.31 4.52 o 7 -1 5 311.40 323.76 8.21 o 7 1 -7 281.89 272.45 8.21 o 7 1 -6 1.97 4.85 5.69 < 7 1 -5 856.21 837.71 10.08 o 7 1 -4 4.64 12.22 4.18 < 7 1 -3 656.41 602.81 8.90 o 7 1 -2 409.30 449.08 6.37 o 7 1 -1 5.24 15.23 2.68 o 7 1 0 2054.79 1957.50 12.17 o 7 1 1 13.64 17.74 3.35 o 7 1 2 77.72 80.03 3.68 o 7 1 3 162.15 176.18 5.19 o 7 1 4 19.94 19.25 5.02 o 7 1 5 224.92 231.34 8.21 o 7 3 -7 16.76 17.07 6.53 < 7 3 -6 529.66 534.18 8.39 o 7 3 -5 82.32 96.60 4.52 o 7 3 -4 1450.83 1375.14 10.27 o 7 3 -3 76.93 69.98 3.85 o 7 3 -2 282.53 275.67 6.70 o 7 3 -1 2935.78 2842.75 15.95 o 7 3 0 258.65 262.90 5.36 o 7 3 1 1402.88 1459.04 10.94 o 7 3 2 284.47 313.84 6.20 o 7 3 3 295.75 315.86 9.22 o 7 3 4 718.36 748.25 10.91 o 7 3 5 64.26 70.31 10.38 o 7 5 -7 185.99 178.55 9.38 o 7 5 -6 13.60 10.88 6.36 < 7 5 -5 463.07 419.02 9.89 o 7 5 -4 8.89 6.03 4.02 < 7 5 -3 641.11 622.76 7.38 o 7 5 -2 584.18 558.06 7.05 o 7 5 -1 21.65 20.09 2.85 o 7 5 0 2016.11 1994.60 9.45 o 7 5 1 164.24 163.63 4.35 o 7 5 2 509.67 507.48 7.38 o 7 5 3 513.13 502.78 11.24 o 7 5 4 217.07 241.05 10.39 o 7 7 -6 72.01 52.57 10.04 o 7 7 -5 160.83 172.83 7.54 o 7 7 -4 76.23 76.84 6.19 o 7 7 -3 0.42 0.17 4.85 < 7 7 -2 20.25 19.25 3.85 o 7 7 -1 373.21 364.07 5.70 o 7 7 0 260.39 261.37 4.19 o 7 7 1 320.86 312.54 5.19 o 7 7 2 175.82 168.99 6.53 o 7 7 3 84.45 95.10 5.69 o 7 7 4 60.58 59.26 5.69 o 7 9 -5 9.02 15.57 12.55 < 7 9 -4 342.08 344.57 13.07 o 7 9 -3 4.71 6.86 5.36 < 7 9 -2 6.81 6.03 9.04 < 7 9 -1 600.26 641.87 10.07 o 7 9 0 5.81 6.19 6.19 < 7 9 1 171.71 192.94 6.70 o 7 9 2 1.74 2.68 4.18 < 7 9 3 13.73 12.89 4.69 < 7 11 -3 365.97 391.04 15.09 o 7 11 -2 409.22 418.93 11.90 o 7 11 -1 20.51 21.26 7.87 < 7 11 0 562.98 611.26 13.42 o 7 11 1 81.62 60.61 9.21 o 8 -12 -1 67.56 62.78 7.87 o 8 -10 -4 313.57 286.06 9.72 o 8 -10 -3 9.73 9.87 5.36 < 8 -10 -2 420.41 443.43 7.38 o 8 -10 -1 258.95 265.38 6.53 o 8 -10 0 200.55 188.10 6.87 o 8 -10 1 236.50 233.03 7.54 o 8 -10 2 9.97 6.36 7.20 < 8 -8 -5 293.79 276.31 9.05 o 8 -8 -4 5.84 4.02 5.52 < 8 -8 -3 382.43 379.66 9.05 o 8 -8 -2 84.43 91.75 5.69 o 8 -8 -1 525.50 533.50 8.55 o 8 -8 0 291.74 287.20 6.70 o 8 -8 1 61.94 65.46 5.02 o 8 -8 2 715.42 725.09 10.07 o 8 -8 3 40.10 46.03 7.20 o 8 -6 -6 6.42 1.67 7.53 < 8 -6 -5 62.03 51.06 6.53 o 8 -6 -4 396.98 425.44 7.21 o 8 -6 -3 39.30 32.64 4.18 o 8 -6 -2 106.03 101.63 4.52 o 8 -6 -1 2.84 5.69 3.51 < 8 -6 0 134.13 137.65 4.69 o 8 -6 1 420.82 410.23 8.72 o 8 -6 2 28.51 32.97 5.02 o 8 -6 3 321.73 315.39 6.20 o 8 -6 4 30.30 16.40 13.06 < 8 -4 -6 88.41 87.90 8.87 o 8 -4 -5 0.48 9.71 4.85 < 8 -4 -4 511.15 474.78 7.21 o 8 -4 -3 99.13 110.84 4.19 o 8 -4 -2 492.99 520.24 6.37 o 8 -4 -1 63.82 60.94 3.01 o 8 -4 0 94.41 97.44 4.19 o 8 -4 1 79.73 87.23 4.02 o 8 -4 2 159.39 145.20 6.20 o 8 -4 3 399.56 409.36 9.22 o 8 -4 4 0.73 0.67 4.85 < 8 -2 -7 1.18 -2.51 8.70 < 8 -2 -6 104.38 109.84 7.53 o 8 -2 -5 716.57 683.96 14.27 o 8 -2 -4 2.03 7.20 4.02 < 8 -2 -3 1358.22 1381.06 10.94 o 8 -2 -2 72.99 78.35 4.52 o 8 -2 -1 1019.32 1075.03 6.72 o 8 -2 0 448.23 459.96 4.70 o 8 -2 1 178.97 169.67 3.85 o 8 -2 2 1218.09 1146.32 10.60 o 8 -2 3 3.47 1.17 4.02 < 8 -2 4 262.35 251.15 7.54 o 8 0 -7 201.10 196.48 8.04 o 8 0 -6 37.34 29.80 5.86 o 8 0 -5 7.73 8.37 6.19 < 8 0 -4 1642.47 1712.66 15.50 o 8 0 -3 44.94 46.70 5.36 o 8 0 -2 1045.95 1071.81 9.42 o 8 0 -1 67.76 73.83 3.68 o 8 0 0 917.76 913.55 6.38 o 8 0 1 1649.40 1542.19 9.94 o 8 0 2 44.83 39.51 4.52 o 8 0 3 858.33 856.97 8.73 o 8 0 4 147.88 149.04 6.87 o 8 2 -7 16.20 22.26 6.19 o 8 2 -6 0.32 4.52 5.52 < 8 2 -5 202.76 234.16 7.04 o 8 2 -4 148.02 134.98 7.20 o 8 2 -3 817.14 840.19 11.59 o 8 2 -2 9.39 17.41 5.19 o 8 2 -1 349.70 369.93 7.88 o 8 2 0 127.26 139.49 4.69 o 8 2 1 70.49 74.33 5.19 o 8 2 2 1042.45 1095.93 9.08 o 8 2 3 5.77 7.70 5.86 < 8 2 4 225.67 227.82 7.54 o 8 4 -6 4.75 7.70 5.52 < 8 4 -5 254.77 259.68 6.53 o 8 4 -4 54.30 48.55 4.52 o 8 4 -3 629.51 635.10 8.73 o 8 4 -2 55.75 52.56 5.86 o 8 4 -1 80.76 75.17 5.86 o 8 4 0 8.66 7.03 3.85 < 8 4 1 4.05 3.51 4.02 < 8 4 2 342.03 354.96 8.04 o 8 4 3 255.21 260.69 8.04 o 8 4 4 0.04 0.00 7.20 < 8 6 -6 45.54 45.70 8.04 o 8 6 -5 1.21 1.17 6.19 < 8 6 -4 957.76 950.21 11.76 o 8 6 -3 50.06 51.73 5.19 o 8 6 -2 571.55 556.09 8.89 o 8 6 -1 36.78 34.31 4.35 o 8 6 0 365.75 372.10 5.70 o 8 6 1 845.73 877.92 9.74 o 8 6 2 1.49 2.01 4.69 < 8 6 3 372.98 382.00 9.22 o 8 8 -5 306.61 307.16 11.40 o 8 8 -4 1.34 -0.50 6.19 < 8 8 -3 590.92 590.01 9.39 o 8 8 -2 108.99 116.54 6.86 o 8 8 -1 606.46 595.58 10.57 o 8 8 0 335.36 339.37 8.71 o 8 8 1 107.75 102.47 4.86 o 8 8 2 823.13 834.23 9.91 o 8 10 -3 12.96 12.89 7.20 < 8 10 -2 254.10 243.60 10.39 o 8 10 -1 99.72 95.27 6.70 o 8 10 0 124.38 121.23 8.37 o 8 10 1 171.05 167.31 10.38 o 9 -9 -4 51.83 60.93 7.70 o 9 -9 -3 14.51 4.52 5.86 < 9 -9 -2 65.93 69.14 7.03 o 9 -9 -1 232.15 224.31 8.71 o 9 -9 0 14.82 13.89 5.86 < 9 -9 1 0.25 0.17 5.36 < 9 -7 -5 300.09 310.67 7.71 o 9 -7 -4 79.47 67.80 6.19 o 9 -7 -3 40.97 50.22 8.03 o 9 -7 -2 444.83 450.00 9.05 o 9 -7 -1 2.19 2.01 5.69 < 9 -7 0 631.88 631.38 10.23 o 9 -7 1 101.26 100.63 7.37 o 9 -7 2 42.91 43.02 6.70 o 9 -5 -6 155.68 172.16 9.55 o 9 -5 -5 13.17 12.39 5.69 < 9 -5 -4 372.76 363.55 6.87 o 9 -5 -3 435.85 447.30 7.71 o 9 -5 -2 2.25 2.34 3.85 < 9 -5 -1 1207.30 1231.51 12.28 o 9 -5 0 93.90 91.42 4.35 o 9 -5 1 534.53 526.47 7.38 o 9 -5 2 256.93 256.00 8.88 o 9 -5 3 150.60 150.89 5.69 o 9 -3 -6 0.64 3.68 7.36 < 9 -3 -5 109.92 114.86 7.70 o 9 -3 -4 1.68 6.19 4.85 < 9 -3 -3 47.59 67.29 5.19 o 9 -3 -2 1190.79 1338.79 9.08 o 9 -3 -1 57.61 60.60 3.68 o 9 -3 0 519.84 501.46 5.37 o 9 -3 1 117.43 119.22 6.53 o 9 -3 2 400.32 401.64 9.56 o 9 -3 3 299.54 290.56 7.71 o 9 -1 -6 30.76 31.13 7.53 o 9 -1 -5 135.18 141.33 8.71 o 9 -1 -4 1.75 9.37 6.69 < 9 -1 -3 45.15 70.31 5.69 o 9 -1 -2 257.59 268.07 5.36 o 9 -1 -1 496.26 513.68 5.87 o 9 -1 0 243.56 239.90 5.03 o 9 -1 1 45.94 50.55 4.85 o 9 -1 2 29.94 30.80 5.69 o 9 -1 3 18.81 17.07 4.85 o 9 1 -6 203.39 200.84 7.87 o 9 1 -5 1.11 6.19 6.03 < 9 1 -4 221.09 230.16 7.04 o 9 1 -3 508.92 508.83 9.56 o 9 1 -2 15.09 23.60 5.36 o 9 1 -1 1163.88 1158.94 15.64 o 9 1 0 6.71 14.73 5.19 < 9 1 1 282.73 273.78 6.53 o 9 1 2 111.06 117.71 8.87 o 9 1 3 47.24 45.53 7.37 o 9 3 -6 26.05 21.26 5.86 o 9 3 -5 273.24 252.49 7.20 o 9 3 -4 47.07 52.23 5.36 o 9 3 -3 157.46 177.85 6.87 o 9 3 -2 1765.17 1767.09 18.88 o 9 3 -1 2.71 -1.17 5.19 < 9 3 0 726.91 707.33 12.76 o 9 3 1 200.67 206.69 6.03 o 9 3 2 546.54 544.28 9.90 o 9 3 3 401.83 395.12 11.90 o 9 5 -6 150.96 129.62 7.87 o 9 5 -5 0.38 -2.51 6.36 < 9 5 -4 161.29 159.77 6.70 o 9 5 -3 277.56 261.21 7.20 o 9 5 -2 2.28 2.68 4.69 < 9 5 -1 1017.97 963.22 9.24 o 9 5 0 31.19 29.79 4.35 o 9 5 1 397.51 382.87 9.22 o 9 5 2 239.60 229.68 7.20 o 9 5 3 158.36 150.89 9.71 o 9 7 -5 77.68 81.70 10.55 o 9 7 -4 2.65 2.85 6.69 < 9 7 -3 23.05 26.28 6.70 o 9 7 -2 122.40 112.86 6.53 o 9 7 -1 95.73 86.90 7.53 o 9 7 0 260.82 249.63 5.86 o 9 7 1 10.97 8.87 4.52 < 9 7 2 12.54 9.21 5.36 < 9 9 -4 1.99 0.50 8.87 < 9 9 -3 30.33 44.52 8.03 o 9 9 -2 408.94 418.43 11.06 o 9 9 -1 12.80 15.90 6.53 < 9 9 0 114.47 114.20 10.55 o 10 -8 -3 42.55 38.84 7.53 o 10 -8 -2 207.73 217.59 10.39 o 10 -8 -1 70.14 72.99 8.87 o 10 -8 0 23.44 16.74 10.04 < 10 -6 -5 82.47 92.08 7.20 o 10 -6 -4 55.68 51.06 7.53 o 10 -6 -3 27.64 36.82 7.03 o 10 -6 -2 0.33 -0.84 5.69 < 10 -6 -1 47.81 56.58 6.03 o 10 -6 0 131.88 122.41 5.69 o 10 -6 1 91.07 88.07 6.86 o 10 -4 -5 149.81 154.74 10.05 o 10 -4 -4 0.83 -3.01 7.70 < 10 -4 -3 259.12 243.26 9.21 o 10 -4 -2 11.13 3.68 5.19 < 10 -4 -1 10.82 8.87 6.36 < 10 -4 0 198.48 206.19 8.37 o 10 -4 1 40.57 40.68 7.53 o 10 -4 2 333.11 321.94 8.71 o 10 -2 -5 1.75 1.51 7.53 < 10 -2 -4 332.22 331.82 8.88 o 10 -2 -3 76.80 72.32 6.03 o 10 -2 -2 422.52 442.42 6.54 o 10 -2 -1 291.60 291.55 6.37 o 10 -2 0 24.80 22.09 6.19 o 10 -2 1 940.30 878.77 11.76 o 10 -2 2 2.62 5.19 7.70 < 10 0 -6 16.36 23.93 7.87 o 10 0 -5 364.46 374.44 8.88 o 10 0 -4 3.08 -1.84 6.53 < 10 0 -3 213.75 217.93 9.05 o 10 0 -2 136.27 154.06 7.20 o 10 0 -1 381.55 421.56 7.88 o 10 0 0 780.17 799.29 11.75 o 10 0 1 15.51 19.58 5.69 o 10 0 2 751.25 758.11 14.27 o 10 2 -5 16.36 19.92 5.86 o 10 2 -4 109.94 110.68 7.70 o 10 2 -3 8.92 9.87 6.36 < 10 2 -2 102.19 128.09 8.04 o 10 2 -1 101.57 104.14 7.53 o 10 2 0 0.78 -1.00 7.03 < 10 2 1 544.93 553.67 9.06 o 10 2 2 17.21 15.06 6.86 < 10 4 -5 2.74 9.04 6.36 < 10 4 -4 116.86 101.14 7.03 o 10 4 -3 7.36 4.02 5.86 < 10 4 -2 117.92 116.54 8.04 o 10 4 -1 53.48 55.07 5.69 o 10 4 0 19.20 27.62 5.52 o 10 4 1 214.09 202.69 6.53 o 10 4 2 111.93 104.32 6.87 o 10 6 -4 6.40 4.85 7.53 < 10 6 -3 207.21 214.91 9.72 o 10 6 -2 60.10 63.28 5.86 o 10 6 -1 281.74 261.72 8.04 o 10 6 0 421.20 378.72 8.05 o 10 6 1 10.43 6.69 6.03 < 10 8 -3 33.05 20.42 14.40 < 10 8 -2 273.68 274.62 11.90 o 10 8 -1 134.62 114.88 9.04 o 11 -5 -4 81.69 93.92 8.37 o 11 -5 -3 2.30 4.18 6.36 < 11 -5 -2 489.21 476.76 10.06 o 11 -5 -1 71.60 64.45 6.53 o 11 -5 0 207.56 202.52 8.71 o 11 -3 -4 39.11 44.02 6.70 o 11 -3 -3 189.52 194.79 7.37 o 11 -3 -2 23.96 24.44 5.52 o 11 -3 -1 212.86 238.53 7.20 o 11 -3 0 112.12 106.49 9.38 o 11 -3 1 123.87 128.10 10.05 o 11 -1 -5 24.92 38.67 9.37 o 11 -1 -4 0.21 7.20 11.55 < 11 -1 -3 95.58 109.67 9.21 o 11 -1 -2 38.28 55.41 7.53 o 11 -1 -1 53.19 43.19 6.36 o 11 -1 0 17.63 28.29 10.54 < 11 -1 1 6.04 3.85 12.05 < 11 1 -4 88.70 91.41 8.71 o 11 1 -3 0.72 2.68 7.20 < 11 1 -2 342.63 340.05 12.90 o 11 1 -1 21.67 23.10 7.70 o 11 1 0 172.83 162.79 10.05 o 11 1 1 73.05 61.94 7.70 o 11 3 -4 144.58 132.13 10.38 o 11 3 -3 377.35 355.52 8.88 o 11 3 -2 1.39 4.18 6.69 < 11 3 -1 364.55 378.97 10.73 o 11 3 0 203.89 189.28 8.38 o 11 3 1 266.10 218.48 12.06 o 11 5 -3 0.47 -1.84 7.70 < 11 5 -2 309.62 292.08 10.05 o 11 5 -1 14.06 14.06 6.70 < 11 5 0 197.24 176.38 6.70 o 12 -2 -3 293.12 276.32 17.59 o 12 -2 -2 31.68 27.12 14.90 < 12 0 -3 6.59 8.54 9.54 < 12 0 -2 196.30 194.97 11.56 o 12 0 -1 143.59 138.49 10.89 o 12 2 -2 0.38 3.01 14.56 < #======================================================================= data_alpha3_split #======================================================================= # 5. CHEMICAL DATA _chemical_name_systematic ? _chemical_name_common ? _chemical_formula_moiety ? _chemical_formula_structural ? _chemical_formula_analytical ? _chemical_formula_iupac ? _chemical_formula_sum 'Fe2 O7 P2' _chemical_formula_weight 285.6 _chemical_melting_point ? _chemical_compound_source ? _chemical_absolute_configuration . #======================================================================= # 6. CRYSTAL DATA _space_group_crystal_system triclinic _space_group_name_H-M_alt 'C-1' _space_group_name_Hall '-C 1' _space_group_IT_number 2 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,-y,-z 3 x+1/2,y+1/2,z 4 -x+1/2,-y+1/2,-z _cell_length_a 6.6161(5) _cell_length_b 8.4673(4) _cell_length_c 4.4825(3) _cell_angle_alpha 90.135(5) _cell_angle_beta 103.645(7) _cell_angle_gamma 91.616(7) _cell_volume 243.92(3) _cell_formula_units_Z 2 _cell_measurement_reflns_used 11950 _cell_measurement_theta_min 3.92 _cell_measurement_theta_max 41.04 _cell_measurement_temperature 400 _cell_special_details ? _exptl_crystal_density_diffrn 3.8891 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_F_000 276 _exptl_crystal_type_of_structure cryst _exptl_absorpt_coefficient_mu 6.582 _exptl_crystal_description 'plate' _exptl_crystal_colour 'light brown' _exptl_crystal_size_max 0.060 _exptl_crystal_size_mid 0.037 _exptl_crystal_size_min 0.010 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; STOE LANA, absorption correction by scaling of reflection intensities. J. Koziskova, F. Hahn, J. Richter, J. Kozisek, "Comparison of different absorption corrections on the model structure of tetrakis(\m~2~-acetato)- diaqua-di-copper(II)", Acta Chimica Slovaca, vol. 9, no. 2, 2016, pp. 136 - 140. Afterwards a spherical absorption correction was performed within STOE LANA. ; _exptl_absorpt_correction_T_min 0.5683 _exptl_absorpt_correction_T_max 0.6892 #======================================================================= # 7. EXPERIMENTAL DATA _diffrn_measurement_device 'Eulerian 4-circle diffractometer' _diffrn_measurement_device_type 'STOE STADIVARI' _diffrn_detector 'EIGER2 1M CDTE' _diffrn_detector_type ? _diffrn_detector_area_resol_mean 13.33 _diffrn_source 'X-ray tube. Axo_Mo' _diffrn_source_type ? _diffrn_radiation_probe x-ray _diffrn_source_target ? _diffrn_source_voltage 60 _diffrn_source_current 0.830 _diffrn_source_power 0.050 _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_monochromator 'Graded multilayer mirror' _diffrn_radiation_polarisn_norm -90 _diffrn_radiation_collimation '1.2 0.6 mm diameter' _diffrn_ambient_temperature 400 _diffrn_measurement_method 'rotation method, \w scans' _diffrn_measurement_details ; 1960 frames, detector distance = 45 mm ; _diffrn_reflns_number 7257 _diffrn_reflns_theta_min 3.92 _diffrn_reflns_theta_max 41.04 _diffrn_reflns_theta_full 40.95 _diffrn_measured_fraction_theta_max 0.97 _diffrn_measured_fraction_theta_full 0.98 _diffrn_reflns_av_R_equivalents 0.0158 _diffrn_reflns_av_unetI/netI 0.0111 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_k_min -9 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_l_min -8 _diffrn_reflns_limit_l_max 8 _diffrn_reflns_reduction_process ? _diffrn_standards_number ? _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% ? loop_ _diffrn_standard_refln_index_h _diffrn_standard_refln_index_k _diffrn_standard_refln_index_l ? ? ? #_diffrn_radiation_source 'X-ray tube' #_diffrn_reflns_av_sigmaI/netI 0.0111 _reflns_number_total 1563 _reflns_number_gt 1341 _reflns_threshold_expression 'I>3\s(I)' _refine_ls_R_factor_gt 0.0218 _refine_ls_wR_factor_gt 0.0615 _refine_ls_R_factor_all 0.0258 _refine_ls_wR_factor_ref 0.0627 _refine_ls_goodness_of_fit_ref 1.1684 _refine_ls_goodness_of_fit_gt 1.2421 _refine_ls_number_reflns 1563 _refine_ls_number_parameters 56 _refine_ls_weighting_scheme sigma _refine_ls_weighting_details 'w=1/(\s^2^(I)+0.0016I^2^)' _refine_ls_shift/su_max 0.0144 _refine_ls_shift/su_mean 0.0034 _refine_diff_density_max 0.37 _refine_diff_density_min -0.15 _refine_ls_extinction_method 'B-C type 1 Gaussian isotropic (Becker & Coppens, 1974)' _refine_ls_number_constraints 0 _refine_ls_number_restraints 0 _refine_ls_structure_factor_coef Fsqd _refine_ls_extinction_coef 540(60) loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Fe 0.3463 0.8444 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' O 0.0106 0.0060 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' P 0.1023 0.0942 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_adp_type _atom_site_U_iso_or_equiv _atom_site_site_symmetry_multiplicity _atom_site_occupancy _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_disorder_assembly _atom_site_disorder_group Fe1 Fe 0.49492(3) 0.190858(17) 0.50928(4) Uani 0.01288(5) 4 1 d . . . P1 P 0.21344(4) 0.00054(3) -0.09088(6) Uani 0.00888(6) 4 1 d . . . O1 O 0.37352(13) 0.00272(10) 0.21365(18) Uani 0.01151(18) 4 1 d . . . O2 O 0.22526(16) 0.14812(10) -0.2778(2) Uani 0.0150(2) 4 1 d . . . O3 O 0.21854(18) -0.14926(10) -0.2769(2) Uani 0.0193(2) 4 1 d . . . O4 O -0.0016(10) -0.0263(5) -0.0139(18) Uani 0.0287(12) 4 0.5 d . . . loop_ _atom_site_aniso_label _atom_site_aniso_type_symbol _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Fe1 Fe 0.01280(8) 0.00943(8) 0.01399(8) -0.00045(5) -0.00156(5) -0.00023(5) P1 P 0.00697(10) 0.01234(11) 0.00712(10) -0.00035(8) 0.00128(8) 0.00087(8) O1 O 0.0115(3) 0.0135(3) 0.0082(3) 0.0010(2) -0.0004(2) -0.0004(2) O2 O 0.0195(4) 0.0124(3) 0.0131(3) 0.0039(3) 0.0034(3) 0.0035(2) O3 O 0.0275(5) 0.0125(3) 0.0144(4) -0.0052(3) -0.0012(3) -0.0027(3) O4 O 0.0090(6) 0.050(3) 0.0317(16) 0.002(2) 0.0127(9) 0.001(2) #======================================================================= # 10. MOLECULAR GEOMETRY loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_1 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Fe1 O1 . . 2.0868(8) ? Fe1 O1 . 2_656 2.1370(8) ? Fe1 O2 . 1_556 2.2347(11) ? Fe1 O2 . 4_555 2.1127(9) ? Fe1 O3 . 3_556 2.0376(10) ? Fe1 O3 . 2_655 2.4022(13) ? P1 O1 . . 1.5173(8) ? P1 O2 . . 1.5164(9) ? P1 O3 . . 1.5219(10) ? P1 O4 . . 1.552(8) ? P1 O4 . 2_555 1.600(8) ? O4 O4 . 2_555 0.461(7) ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_2 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag O1 Fe1 O1 . . 2_656 79.99(3) ? O1 Fe1 O2 . . 1_556 86.54(3) ? O1 Fe1 O2 . . 4_555 94.07(3) ? O1 Fe1 O3 . . 3_556 155.39(4) ? O1 Fe1 O3 . . 2_655 79.82(3) ? O1 Fe1 O2 2_656 . 1_556 84.19(3) ? O1 Fe1 O2 2_656 . 4_555 160.68(4) ? O1 Fe1 O3 2_656 . 3_556 94.43(3) ? O1 Fe1 O3 2_656 . 2_655 82.33(3) ? O2 Fe1 O2 1_556 . 4_555 77.08(4) ? O2 Fe1 O3 1_556 . 3_556 116.95(4) ? O2 Fe1 O3 1_556 . 2_655 162.26(3) ? O2 Fe1 O3 4_555 . 3_556 98.19(4) ? O2 Fe1 O3 4_555 . 2_655 114.93(4) ? O3 Fe1 O3 3_556 . 2_655 75.68(4) ? O1 P1 O2 . . . 112.89(5) ? O1 P1 O3 . . . 112.58(5) ? O1 P1 O4 . . . 106.3(3) ? O1 P1 O4 . . 2_555 102.2(3) ? O2 P1 O3 . . . 111.89(5) ? O2 P1 O4 . . . 113.1(2) ? O2 P1 O4 . . 2_555 101.1(2) ? O3 P1 O4 . . . 99.3(2) ? O3 P1 O4 . . 2_555 115.38(19) ? O4 P1 O4 . . 2_555 16.7(2) ? Fe1 O1 Fe1 . . 2_656 100.01(3) ? Fe1 O1 P1 . . . 130.26(5) ? Fe1 O1 P1 2_656 . . 129.22(5) ? Fe1 O2 Fe1 1_554 . 4_555 102.92(4) ? Fe1 O2 P1 1_554 . . 120.14(6) ? Fe1 O2 P1 4_555 . . 134.47(6) ? Fe1 O3 Fe1 3_444 . 2_655 104.32(4) ? Fe1 O3 P1 3_444 . . 133.28(7) ? Fe1 O3 P1 2_655 . . 119.94(6) ? P1 O4 P1 . . 2_555 163.3(3) ? P1 O4 O4 . . 2_555 87.6(13) ? P1 O4 O4 2_555 . 2_555 75.7(13) ? #------------------------------------------------------------------------------- # STOE DATA #------------------------------------------------------------------------------- #_STOE_detector_size_x '8.0 cm' #_STOE_detector_size_y '7.7 cm' #_STOE_detector_pixelsize_x '0.075 mm' #_STOE_detector_pixelsize_y '0.075 mm' #_STOE_detector_distance '45.0 mm' #_STOE_measurement_tube_power '49.8 W' #_STOE_measurement_total_run_number 29 #_STOE_measurement_total_frame_number 1960 #_STOE_measurement_min_exposure_per_frame '30.0 s' #_STOE_measurement_max_exposure_per_frame '30.0 s' #_STOE_measurement_mean_exposure_per_frame '30.0 s' #_STOE_measurement_total_exposure_time '16.3 h' #_STOE_evaluation_integration_A 15.1 #_STOE_evaluation_integration_B -1.0 #_STOE_evaluation_integration_EMS 0.037 #_STOE_evaluation_LANA_point_group '-1' #_STOE_evaluation_LANA_FS_max_order 3 #_STOE_evaluation_LANA_DXS_max_order - #_STOE_evaluation_LANA_DYS_max_order - #_STOE_evaluation_LANA_BIS_l_even_max 4 #_STOE_evaluation_LANA_BIS_l_odd_max 1 #_STOE_evaluation_LANA_BOS_l_even_max 4 #_STOE_evaluation_LANA_BOS_l_odd_max 1 #_STOE_evaluation_LANA_OR_c1 0.035 #_STOE_evaluation_LANA_OR_c2 0 #_STOE_evaluation_LANA_OR_c3 0 #_STOE_evaluation_LANA_OR_c4 0.7 #_STOE_evaluation_LANA_max_2theta_available 82.1 #_STOE_evaluation_LANA_max_2theta_desired 82.1 #_STOE_evaluation_LANA_number_refls_total 8369 #_STOE_evaluation_LANA_number_refls_outliers 1112 #_STOE_evaluation_LANA_number_refls_after_OR 7257 #_STOE_evaluation_LANA_number_refls_unique 1567 #_STOE_evaluation_LANA_number_refls_written 7257 #_STOE_evaluation_LANA_completeness 97.5 #_STOE_evaluation_LANA_mean_redundancy 4.6 #_STOE_evaluation_LANA_table #; #---------------------------------------------------------------------------- #2Theta 11.4 19.8 28.2 36.6 45.0 53.4 61.8 70.2 78.6 #---------------------------------------------------------------------------- #<Resolution> 3.53 2.03 1.42 1.13 0.91 0.79 0.69 0.62 0.57 #N(total) 108 353 490 792 907 1403 1571 1547 1198 #<Redundancy> 7.3 7.2 5.3 5.8 4.5 5.3 4.9 4.1 3.5 #Complet. [%%] 100.0 100.0 100.0 99.2 98.8 100.0 100.0 100.0 89.5 #<I/sigma> 265.9 169.9 149.1 76.8 43.7 33.2 19.3 13.4 6.8 #R(int) 0.010 0.013 0.014 0.014 0.015 0.016 0.021 0.026 0.039 #---------------------------------------------------------------------------- #; #======================================================================= # 11. STRUCTURE-FACTOR LIST loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_include_status 0 0 1 1550.97 1568.02 2.96 o 0 0 2 1852.93 1619.77 3.94 o 0 0 3 2473.16 2552.74 6.15 o 0 0 4 1918.84 1929.94 8.13 o 0 0 5 2367.80 2365.29 16.76 o 0 0 6 2.59 1.51 3.35 < 0 0 7 406.62 421.57 9.90 o 0 0 8 87.04 91.14 14.91 o 0 2 -7 44.40 40.87 6.20 o 0 2 -6 516.14 518.77 11.41 o 0 2 -5 25.27 30.99 2.68 o 0 2 -4 1183.22 1236.49 7.08 o 0 2 -3 459.13 459.28 3.36 o 0 2 -2 801.61 780.11 2.87 o 0 2 -1 13351.60 14334.50 8.47 o 0 2 0 38.70 39.73 0.50 o 0 2 1 14404.30 14952.70 8.38 o 0 2 2 1664.39 1663.17 4.26 o 0 2 3 1154.24 1143.61 4.39 o 0 2 4 2090.06 2068.19 7.45 o 0 2 5 255.74 254.70 6.20 o 0 2 6 1108.96 1147.17 7.40 o 0 2 7 4.29 6.87 6.36 < 0 4 -7 110.53 104.56 7.37 o 0 4 -6 253.22 261.20 7.88 o 0 4 -5 0.69 5.53 3.52 < 0 4 -4 514.23 509.47 7.89 o 0 4 -3 137.70 117.17 1.68 o 0 4 -2 594.89 629.97 2.02 o 0 4 -1 1865.68 1918.76 2.73 o 0 4 0 1341.38 1234.83 2.38 o 0 4 1 1086.62 1052.93 3.22 o 0 4 2 1305.62 1360.75 4.57 o 0 4 3 742.98 717.65 3.53 o 0 4 4 30.78 35.18 3.35 o 0 4 5 206.16 215.58 3.69 o 0 4 6 10.00 8.04 4.02 < 0 4 7 494.56 499.92 7.89 o 0 6 -7 300.56 314.08 9.06 o 0 6 -6 2.10 5.19 5.53 < 0 6 -5 1134.24 1151.75 8.08 o 0 6 -4 491.67 506.43 5.54 o 0 6 -3 953.99 922.61 5.55 o 0 6 -2 518.98 536.01 2.69 o 0 6 -1 72.23 65.52 2.01 o 0 6 0 9296.50 8885.02 10.22 o 0 6 1 46.44 37.86 1.34 o 0 6 2 185.54 201.38 2.18 o 0 6 3 352.02 340.29 7.89 o 0 6 4 144.14 138.93 3.35 o 0 6 5 536.79 524.54 4.87 o 0 6 6 104.82 108.24 5.03 o 0 6 7 87.93 82.77 4.86 o 0 8 -6 660.97 662.80 10.41 o 0 8 -5 72.20 71.87 4.86 o 0 8 -4 948.01 969.17 6.39 o 0 8 -3 713.60 693.43 5.88 o 0 8 -2 1413.64 1375.24 6.24 o 0 8 -1 3699.34 3666.30 6.49 o 0 8 0 28.17 30.32 1.68 o 0 8 1 3333.66 3243.60 9.72 o 0 8 2 1357.85 1309.71 6.91 o 0 8 3 716.59 711.91 5.54 o 0 8 4 736.20 725.90 5.88 o 0 8 5 52.41 51.76 3.69 o 0 8 6 617.97 609.13 8.39 o 0 10 -6 7.93 4.86 6.53 < 0 10 -5 169.50 157.38 6.70 o 0 10 -4 3.51 2.68 3.35 < 0 10 -3 766.51 786.61 9.58 o 0 10 -2 1119.61 1111.48 8.41 o 0 10 -1 55.86 57.46 5.36 o 0 10 0 1427.48 1451.53 8.09 o 0 10 1 106.01 107.41 3.18 o 0 10 2 1315.98 1311.78 7.41 o 0 10 3 963.66 922.91 6.39 o 0 10 4 92.62 92.49 5.70 o 0 10 5 322.56 317.62 5.70 o 0 10 6 51.60 54.44 6.70 o 0 12 -5 33.14 40.03 11.56 o 0 12 -4 13.79 11.39 7.87 < 0 12 -3 10.17 13.23 7.03 < 0 12 -2 11.48 9.04 5.69 < 0 12 -1 262.87 288.04 8.89 o 0 12 0 140.27 134.06 6.20 o 0 12 1 301.86 310.89 6.04 o 0 12 2 72.15 72.88 4.02 o 0 12 3 30.29 31.66 4.02 o 0 12 4 91.02 102.20 5.53 o 0 12 5 7.05 11.22 10.55 < 0 14 -3 72.25 71.03 11.22 o 0 14 -2 192.23 203.32 10.56 o 0 14 -1 288.30 311.21 10.73 o 0 14 0 65.29 74.05 9.21 o 0 14 1 181.44 178.17 7.71 o 0 14 2 105.91 105.90 8.21 o 0 14 3 32.47 27.64 9.38 < 1 -15 -2 200.83 211.54 11.40 o 1 -15 -1 113.68 123.83 8.71 o 1 -15 0 104.17 112.10 10.05 o 1 -15 1 182.07 190.07 11.40 o 1 -13 -4 12.07 9.88 5.19 < 1 -13 -3 479.39 479.25 8.22 o 1 -13 -2 256.76 254.67 5.87 o 1 -13 -1 761.68 766.20 10.58 o 1 -13 0 505.95 533.50 9.57 o 1 -13 1 101.29 96.18 9.22 o 1 -13 2 680.86 735.06 13.77 o 1 -13 3 108.07 107.07 11.23 o 1 -13 4 507.63 479.99 13.26 o 1 -11 -5 41.17 46.07 5.86 o 1 -11 -4 480.92 482.27 8.39 o 1 -11 -3 10.98 14.07 3.18 o 1 -11 -2 652.20 649.71 5.54 o 1 -11 -1 626.25 628.85 5.37 o 1 -11 0 469.85 478.10 5.87 o 1 -11 1 500.40 473.95 7.22 o 1 -11 2 17.34 17.75 3.52 o 1 -11 3 1413.57 1410.54 10.95 o 1 -11 4 183.89 185.37 9.55 o 1 -11 5 111.10 113.94 7.04 o 1 -9 -6 1.46 0.33 5.53 < 1 -9 -5 2.77 3.01 4.52 < 1 -9 -4 272.66 268.61 4.86 o 1 -9 -3 473.80 453.46 5.71 o 1 -9 -2 61.85 61.65 2.35 o 1 -9 -1 0.79 -0.67 2.18 < 1 -9 0 47.90 47.07 2.51 o 1 -9 1 30.11 29.82 1.84 o 1 -9 2 884.33 868.98 6.05 o 1 -9 3 243.22 248.13 4.02 o 1 -9 4 243.55 251.81 4.36 o 1 -9 5 182.91 193.75 5.53 o 1 -9 6 6.80 12.06 6.03 < 1 -7 -7 2.86 3.01 4.86 < 1 -7 -6 478.45 488.64 6.71 o 1 -7 -5 933.26 955.22 6.39 o 1 -7 -4 41.32 39.20 2.51 o 1 -7 -3 1093.98 1062.30 5.56 o 1 -7 -2 373.97 377.12 5.20 o 1 -7 -1 2107.40 2016.96 6.11 o 1 -7 0 936.30 968.70 3.54 o 1 -7 1 28.75 25.46 1.17 o 1 -7 2 1268.40 1219.49 4.72 o 1 -7 3 15.70 18.26 3.35 o 1 -7 4 799.37 782.45 6.39 o 1 -7 5 24.35 26.97 4.86 o 1 -7 6 101.53 111.59 7.20 o 1 -7 7 75.13 66.68 12.90 o 1 -5 -7 490.65 483.30 7.89 o 1 -5 -6 212.94 224.12 4.86 o 1 -5 -5 242.33 249.98 4.36 o 1 -5 -4 3219.08 3220.60 11.06 o 1 -5 -3 276.03 264.38 3.02 o 1 -5 -2 3772.35 3563.14 7.74 o 1 -5 -1 3994.30 4082.32 8.31 o 1 -5 0 3569.60 3597.38 6.74 o 1 -5 1 4798.38 4609.71 11.84 o 1 -5 2 179.34 182.78 2.18 o 1 -5 3 4933.86 4834.35 16.17 o 1 -5 4 209.45 199.84 3.86 o 1 -5 5 328.85 322.68 6.37 o 1 -5 6 539.15 537.09 10.41 o 1 -5 7 14.44 10.72 6.36 < 1 -3 -8 275.21 245.47 12.91 o 1 -3 -7 6.84 5.86 5.36 < 1 -3 -6 181.26 202.64 4.53 o 1 -3 -5 502.82 531.95 5.20 o 1 -3 -4 58.65 67.52 2.01 o 1 -3 -3 7246.32 7096.24 9.33 o 1 -3 -2 1740.52 1792.72 5.11 o 1 -3 0 4672.34 4362.14 7.34 o 1 -3 1 6972.36 7216.43 8.90 o 1 -3 2 12377.60 12148.30 24.69 o 1 -3 3 82.30 81.11 2.01 o 1 -3 4 1768.36 1744.07 8.62 o 1 -3 5 1191.24 1205.14 8.42 o 1 -3 6 291.85 316.08 8.55 o 1 -3 7 419.56 422.77 10.90 o 1 -1 -8 34.36 30.82 10.89 < 1 -1 -7 138.33 140.26 7.71 o 1 -1 -6 103.29 109.92 4.69 o 1 -1 -5 226.40 237.91 4.19 o 1 -1 -4 1438.21 1477.68 5.40 o 1 -1 -3 12.16 20.27 1.17 o 1 -1 -2 224.11 215.46 1.34 o 1 -1 -1 15.16 21.11 0.50 o 1 -1 0 366.22 362.51 1.52 o 1 -1 1 6960.63 7148.91 9.77 o 1 -1 2 51.10 61.33 1.84 o 1 -1 3 3470.44 3453.27 8.58 o 1 -1 4 19.44 27.81 2.85 o 1 -1 5 272.60 278.53 6.20 o 1 -1 6 743.12 762.31 12.09 o 1 -1 7 9.19 17.59 6.20 < 1 1 -8 14.54 19.93 7.03 < 1 1 -7 564.65 562.83 8.06 o 1 1 -6 19.71 31.66 4.52 o 1 1 -5 11.25 25.46 3.52 o 1 1 -4 3296.47 3207.72 8.70 o 1 1 -3 289.53 305.36 2.52 o 1 1 -2 1169.28 1067.78 3.74 o 1 1 -1 393.01 386.02 1.86 o 1 1 0 683.91 699.31 2.22 o 1 1 1 5958.37 6516.71 6.65 o 1 1 2 320.22 327.51 2.35 o 1 1 3 2017.51 2004.86 6.12 o 1 1 4 315.50 310.70 4.53 o 1 1 5 7.40 16.58 3.01 o 1 1 6 221.57 246.76 5.53 o 1 1 7 56.75 66.67 9.72 o 1 3 -7 56.05 68.68 6.03 o 1 3 -6 420.28 425.46 8.22 o 1 3 -5 857.96 861.82 7.90 o 1 3 -4 281.28 302.94 9.23 o 1 3 -3 8717.73 8288.24 16.71 o 1 3 -2 2641.60 2703.31 5.32 o 1 3 0 4448.30 4193.45 4.28 o 1 3 1 6665.62 6897.97 9.76 o 1 3 2 11311.80 11514.70 16.54 o 1 3 3 170.93 166.49 2.35 o 1 3 4 1159.66 1219.47 9.60 o 1 3 5 827.39 862.23 7.23 o 1 3 6 147.97 150.83 5.36 o 1 3 7 235.99 235.71 6.87 o 1 5 -7 438.06 420.45 7.21 o 1 5 -6 100.03 104.05 7.37 o 1 5 -5 102.38 90.82 4.86 o 1 5 -4 2582.40 2592.22 12.21 o 1 5 -3 208.88 203.74 2.85 o 1 5 -2 3221.65 2979.41 7.03 o 1 5 -1 3130.50 3132.90 4.47 o 1 5 0 3701.41 3514.39 4.67 o 1 5 1 4951.64 4874.67 22.81 o 1 5 2 260.98 268.11 3.02 o 1 5 3 5090.09 5120.54 14.46 o 1 5 4 394.69 374.33 5.03 o 1 5 5 455.51 436.61 4.87 o 1 5 6 673.39 663.16 9.24 o 1 5 7 63.07 67.85 5.86 o 1 7 -7 95.17 103.21 7.87 o 1 7 -6 138.82 121.49 6.87 o 1 7 -5 373.03 357.45 8.05 o 1 7 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86.45 4.19 o 3 -5 -5 1701.82 1634.88 8.60 o 3 -5 -4 78.89 73.39 4.19 o 3 -5 -3 2824.30 2617.93 10.55 o 3 -5 -2 1471.36 1464.89 4.73 o 3 -5 -1 3327.97 3197.54 8.23 o 3 -5 0 3099.63 3140.03 8.73 o 3 -5 1 455.49 480.94 4.70 o 3 -5 2 5229.05 5061.05 16.03 o 3 -5 3 420.08 426.10 4.36 o 3 -5 4 403.99 397.79 5.37 o 3 -5 5 747.35 759.79 9.41 o 3 -5 6 66.74 65.67 7.04 o 3 -3 -8 35.29 32.33 7.04 o 3 -3 -7 70.74 72.04 5.86 o 3 -3 -6 585.19 609.24 7.89 o 3 -3 -5 8.21 14.57 3.85 o 3 -3 -4 2159.02 2116.39 8.13 o 3 -3 -3 2.98 7.20 1.51 o 3 -3 -2 2775.55 2648.53 5.48 o 3 -3 -1 3893.80 3954.52 7.29 o 3 -3 0 4231.20 4591.59 7.67 o 3 -3 1 4112.42 3877.08 9.87 o 3 -3 2 7.88 5.53 2.85 < 3 -3 3 3297.76 3332.99 12.44 o 3 -3 4 1898.82 1950.87 10.13 o 3 -3 5 136.98 147.80 5.70 o 3 -3 6 381.40 383.11 8.39 o 3 -3 7 38.27 41.88 7.54 o 3 -1 -8 22.64 28.64 8.54 o 3 -1 -7 89.20 95.84 5.86 o 3 -1 -6 89.90 91.98 4.19 o 3 -1 -5 964.20 983.11 6.73 o 3 -1 -4 696.75 642.11 4.54 o 3 -1 -3 92.89 121.51 1.68 o 3 -1 -2 120.62 157.78 2.01 o 3 -1 -1 3211.63 3624.39 7.82 o 3 -1 0 1036.63 1049.58 3.90 o 3 -1 1 663.68 702.32 3.20 o 3 -1 2 2027.34 2052.83 6.46 o 3 -1 3 104.88 113.96 3.02 o 3 -1 4 315.76 310.47 5.20 o 3 -1 5 499.22 533.02 5.71 o 3 -1 6 1.79 1.67 5.36 < 3 -1 7 256.23 262.05 10.23 o 3 1 -8 226.09 237.21 7.71 o 3 1 -7 24.93 35.18 5.53 o 3 1 -6 44.39 54.44 3.85 o 3 1 -5 2362.20 2294.98 10.16 o 3 1 -4 36.11 53.10 2.85 o 3 1 -3 1358.85 1317.03 4.74 o 3 1 -2 200.60 184.58 2.52 o 3 1 -1 5461.85 5796.26 10.50 o 3 1 0 1839.27 1838.27 5.13 o 3 1 1 387.36 401.08 2.35 o 3 1 2 1982.22 1975.13 5.95 o 3 1 3 8.63 17.25 2.18 o 3 1 4 79.24 84.28 3.18 o 3 1 5 172.61 188.05 5.20 o 3 1 6 79.43 78.41 5.36 o 3 1 7 55.98 52.60 14.07 o 3 3 -8 3.14 -0.67 6.87 < 3 3 -7 172.43 177.49 5.70 o 3 3 -6 1015.15 1051.57 9.42 o 3 3 -5 130.24 141.77 4.02 o 3 3 -4 3297.65 3256.00 14.48 o 3 3 -3 67.62 71.38 1.68 o 3 3 -2 4092.62 3644.79 11.76 o 3 3 -1 4860.24 4802.01 11.72 o 3 3 0 4864.21 4931.50 11.02 o 3 3 1 4495.81 4585.68 8.85 o 3 3 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13.44 11.72 3.52 o 3 9 -2 306.38 310.93 6.21 o 3 9 -1 179.43 198.80 4.02 o 3 9 0 22.71 25.46 2.51 o 3 9 1 465.91 452.62 4.70 o 3 9 2 327.23 337.77 3.35 o 3 9 3 219.58 216.41 3.52 o 3 9 4 40.01 37.19 3.85 o 3 9 5 30.76 33.17 4.02 o 3 11 -5 430.97 428.50 14.60 o 3 11 -4 57.15 61.31 10.22 o 3 11 -3 911.12 912.72 13.11 o 3 11 -2 268.36 260.38 7.54 o 3 11 -1 387.72 416.68 8.56 o 3 11 0 582.39 578.84 6.72 o 3 11 1 74.56 76.73 4.36 o 3 11 2 1374.44 1396.16 9.26 o 3 11 3 66.86 62.66 3.69 o 3 11 4 57.96 52.44 4.19 o 3 13 -4 398.57 367.55 20.63 o 3 13 -2 497.34 529.80 11.41 o 3 13 -1 120.95 110.43 7.37 o 3 13 0 144.18 146.30 8.71 o 3 13 1 1181.02 1233.09 15.99 o 3 13 2 132.23 134.73 8.71 o 3 13 3 333.23 310.10 10.40 o 4 -14 -3 54.02 65.50 13.23 o 4 -14 -2 3.23 4.69 5.86 < 4 -14 -1 195.72 203.49 8.05 o 4 -14 0 1.00 0.33 7.37 < 4 -14 1 2.96 5.69 7.87 < 4 -12 -4 70.44 65.67 5.53 o 4 -12 -3 296.09 292.94 6.04 o 4 -12 -2 10.13 13.90 4.02 o 4 -12 -1 307.99 311.73 6.88 o 4 -12 0 13.99 15.07 4.52 o 4 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265.25 7.88 o 4 0 -6 2.48 1.84 3.52 < 4 0 -5 1192.97 1196.51 9.43 o 4 0 -4 2280.82 2175.11 9.83 o 4 0 -3 213.97 221.56 3.19 o 4 0 -2 6180.28 6179.61 10.36 o 4 0 -1 99.42 86.83 2.85 o 4 0 0 8645.22 8475.15 11.53 o 4 0 1 4596.83 4793.35 9.53 o 4 0 2 1470.33 1534.96 7.27 o 4 0 3 1448.00 1543.98 10.12 o 4 0 4 103.57 99.87 3.18 o 4 0 5 2163.09 2323.46 13.51 o 4 0 6 236.18 247.78 6.71 o 4 2 -8 118.35 108.92 7.54 o 4 2 -7 16.85 21.61 5.19 o 4 2 -6 183.75 191.74 5.70 o 4 2 -5 1.21 9.55 3.52 < 4 2 -4 254.73 269.00 5.37 o 4 2 -3 2724.64 2713.12 6.98 o 4 2 -2 597.38 621.08 3.87 o 4 2 -1 3830.12 3891.63 11.23 o 4 2 0 1026.44 1077.01 3.88 o 4 2 1 2173.84 2252.71 7.31 o 4 2 2 911.37 983.83 5.72 o 4 2 3 125.97 116.64 3.18 o 4 2 4 2043.71 2112.43 8.95 o 4 2 5 36.38 37.02 5.53 o 4 2 6 330.66 352.35 7.38 o 4 4 -7 18.28 21.61 5.53 o 4 4 -6 136.40 158.53 4.69 o 4 4 -5 0.72 9.55 3.01 o 4 4 -4 194.39 206.70 3.69 o 4 4 -3 1210.84 1252.36 6.41 o 4 4 -2 1909.46 1804.43 6.27 o 4 4 -1 611.41 617.89 3.70 o 4 4 0 10.38 10.22 1.51 o 4 4 1 174.93 178.23 3.02 o 4 4 2 34.99 30.66 2.68 o 4 4 3 641.78 657.96 6.89 o 4 4 4 223.97 224.64 5.70 o 4 4 5 205.81 218.41 6.03 o 4 4 6 1.08 -0.67 6.36 < 4 6 -7 256.07 256.35 8.05 o 4 6 -6 1.69 1.84 4.69 < 4 6 -5 714.52 746.96 6.89 o 4 6 -4 983.47 1034.44 8.07 o 4 6 -3 63.28 59.14 3.35 o 4 6 -2 2357.69 2204.62 11.36 o 4 6 -1 6.23 7.03 1.51 o 4 6 0 2180.33 2142.57 6.44 o 4 6 1 1027.28 1056.46 10.61 o 4 6 2 185.30 188.25 3.69 o 4 6 3 430.33 411.59 5.20 o 4 6 4 9.47 10.89 3.35 o 4 6 5 753.78 753.75 8.74 o 4 6 6 18.24 20.94 5.86 o 4 8 -6 485.96 491.51 8.89 o 4 8 -5 58.88 59.30 6.20 o 4 8 -4 313.10 307.39 6.20 o 4 8 -3 1679.66 1658.80 9.78 o 4 8 -2 86.81 84.45 4.19 o 4 8 -1 2591.69 2514.45 10.34 o 4 8 0 592.70 611.80 4.87 o 4 8 1 867.07 874.91 6.39 o 4 8 2 939.21 912.51 6.39 o 4 8 3 305.49 295.97 5.03 o 4 8 4 1274.88 1239.57 9.26 o 4 8 5 16.47 14.40 4.86 < 4 10 -6 11.31 10.22 9.04 < 4 10 -5 194.04 179.68 9.39 o 4 10 -4 20.98 15.24 7.37 < 4 10 -3 1.28 1.84 5.19 < 4 10 -2 1666.71 1563.89 12.98 o 4 10 -1 112.90 118.97 5.19 o 4 10 0 334.02 331.57 5.53 o 4 10 1 159.74 151.67 3.52 o 4 10 2 446.38 455.53 5.87 o 4 10 3 1007.76 998.82 7.57 o 4 10 4 14.95 14.91 3.85 o 4 12 -4 11.03 17.42 10.05 < 4 12 -3 53.11 48.25 10.05 o 4 12 -2 112.50 109.42 10.39 o 4 12 -1 119.44 129.53 8.21 o 4 12 0 7.64 9.88 6.53 < 4 12 1 13.67 17.92 6.53 < 4 12 2 58.58 62.82 5.70 o 4 12 3 0.60 0.33 4.52 < 4 14 -2 24.23 30.82 10.89 < 4 14 -1 354.35 384.76 17.11 o 4 14 0 20.54 19.43 7.87 < 4 14 1 32.19 40.37 12.06 o 5 -13 -3 161.83 157.04 6.03 o 5 -13 -2 133.27 128.20 6.54 o 5 -13 -1 311.99 329.18 7.04 o 5 -13 0 811.89 835.44 14.45 o 5 -13 1 10.36 8.54 6.03 < 5 -13 2 286.31 288.74 8.05 o 5 -11 -5 2.33 4.86 5.69 < 5 -11 -4 192.07 187.39 6.87 o 5 -11 -3 4.45 3.85 4.19 < 5 -11 -2 141.20 146.30 6.20 o 5 -11 -1 418.70 423.43 5.87 o 5 -11 0 43.09 45.56 4.02 o 5 -11 1 774.50 811.60 7.56 o 5 -11 2 12.62 12.39 4.19 < 5 -11 3 161.12 156.53 5.87 o 5 -11 4 379.38 288.69 16.61 o 5 -9 -6 185.09 172.47 5.70 o 5 -9 -5 15.38 15.41 4.52 o 5 -9 -4 96.66 82.94 5.36 o 5 -9 -3 37.20 39.03 3.69 o 5 -9 -2 22.00 22.28 3.52 o 5 -9 -1 89.34 89.64 3.35 o 5 -9 0 266.25 268.44 4.19 o 5 -9 1 178.56 187.55 4.19 o 5 -9 2 241.73 228.50 4.53 o 5 -9 3 10.79 11.05 4.19 < 5 -9 4 3.44 6.53 4.86 < 5 -7 -7 96.90 85.95 6.37 o 5 -7 -6 2.16 4.52 4.19 < 5 -7 -5 1018.04 983.75 6.89 o 5 -7 -4 96.61 87.80 3.02 o 5 -7 -3 342.74 328.42 4.86 o 5 -7 -2 152.32 153.02 4.02 o 5 -7 -1 491.11 518.39 4.87 o 5 -7 0 2623.45 2791.11 9.15 o 5 -7 1 124.21 114.46 3.85 o 5 -7 2 370.93 348.41 5.54 o 5 -7 3 185.99 175.82 4.86 o 5 -7 4 117.42 107.74 7.71 o 5 -7 5 140.32 142.95 6.87 o 5 -5 -7 25.77 28.64 5.86 o 5 -5 -6 696.59 695.13 9.91 o 5 -5 -5 46.37 44.89 3.02 o 5 -5 -4 1270.36 1211.94 7.41 o 5 -5 -3 459.80 444.82 5.04 o 5 -5 -2 1392.39 1423.25 9.45 o 5 -5 -1 2438.39 2495.63 9.84 o 5 -5 0 169.55 195.80 4.02 o 5 -5 1 4497.49 4470.29 16.44 o 5 -5 2 211.43 192.12 4.19 o 5 -5 3 653.90 605.61 6.05 o 5 -5 4 731.67 718.92 9.24 o 5 -5 5 169.39 163.58 7.37 o 5 -5 6 371.83 332.12 13.25 o 5 -3 -7 230.33 249.28 9.56 o 5 -3 -6 33.44 34.00 5.03 o 5 -3 -5 417.29 410.05 7.05 o 5 -3 -4 48.27 50.42 3.69 o 5 -3 -3 1869.21 1943.49 7.10 o 5 -3 -2 1080.54 1120.16 5.56 o 5 -3 -1 102.56 127.71 2.18 o 5 -3 0 3682.75 3832.97 8.22 o 5 -3 1 54.06 49.93 2.35 o 5 -3 2 3608.76 3439.64 15.68 o 5 -3 3 623.97 635.33 6.55 o 5 -3 4 126.31 121.99 4.19 o 5 -3 5 545.95 554.40 9.23 o 5 -3 6 153.03 163.73 8.38 o 5 -1 -8 36.29 28.64 8.71 o 5 -1 -7 15.85 19.93 7.37 < 5 -1 -6 135.14 144.79 5.70 o 5 -1 -5 495.37 474.66 7.89 o 5 -1 -4 52.25 83.43 4.19 o 5 -1 -3 4.51 24.12 2.01 o 5 -1 -1 186.33 220.86 3.02 o 5 -1 0 1467.99 1481.89 5.58 o 5 -1 1 3139.14 3010.48 8.02 o 5 -1 2 5.73 7.70 4.35 < 5 -1 3 150.95 153.52 4.02 o 5 -1 4 108.02 112.26 4.19 o 5 -1 5 15.77 17.08 4.69 o 5 -1 6 383.11 383.29 10.90 o 5 1 -8 21.14 25.96 6.70 o 5 1 -7 51.96 60.47 6.20 o 5 1 -6 625.47 610.00 8.73 o 5 1 -5 7.00 25.29 3.52 o 5 1 -4 936.36 928.91 5.89 o 5 1 -3 525.52 470.36 5.04 o 5 1 -2 1149.78 1203.04 6.07 o 5 1 -1 1212.95 1234.04 7.94 o 5 1 0 413.33 428.61 3.69 o 5 1 1 3990.65 4101.15 9.43 o 5 1 2 15.21 19.76 2.68 o 5 1 3 132.96 139.43 3.18 o 5 1 4 62.93 72.20 3.35 o 5 1 5 1.44 -2.68 6.20 < 5 1 6 171.70 180.34 10.39 o 5 3 -7 449.52 446.14 9.23 o 5 3 -6 7.98 6.87 4.02 < 5 3 -5 737.09 726.28 7.73 o 5 3 -4 216.42 211.24 4.86 o 5 3 -2 1923.98 1899.98 8.98 o 5 3 -1 317.30 348.89 3.19 o 5 3 0 4218.29 4266.60 8.07 o 5 3 1 147.18 150.52 3.02 o 5 3 2 3706.29 3808.01 12.28 o 5 3 3 626.95 659.00 6.72 o 5 3 4 95.38 96.68 4.19 o 5 3 5 430.55 442.58 8.56 o 5 3 6 99.27 104.89 7.37 o 5 5 -7 13.05 11.72 6.70 < 5 5 -6 530.26 492.26 8.73 o 5 5 -5 1.99 2.68 3.18 < 5 5 -4 798.86 775.63 7.23 o 5 5 -3 250.26 234.93 6.04 o 5 5 -2 1236.16 1212.20 7.08 o 5 5 -1 1932.52 1847.28 7.45 o 5 5 0 43.88 42.38 3.52 o 5 5 1 4029.18 4020.47 21.01 o 5 5 2 306.50 312.79 5.70 o 5 5 3 661.63 651.96 6.89 o 5 5 4 675.58 662.50 10.92 o 5 5 5 230.71 225.81 6.54 o 5 7 -7 0.02 3.85 8.04 < 5 7 -6 79.19 85.95 7.37 o 5 7 -5 345.70 310.78 9.22 o 5 7 -4 25.62 37.19 3.69 o 5 7 -3 38.35 33.34 3.35 o 5 7 -2 4.40 7.70 2.85 < 5 7 -1 78.03 70.54 2.51 o 5 7 0 1783.02 1752.21 8.95 o 5 7 1 191.27 182.38 3.35 o 5 7 2 256.36 250.66 4.53 o 5 7 3 184.36 179.01 4.69 o 5 7 4 212.56 208.53 5.53 o 5 7 5 244.51 249.63 6.20 o 5 9 -6 0.97 -3.01 9.38 < 5 9 -5 215.52 220.26 10.39 o 5 9 -4 0.94 -2.85 9.21 < 5 9 -3 506.08 535.70 7.89 o 5 9 -2 87.41 94.33 4.36 o 5 9 -1 0.65 2.51 3.35 < 5 9 0 516.31 517.28 6.71 o 5 9 1 48.07 46.24 3.02 o 5 9 2 311.50 320.29 6.37 o 5 9 3 6.49 3.68 3.68 < 5 9 4 13.45 15.58 5.02 o 5 11 -5 56.91 55.28 11.56 o 5 11 -4 442.81 452.00 15.10 o 5 11 -3 52.58 52.60 8.71 o 5 11 -2 387.58 424.55 10.57 o 5 11 -1 675.08 699.94 9.57 o 5 11 0 92.13 98.18 7.37 o 5 11 1 906.58 927.16 10.76 o 5 11 2 45.57 42.72 4.19 o 5 11 3 165.90 162.90 5.36 o 5 13 -2 80.49 72.04 12.73 o 5 13 -1 266.82 281.01 14.59 o 5 13 0 884.22 939.23 14.62 o 5 13 1 20.93 18.26 8.04 < 6 -12 -4 212.01 189.76 8.88 o 6 -12 -3 10.09 12.90 5.53 < 6 -12 -2 224.67 219.43 6.37 o 6 -12 -1 31.31 32.16 4.69 o 6 -12 0 88.34 95.17 5.19 o 6 -12 1 44.96 48.58 4.86 o 6 -12 2 1.75 0.50 4.52 < 6 -10 -5 123.84 122.49 6.87 o 6 -10 -4 110.63 115.62 5.86 o 6 -10 -3 1060.91 1000.88 9.42 o 6 -10 -2 11.78 16.75 4.35 o 6 -10 -1 361.34 376.38 6.37 o 6 -10 0 466.76 485.60 7.38 o 6 -10 1 498.29 517.04 7.38 o 6 -10 2 460.60 465.45 6.88 o 6 -10 3 6.28 6.87 4.69 < 6 -8 -6 0.72 0.33 5.53 < 6 -8 -5 112.33 122.82 5.53 o 6 -8 -4 738.22 722.13 9.57 o 6 -8 -3 12.28 14.57 3.35 o 6 -8 -2 1004.75 1004.38 7.23 o 6 -8 -1 184.52 202.81 4.19 o 6 -8 0 644.30 679.12 9.07 o 6 -8 1 839.64 833.56 7.56 o 6 -8 2 183.57 187.05 5.36 o 6 -8 3 965.96 962.85 12.61 o 6 -8 4 13.76 12.56 4.86 < 6 -6 -7 28.56 21.61 6.20 o 6 -6 -6 157.62 188.37 6.03 o 6 -6 -5 3.03 4.02 3.52 < 6 -6 -4 152.47 153.85 3.52 o 6 -6 -3 634.44 623.24 6.21 o 6 -6 -2 0.28 -1.51 3.01 < 6 -6 -1 478.68 493.15 4.70 o 6 -6 0 67.49 71.04 3.52 o 6 -6 1 37.56 36.18 4.02 o 6 -6 2 779.76 712.42 9.24 o 6 -6 3 1.24 2.34 3.85 < 6 -6 4 701.99 652.82 8.90 o 6 -6 5 15.83 15.74 5.69 < 6 -4 -7 4.25 15.41 6.36 < 6 -4 -6 170.52 164.08 6.54 o 6 -4 -5 41.79 46.57 3.35 o 6 -4 -4 18.04 23.62 3.18 o 6 -4 -3 1542.35 1492.57 7.93 o 6 -4 -2 120.99 150.49 4.86 o 6 -4 -1 70.19 78.41 3.18 o 6 -4 0 187.07 192.79 4.02 o 6 -4 1 145.35 152.01 5.03 o 6 -4 2 314.17 296.52 5.70 o 6 -4 3 639.93 596.96 6.38 o 6 -4 4 255.06 243.27 5.53 o 6 -4 5 0.12 -1.34 5.86 < 6 -2 -7 470.80 463.29 9.56 o 6 -2 -6 19.99 20.27 4.69 o 6 -2 -5 399.19 392.39 6.04 o 6 -2 -4 1263.92 1224.53 8.93 o 6 -2 -3 34.77 37.36 2.85 o 6 -2 -2 2656.10 2773.57 9.51 o 6 -2 -1 917.56 931.45 6.73 o 6 -2 0 947.83 1004.20 6.06 o 6 -2 1 1099.07 1103.92 8.08 o 6 -2 2 115.25 106.58 3.85 o 6 -2 3 2021.12 2136.14 11.15 o 6 -2 4 5.73 7.37 4.19 < 6 -2 5 248.35 252.99 6.37 o 6 -2 6 168.90 143.97 15.08 o 6 0 -7 0.89 1.84 6.03 < 6 0 -6 917.94 950.91 10.42 o 6 0 -5 256.01 257.70 7.38 o 6 0 -4 3.33 4.35 2.51 < 6 0 -3 2226.70 2285.59 9.82 o 6 0 -2 825.68 840.92 7.40 o 6 0 -1 2924.23 3114.77 11.41 o 6 0 0 1087.90 1064.76 5.39 o 6 0 1 453.35 450.58 4.87 o 6 0 2 2595.65 2780.54 14.41 o 6 0 3 161.63 163.41 5.36 o 6 0 4 1774.89 1944.21 11.47 o 6 0 5 82.58 91.98 6.70 o 6 0 6 75.42 69.03 9.05 o 6 2 -7 154.59 159.38 7.04 o 6 2 -6 26.60 25.96 5.03 o 6 2 -5 118.97 113.28 4.52 o 6 2 -4 406.45 431.39 6.88 o 6 2 -3 152.87 163.42 6.03 o 6 2 -1 415.57 426.55 4.36 o 6 2 0 480.30 521.04 5.04 o 6 2 1 521.92 564.88 5.54 o 6 2 2 56.80 56.79 4.36 o 6 2 3 2094.14 2263.89 10.47 o 6 2 4 2.31 -1.67 4.52 < 6 2 5 282.26 296.61 7.55 o 6 4 -7 264.54 290.39 8.05 o 6 4 -6 0.67 3.85 4.19 < 6 4 -5 88.45 88.30 4.19 o 6 4 -4 213.98 226.65 4.19 o 6 4 -3 279.69 258.76 4.53 o 6 4 -2 859.93 863.82 7.06 o 6 4 -1 32.87 34.34 4.19 o 6 4 0 4.81 3.18 4.52 < 6 4 1 8.94 8.88 3.18 < 6 4 2 172.75 178.84 4.53 o 6 4 3 590.60 595.83 7.22 o 6 4 4 270.82 280.33 7.38 o 6 4 5 10.40 7.20 5.86 < 6 6 -7 0.76 1.17 8.37 < 6 6 -6 636.78 674.49 10.58 o 6 6 -5 224.67 232.01 6.03 o 6 6 -4 2.36 1.00 3.52 < 6 6 -3 1258.31 1275.65 9.43 o 6 6 -2 190.94 200.65 4.86 o 6 6 -1 1376.47 1387.42 6.91 o 6 6 0 237.61 251.16 5.20 o 6 6 1 140.95 144.29 4.19 o 6 6 2 911.18 886.09 9.25 o 6 6 3 9.74 13.06 3.85 o 6 6 4 607.89 608.26 8.56 o 6 6 5 4.17 3.18 5.02 < 6 8 -6 4.04 6.70 8.88 < 6 8 -5 216.85 214.90 9.89 o 6 8 -4 818.20 818.63 8.57 o 6 8 -3 24.97 23.62 4.36 o 6 8 -2 1162.55 1177.96 8.58 o 6 8 -1 269.70 277.83 5.70 o 6 8 0 848.69 834.11 6.39 o 6 8 1 748.03 724.53 7.39 o 6 8 2 216.42 216.74 5.36 o 6 8 3 1058.43 1045.28 9.92 o 6 8 4 27.35 25.46 4.86 o 6 10 -5 21.54 17.08 9.55 < 6 10 -4 17.88 11.39 10.38 < 6 10 -3 670.09 677.93 11.08 o 6 10 -2 6.30 8.88 6.03 < 6 10 -1 206.18 209.53 6.20 o 6 10 0 220.12 219.93 9.22 o 6 10 1 449.21 468.62 7.89 o 6 10 2 454.14 453.36 6.21 o 6 10 3 5.20 5.02 4.35 < 6 12 -3 106.49 109.92 12.90 o 6 12 -2 26.94 17.42 10.72 < 6 12 -1 26.80 31.16 8.71 o 6 12 0 26.61 23.79 8.21 < 6 12 1 10.35 13.57 8.54 < 7 -11 -4 0.39 0.50 6.03 < 7 -11 -3 147.25 177.97 7.21 o 7 -11 -2 215.84 213.23 7.21 o 7 -11 -1 3.41 5.19 5.36 < 7 -11 0 363.56 371.68 9.06 o 7 -11 1 24.87 24.29 4.69 o 7 -11 2 208.65 200.99 7.88 o 7 -9 -5 46.33 36.18 7.71 o 7 -9 -4 3.40 3.68 5.53 < 7 -9 -3 92.17 97.18 5.86 o 7 -9 -2 47.72 50.09 4.36 o 7 -9 -1 206.36 221.09 5.53 o 7 -9 0 195.38 192.93 7.21 o 7 -9 1 42.33 39.70 4.69 o 7 -9 2 0.07 -0.33 4.69 < 7 -9 3 1.15 2.01 4.86 < 7 -7 -6 315.62 284.92 8.05 o 7 -7 -5 1.37 3.68 5.53 < 7 -7 -4 341.22 336.77 6.71 o 7 -7 -3 213.49 210.71 4.19 o 7 -7 -2 313.08 315.28 4.86 o 7 -7 -1 890.27 936.48 6.56 o 7 -7 0 74.62 76.56 3.85 o 7 -7 1 620.82 628.63 7.22 o 7 -7 2 351.08 359.92 7.55 o 7 -7 3 68.18 71.54 5.86 o 7 -7 4 59.09 51.93 6.37 o 7 -5 -7 301.24 287.09 8.55 o 7 -5 -6 11.30 10.22 5.19 < 7 -5 -5 529.11 549.83 8.56 o 7 -5 -4 44.32 49.42 3.85 o 7 -5 -3 873.66 853.45 7.56 o 7 -5 -2 1008.21 1019.91 7.57 o 7 -5 -1 89.26 94.83 3.18 o 7 -5 0 2116.67 2196.04 9.46 o 7 -5 1 213.05 218.93 4.86 o 7 -5 2 591.52 578.36 7.89 o 7 -5 3 641.02 590.87 9.40 o 7 -5 4 145.87 138.59 7.88 o 7 -3 -7 66.01 59.31 8.88 o 7 -3 -6 294.86 323.96 7.71 o 7 -3 -5 9.95 15.41 4.19 o 7 -3 -4 745.96 766.11 7.56 o 7 -3 -3 2.12 6.87 3.01 < 7 -3 -2 106.30 122.16 4.36 o 7 -3 -1 2223.92 2445.60 16.25 o 7 -3 0 79.89 88.46 3.85 o 7 -3 1 1047.26 1027.68 7.57 o 7 -3 2 259.57 237.41 4.69 o 7 -3 3 233.38 211.90 5.70 o 7 -3 4 738.29 668.37 8.73 o 7 -3 5 66.93 64.83 6.37 o 7 -1 -7 23.09 34.17 7.71 o 7 -1 -6 261.23 228.01 7.88 o 7 -1 -5 189.35 207.17 6.03 o 7 -1 -4 152.53 160.05 5.20 o 7 -1 -3 40.98 59.30 4.86 o 7 -1 -2 2.63 16.08 3.01 o 7 -1 -1 225.82 245.80 5.70 o 7 -1 0 1208.21 1271.78 12.13 o 7 -1 1 25.89 26.47 3.85 o 7 -1 2 1.64 2.34 3.18 < 7 -1 3 110.85 116.12 5.36 o 7 -1 4 32.11 34.34 4.52 o 7 -1 5 310.73 323.99 8.22 o 7 1 -7 282.00 272.64 8.22 o 7 1 -6 1.91 4.86 5.69 < 7 1 -5 853.83 838.29 10.08 o 7 1 -4 4.84 12.23 4.19 < 7 1 -3 654.87 603.23 8.90 o 7 1 -2 410.92 449.41 6.38 o 7 1 -1 5.14 15.24 2.68 o 7 1 0 2058.66 1958.86 12.18 o 7 1 1 13.70 17.75 3.35 o 7 1 2 77.54 80.08 3.69 o 7 1 3 162.84 176.31 5.20 o 7 1 4 20.03 19.26 5.02 o 7 1 5 225.25 231.51 8.21 o 7 3 -7 16.51 17.08 6.53 < 7 3 -6 527.97 534.55 8.39 o 7 3 -5 83.34 96.67 4.52 o 7 3 -4 1449.46 1376.08 10.28 o 7 3 -3 76.86 70.03 3.85 o 7 3 -2 283.59 275.87 6.71 o 7 3 -1 2931.39 2844.57 15.96 o 7 3 0 261.06 263.10 5.37 o 7 3 1 1399.58 1460.02 10.95 o 7 3 2 286.24 314.07 6.20 o 7 3 3 294.76 316.08 9.22 o 7 3 4 719.89 748.78 10.92 o 7 3 5 64.55 70.36 10.39 o 7 5 -7 185.66 178.67 9.39 o 7 5 -6 13.53 10.89 6.36 < 7 5 -5 463.36 419.31 9.90 o 7 5 -4 8.80 6.03 4.02 < 7 5 -3 644.07 623.21 7.39 o 7 5 -2 580.17 558.44 7.05 o 7 5 -1 22.23 20.10 2.85 o 7 5 0 2013.39 1995.93 9.46 o 7 5 1 164.91 163.74 4.36 o 7 5 2 509.57 507.84 7.38 o 7 5 3 512.47 503.14 11.24 o 7 5 4 218.06 241.22 10.39 o 7 7 -6 72.35 52.61 10.05 o 7 7 -5 161.66 172.96 7.54 o 7 7 -4 76.43 76.90 6.20 o 7 7 -3 0.41 0.17 4.86 < 7 7 -2 20.43 19.26 3.85 o 7 7 -1 373.69 364.33 5.70 o 7 7 0 263.28 261.55 4.19 o 7 7 1 324.24 312.76 5.20 o 7 7 2 173.57 169.11 6.54 o 7 7 3 85.95 95.16 5.70 o 7 7 4 59.29 59.30 5.70 o 7 9 -5 9.15 15.58 12.56 < 7 9 -4 341.53 344.82 13.08 o 7 9 -3 4.95 6.87 5.36 < 7 9 -2 6.32 6.03 9.04 < 7 9 -1 606.89 642.34 10.07 o 7 9 0 6.49 6.20 6.20 < 7 9 1 176.82 193.08 6.70 o 7 9 2 1.38 2.68 4.19 < 7 9 3 14.59 12.90 4.69 < 7 11 -3 362.35 391.31 15.10 o 7 11 -2 415.22 419.24 11.91 o 7 11 -1 19.16 21.27 7.87 < 7 11 0 571.78 611.71 13.43 o 7 11 1 78.69 60.65 9.21 o 8 -12 -1 64.48 62.82 7.87 o 8 -10 -4 303.98 286.25 9.73 o 8 -10 -3 11.49 9.88 5.36 < 8 -10 -2 410.06 443.72 7.38 o 8 -10 -1 265.58 265.58 6.54 o 8 -10 0 196.85 188.23 6.87 o 8 -10 1 239.77 233.20 7.54 o 8 -10 2 9.65 6.36 7.20 < 8 -8 -5 285.83 276.50 9.05 o 8 -8 -4 4.84 4.02 5.53 < 8 -8 -3 374.05 379.92 9.06 o 8 -8 -2 87.67 91.81 5.70 o 8 -8 -1 520.34 533.87 8.56 o 8 -8 0 293.94 287.40 6.71 o 8 -8 1 61.52 65.50 5.03 o 8 -8 2 717.24 725.61 10.08 o 8 -8 3 40.08 46.07 7.20 o 8 -6 -6 7.16 1.67 7.54 < 8 -6 -5 60.26 51.10 6.53 o 8 -6 -4 393.57 425.74 7.21 o 8 -6 -3 38.58 32.66 4.19 o 8 -6 -2 105.32 101.71 4.52 o 8 -6 -1 2.88 5.69 3.52 < 8 -6 0 134.72 137.75 4.69 o 8 -6 1 420.04 410.52 8.72 o 8 -6 2 28.50 33.00 5.03 o 8 -6 3 322.07 315.61 6.20 o 8 -6 4 30.21 16.42 13.07 < 8 -4 -6 87.91 87.96 8.88 o 8 -4 -5 0.47 9.71 4.86 < 8 -4 -4 514.11 475.12 7.22 o 8 -4 -3 100.14 110.92 4.19 o 8 -4 -2 495.41 520.61 6.38 o 8 -4 -1 63.13 60.98 3.02 o 8 -4 0 95.40 97.51 4.19 o 8 -4 1 79.74 87.29 4.02 o 8 -4 2 159.90 145.30 6.20 o 8 -4 3 401.50 409.65 9.23 o 8 -4 4 0.70 0.67 4.86 < 8 -2 -7 1.18 -2.51 8.71 < 8 -2 -6 103.90 109.92 7.54 o 8 -2 -5 720.24 684.45 14.28 o 8 -2 -4 2.10 7.20 4.02 < 8 -2 -3 1361.46 1382.03 10.95 o 8 -2 -2 73.01 78.41 4.52 o 8 -2 -1 1019.12 1075.78 6.73 o 8 -2 0 449.51 460.29 4.70 o 8 -2 1 178.19 169.79 3.85 o 8 -2 2 1223.27 1147.15 10.60 o 8 -2 3 3.37 1.17 4.02 < 8 -2 4 263.74 251.33 7.54 o 8 0 -7 201.54 196.62 8.05 o 8 0 -6 37.32 29.82 5.86 o 8 0 -5 7.74 8.37 6.20 < 8 0 -4 1642.22 1713.84 15.51 o 8 0 -3 45.53 46.74 5.36 o 8 0 -2 1041.98 1072.54 9.42 o 8 0 -1 68.63 73.88 3.69 o 8 0 0 915.64 914.18 6.39 o 8 0 1 1653.26 1543.28 9.95 o 8 0 2 44.50 39.53 4.52 o 8 0 3 860.30 857.58 8.74 o 8 0 4 147.79 149.15 6.87 o 8 2 -7 16.56 22.28 6.20 o 8 2 -6 0.37 4.52 5.53 < 8 2 -5 201.55 234.33 7.04 o 8 2 -4 147.27 135.07 7.21 o 8 2 -3 815.34 840.77 11.60 o 8 2 -2 9.21 17.42 5.19 o 8 2 -1 349.16 370.19 7.88 o 8 2 0 126.52 139.59 4.69 o 8 2 1 71.08 74.39 5.19 o 8 2 2 1041.74 1096.70 9.08 o 8 2 3 5.76 7.70 5.86 < 8 2 4 225.37 227.99 7.54 o 8 4 -6 4.92 7.70 5.53 < 8 4 -5 254.48 259.86 6.54 o 8 4 -4 54.42 48.58 4.52 o 8 4 -3 631.84 635.56 8.73 o 8 4 -2 56.38 52.60 5.86 o 8 4 -1 81.78 75.23 5.86 o 8 4 0 8.35 7.03 3.85 < 8 4 1 3.78 3.52 4.02 < 8 4 2 341.71 355.21 8.05 o 8 4 3 255.47 260.87 8.05 o 8 4 4 0.05 0.00 7.20 < 8 6 -6 45.50 45.73 8.04 o 8 6 -5 1.22 1.17 6.20 < 8 6 -4 961.56 950.89 11.77 o 8 6 -3 49.63 51.76 5.19 o 8 6 -2 573.69 556.49 8.90 o 8 6 -1 36.46 34.34 4.36 o 8 6 0 365.97 372.36 5.70 o 8 6 1 848.48 878.55 9.75 o 8 6 2 1.49 2.01 4.69 < 8 6 3 375.68 382.27 9.23 o 8 8 -5 307.01 307.38 11.40 o 8 8 -4 1.34 -0.50 6.20 < 8 8 -3 591.01 590.42 9.40 o 8 8 -2 110.12 116.62 6.87 o 8 8 -1 602.66 595.99 10.58 o 8 8 0 339.15 339.61 8.72 o 8 8 1 105.54 102.54 4.86 o 8 8 2 830.91 834.84 9.91 o 8 10 -3 12.57 12.90 7.20 < 8 10 -2 250.80 243.77 10.39 o 8 10 -1 103.09 95.34 6.70 o 8 10 0 120.86 121.32 8.38 o 8 10 1 174.60 167.44 10.39 o 9 -9 -4 56.06 60.98 7.71 o 9 -9 -3 12.71 4.52 5.86 < 9 -9 -2 62.87 69.19 7.04 o 9 -9 -1 228.11 224.47 8.72 o 9 -9 0 14.00 13.90 5.86 < 9 -9 1 0.20 0.17 5.36 < 9 -7 -5 306.95 310.90 7.71 o 9 -7 -4 76.28 67.85 6.20 o 9 -7 -3 42.73 50.25 8.04 o 9 -7 -2 442.40 450.32 9.06 o 9 -7 -1 2.13 2.01 5.69 < 9 -7 0 631.24 631.82 10.24 o 9 -7 1 101.78 100.70 7.37 o 9 -7 2 43.01 43.05 6.70 o 9 -5 -6 157.36 172.29 9.55 o 9 -5 -5 12.79 12.39 5.69 < 9 -5 -4 374.13 363.81 6.88 o 9 -5 -3 436.57 447.62 7.72 o 9 -5 -2 2.23 2.34 3.85 < 9 -5 -1 1211.29 1232.39 12.29 o 9 -5 0 93.62 91.48 4.36 o 9 -5 1 534.66 526.85 7.38 o 9 -5 2 257.53 256.18 8.89 o 9 -5 3 150.71 151.00 5.70 o 9 -3 -6 0.60 3.68 7.37 < 9 -3 -5 109.19 114.94 7.71 o 9 -3 -4 1.76 6.20 4.86 < 9 -3 -3 46.85 67.34 5.19 o 9 -3 -2 1194.98 1339.75 9.09 o 9 -3 -1 58.08 60.64 3.69 o 9 -3 0 518.93 501.82 5.37 o 9 -3 1 118.44 119.31 6.53 o 9 -3 2 398.83 401.93 9.56 o 9 -3 3 301.00 290.77 7.71 o 9 -1 -6 30.41 31.16 7.54 o 9 -1 -5 134.85 141.43 8.71 o 9 -1 -4 1.75 9.38 6.70 < 9 -1 -3 44.88 70.36 5.70 o 9 -1 -2 257.21 268.26 5.37 o 9 -1 -1 494.65 514.04 5.87 o 9 -1 0 241.96 240.07 5.03 o 9 -1 1 44.85 50.59 4.86 o 9 -1 2 30.49 30.82 5.70 o 9 -1 3 18.56 17.08 4.86 o 9 1 -6 204.19 200.98 7.88 o 9 1 -5 1.06 6.20 6.03 < 9 1 -4 223.15 230.33 7.04 o 9 1 -3 506.70 509.18 9.57 o 9 1 -2 14.76 23.62 5.36 o 9 1 -1 1162.81 1159.74 15.65 o 9 1 0 6.55 14.74 5.19 < 9 1 1 282.18 273.98 6.54 o 9 1 2 111.59 117.79 8.88 o 9 1 3 47.47 45.56 7.37 o 9 3 -6 25.74 21.27 5.86 o 9 3 -5 274.70 252.68 7.21 o 9 3 -4 46.53 52.27 5.36 o 9 3 -3 157.96 177.98 6.87 o 9 3 -2 1768.89 1768.33 18.89 o 9 3 -1 2.71 -1.17 5.19 < 9 3 0 728.83 707.83 12.77 o 9 3 1 200.11 206.84 6.03 o 9 3 2 548.33 544.67 9.90 o 9 3 3 401.87 395.40 11.91 o 9 5 -6 151.33 129.71 7.88 o 9 5 -5 0.38 -2.51 6.36 < 9 5 -4 160.78 159.88 6.70 o 9 5 -3 278.77 261.40 7.21 o 9 5 -2 2.39 2.68 4.69 < 9 5 -1 1022.44 963.91 9.25 o 9 5 0 30.77 29.82 4.36 o 9 5 1 397.53 383.14 9.23 o 9 5 2 240.20 229.84 7.21 o 9 5 3 158.18 151.00 9.72 o 9 7 -5 77.43 81.76 10.55 o 9 7 -4 2.57 2.85 6.70 < 9 7 -3 23.24 26.30 6.70 o 9 7 -2 122.11 112.94 6.54 o 9 7 -1 95.57 86.96 7.54 o 9 7 0 259.85 249.81 5.87 o 9 7 1 11.42 8.88 4.52 < 9 7 2 11.88 9.21 5.36 < 9 9 -4 1.90 0.50 8.88 < 9 9 -3 31.08 44.56 8.04 o 9 9 -2 406.59 418.73 11.07 o 9 9 -1 12.06 15.91 6.53 < 9 9 0 112.03 114.28 10.56 o 10 -8 -3 40.32 38.86 7.54 o 10 -8 -2 211.84 217.75 10.39 o 10 -8 -1 68.58 73.04 8.88 o 10 -8 0 23.94 16.75 10.05 < 10 -6 -5 84.88 92.15 7.20 o 10 -6 -4 56.90 51.09 7.54 o 10 -6 -3 27.98 36.85 7.04 o 10 -6 -2 0.30 -0.84 5.69 < 10 -6 -1 47.89 56.62 6.03 o 10 -6 0 132.10 122.50 5.70 o 10 -6 1 91.54 88.13 6.87 o 10 -4 -5 150.19 154.85 10.06 o 10 -4 -4 0.89 -3.01 7.70 < 10 -4 -3 257.42 243.44 9.22 o 10 -4 -2 11.45 3.68 5.19 < 10 -4 -1 10.78 8.88 6.36 < 10 -4 0 198.76 206.34 8.38 o 10 -4 1 40.45 40.71 7.54 o 10 -4 2 332.92 322.17 8.72 o 10 -2 -5 1.79 1.51 7.54 < 10 -2 -4 331.04 332.06 8.89 o 10 -2 -3 77.46 72.38 6.03 o 10 -2 -2 423.09 442.73 6.54 o 10 -2 -1 290.42 291.76 6.37 o 10 -2 0 25.35 22.11 6.20 o 10 -2 1 938.56 879.38 11.77 o 10 -2 2 2.73 5.19 7.70 < 10 0 -6 16.12 23.95 7.87 o 10 0 -5 366.14 374.71 8.89 o 10 0 -4 2.99 -1.84 6.53 < 10 0 -3 214.73 218.08 9.05 o 10 0 -2 134.98 154.17 7.21 o 10 0 -1 384.79 421.87 7.88 o 10 0 0 777.44 799.85 11.76 o 10 0 1 15.31 19.60 5.69 o 10 0 2 750.40 758.64 14.28 o 10 2 -5 16.92 19.93 5.86 o 10 2 -4 111.00 110.76 7.71 o 10 2 -3 9.14 9.88 6.36 < 10 2 -2 102.58 128.18 8.04 o 10 2 -1 101.20 104.22 7.54 o 10 2 0 0.77 -1.00 7.03 < 10 2 1 545.72 554.07 9.06 o 10 2 2 17.44 15.07 6.87 < 10 4 -5 2.83 9.04 6.36 < 10 4 -4 116.97 101.21 7.04 o 10 4 -3 7.21 4.02 5.86 < 10 4 -2 117.33 116.62 8.04 o 10 4 -1 54.19 55.11 5.70 o 10 4 0 19.43 27.64 5.53 o 10 4 1 215.16 202.83 6.54 o 10 4 2 112.33 104.39 6.87 o 10 6 -4 6.53 4.86 7.54 < 10 6 -3 206.00 215.06 9.72 o 10 6 -2 60.64 63.32 5.86 o 10 6 -1 282.23 261.91 8.05 o 10 6 0 421.46 378.99 8.05 o 10 6 1 10.33 6.70 6.03 < 10 8 -3 32.85 20.44 14.41 < 10 8 -2 275.07 274.82 11.90 o 10 8 -1 133.12 114.96 9.05 o 11 -5 -4 82.11 93.99 8.38 o 11 -5 -3 2.27 4.19 6.36 < 11 -5 -2 489.15 477.10 10.07 o 11 -5 -1 72.18 64.50 6.53 o 11 -5 0 207.07 202.66 8.72 o 11 -3 -4 39.51 44.06 6.70 o 11 -3 -3 189.34 194.93 7.37 o 11 -3 -2 24.00 24.46 5.53 o 11 -3 -1 212.79 238.70 7.21 o 11 -3 0 111.94 106.57 9.38 o 11 -3 1 124.89 128.19 10.05 o 11 -1 -5 24.98 38.69 9.38 o 11 -1 -4 0.22 7.20 11.56 < 11 -1 -3 96.68 109.75 9.22 o 11 -1 -2 38.98 55.45 7.54 o 11 -1 -1 54.07 43.22 6.37 o 11 -1 0 18.00 28.31 10.55 < 11 -1 1 5.76 3.85 12.06 < 11 1 -4 90.03 91.48 8.71 o 11 1 -3 0.71 2.68 7.20 < 11 1 -2 345.50 340.30 12.91 o 11 1 -1 21.40 23.11 7.70 o 11 1 0 173.65 162.91 10.06 o 11 1 1 72.87 61.99 7.71 o 11 3 -4 144.01 132.22 10.39 o 11 3 -3 378.87 355.78 8.89 o 11 3 -2 1.39 4.19 6.70 < 11 3 -1 363.98 379.24 10.73 o 11 3 0 205.24 189.41 8.38 o 11 3 1 265.98 218.64 12.07 o 11 5 -3 0.48 -1.84 7.70 < 11 5 -2 308.87 292.29 10.06 o 11 5 -1 14.23 14.07 6.70 < 11 5 0 196.65 176.50 6.70 o 12 -2 -3 293.01 276.51 17.61 o 12 -2 -2 31.93 27.14 14.91 < 12 0 -3 6.94 8.54 9.55 < 12 0 -2 194.79 195.11 11.57 o 12 0 -1 145.20 138.59 10.89 o 12 2 -2 0.41 3.01 14.57 < #======================================================================= data_beta_single #======================================================================= # start Validation Reply Form #_vrf_PLAT213_beta_single #; #PROBLEM: Atom O4 has ADP max/min Ratio ..... 5.5 prolat #RESPONSE: This atom is disordered about the center of inversion. The #distribution of the displacement is not well described by a normal #distribution. #; # end Validation Reply Form # 5. CHEMICAL DATA _chemical_name_systematic ? _chemical_name_common ? _chemical_formula_moiety ? _chemical_formula_structural ? _chemical_formula_analytical ? _chemical_formula_iupac ? _chemical_formula_sum 'Fe2 O7 P2' _chemical_formula_weight 285.6 _chemical_melting_point ? _chemical_compound_source ? _chemical_absolute_configuration . #======================================================================= # 6. CRYSTAL DATA _space_group_crystal_system monoclinic _space_group_name_H-M_alt 'C 1 2/m 1' _space_group_name_Hall '-C 2y' _space_group_IT_number 12 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,y,-z 3 -x,-y,-z 4 x,-y,z 5 x+1/2,y+1/2,z 6 -x+1/2,y+1/2,-z 7 -x+1/2,-y+1/2,-z 8 x+1/2,-y+1/2,z _cell_length_a 6.6154(6) _cell_length_b 8.4624(10) _cell_length_c 4.4920(4) _cell_angle_alpha 90 _cell_angle_beta 103.502(7) _cell_angle_gamma 90 _cell_volume 244.52(4) loop_ _twin_individual_id _twin_individual_mass_fraction_refined _twin_individual_twin_matrix_11 _twin_individual_twin_matrix_12 _twin_individual_twin_matrix_13 _twin_individual_twin_matrix_21 _twin_individual_twin_matrix_22 _twin_individual_twin_matrix_23 _twin_individual_twin_matrix_31 _twin_individual_twin_matrix_32 _twin_individual_twin_matrix_33 ? ? ? ? ? ? ? ? ? ? ? _cell_formula_units_Z 2 _cell_measurement_reflns_used 6240 _cell_measurement_theta_min 3.98 _cell_measurement_theta_max 40.76 _cell_measurement_temperature 470 _cell_special_details ? _exptl_crystal_density_diffrn 3.8795 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_F_000 276 _exptl_crystal_type_of_structure cryst _exptl_absorpt_coefficient_mu 6.566 _exptl_crystal_description 'fragment' _exptl_crystal_colour 'light-brownish' _exptl_crystal_size_max 0.110 _exptl_crystal_size_mid 0.070 _exptl_crystal_size_min 0.040 _exptl_crystal_size_rad 0.030 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; STOE LANA, absorption correction by scaling of reflection intensities. J. Koziskova, F. Hahn, J. Richter, J. Kozisek, "Comparison of different absorption corrections on the model structure of tetrakis(\m~2~-acetato)- diaqua-di-copper(II)", Acta Chimica Slovaca, vol. 9, no. 2, 2016, pp. 136 - 140. Afterwards a spherical absorption correction was performed within STOE LANA. ; _exptl_absorpt_correction_T_min 0.4724 _exptl_absorpt_correction_T_max 0.5578 #======================================================================= # 7. EXPERIMENTAL DATA _diffrn_measurement_device 'Eulerian 4-circle diffractometer' _diffrn_measurement_device_type 'STOE STADIVARI' _diffrn_detector 'EIGER2 1M CDTE' _diffrn_detector_type ? _diffrn_detector_area_resol_mean 13.33 _diffrn_source 'Axo_Mo' _diffrn_source_type ? _diffrn_radiation_probe x-ray _diffrn_source_target ? _diffrn_source_voltage 60 _diffrn_source_current 0.830 _diffrn_source_power 0.050 _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_monochromator 'Graded multilayer mirror' _diffrn_radiation_polarisn_norm -90 _diffrn_radiation_collimation '1.2 0.6 mm diameter' _diffrn_ambient_temperature 470 _diffrn_measurement_method 'rotation method, \w scans' _diffrn_measurement_details ; 1492 frames, detector distance = 80 mm ; _diffrn_reflns_number 3414 _diffrn_reflns_theta_min 3.98 _diffrn_reflns_theta_max 40.82 _diffrn_reflns_theta_full 40.82 _diffrn_measured_fraction_theta_max 0.99 _diffrn_measured_fraction_theta_full 0.99 _diffrn_reflns_av_R_equivalents 0.0119 _diffrn_reflns_av_unetI/netI 0.0032 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_l_min -8 _diffrn_reflns_limit_l_max 3 _diffrn_reflns_reduction_process ? _diffrn_standards_number ? _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% ? loop_ _diffrn_standard_refln_index_h _diffrn_standard_refln_index_k _diffrn_standard_refln_index_l ? ? ? #_diffrn_reflns_av_sigmaI/netI 0.0032 #======================================================================= # 8. REFINEMENT DATA _refine_special_details ? _reflns_number_total 826 _reflns_number_gt 815 _reflns_threshold_expression 'I>3\s(I)' _refine_ls_structure_factor_coef Fsqd _refine_ls_R_factor_gt 0.0194 _refine_ls_wR_factor_gt 0.0819 _refine_ls_R_factor_all 0.0196 _refine_ls_wR_factor_ref 0.0825 _refine_ls_goodness_of_fit_ref 1.8774 _refine_ls_goodness_of_fit_gt 1.8760 _refine_ls_restrained_S_gt ? _refine_ls_restrained_S_all ? _refine_ls_number_reflns 826 _refine_ls_number_parameters 32 _refine_ls_number_restraints 0 _refine_ls_number_constraints 0 _refine_ls_weighting_scheme sigma _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.04P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_hydrogen_treatment ? _refine_ls_shift/su_max 0.0097 _refine_ls_shift/su_mean 0.0018 _refine_diff_density_max 0.62 _refine_diff_density_min -0.69 _refine_ls_extinction_method 'B-C type 1 Gaussian isotropic (Becker & Coppens, 1974)' _refine_ls_extinction_coef 330(100) _refine_ls_extinction_expression ? _refine_ls_abs_structure_details ? _refine_ls_abs_structure_Flack ? _refine_ls_abs_structure_Rogers ? loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Fe 0.3463 0.8444 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' O 0.0106 0.0060 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' P 0.1023 0.0942 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' _computing_data_collection ; X-Area Pilatus3_SV 1.31.194.0 (STOE, 2023) ; _computing_cell_refinement ; X-Area Recipe 2.0.2 (STOE, 2024) ; _computing_data_reduction ; X-Area Integrate 2.5.18.0 (STOE, 2024) X-Area LANA 2.8.4 (STOE, 2024) ; _computing_publication_material ; STOE & Cie GmbH, X-Area, software package for collecting single-crystal or multi-domain crystal data on STOE area-detector diffractometers, for image processing, for the correction and scaling of reflection intensities and for outlier rejection, version 2.4, Darmstadt 2024 ; #======================================================================= # 9. ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_adp_type _atom_site_U_iso_or_equiv _atom_site_site_symmetry_multiplicity _atom_site_occupancy _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_disorder_assembly _atom_site_disorder_group Fe1 Fe 0.5 0.190935(18) 0.5 Uani 0.01503(8) 4 1 d . . . P1 P 0.21350(4) 0 -0.09113(6) Uani 0.00973(9) 4 1 d . . . O1 O 0.37349(14) 0 0.21291(19) Uani 0.01322(18) 4 1 d . . . O2 O 0.22244(12) 0.14875(8) -0.27750(16) Uani 0.01845(17) 8 1 d . . . O3 O 0 0 0 Uani 0.0555(10) 2 1 d . . . loop_ _atom_site_aniso_label _atom_site_aniso_type_symbol _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Fe1 Fe 0.01568(13) 0.00997(12) 0.01659(13) 0 -0.00198(8) 0 P1 P 0.00872(14) 0.01254(15) 0.00779(14) 0 0.00167(10) 0 O1 O 0.0140(3) 0.0152(3) 0.0088(3) 0 -0.0006(2) 0 O2 O 0.0261(3) 0.0134(3) 0.0147(3) 0.0052(2) 0.0024(2) 0.00335(19) O3 O 0.0107(6) 0.119(3) 0.0407(11) 0 0.0137(7) 0 #======================================================================= # 10. MOLECULAR GEOMETRY loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_1 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Fe1 O1 . . 2.1143(6) ? Fe1 O1 . 2_656 2.1143(6) ? Fe1 O2 . 1_556 2.3141(9) ? Fe1 O2 . 2_655 2.3141(9) ? Fe1 O2 . 7_555 2.0780(8) ? Fe1 O2 . 8_556 2.0780(8) ? P1 O1 . . 1.5200(9) ? P1 O2 . . 1.5205(8) ? P1 O2 . 4_555 1.5205(8) ? P1 O3 . . 1.5596(4) ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_2 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag O1 Fe1 O1 . . 2_656 80.33(2) ? O1 Fe1 O2 . . 1_556 84.52(3) ? O1 Fe1 O2 . . 2_655 81.93(3) ? O1 Fe1 O2 . . 7_555 94.05(3) ? O1 Fe1 O2 . . 8_556 158.02(3) ? O1 Fe1 O2 2_656 . 1_556 81.93(3) ? O1 Fe1 O2 2_656 . 2_655 84.52(3) ? O1 Fe1 O2 2_656 . 7_555 158.02(3) ? O1 Fe1 O2 2_656 . 8_556 94.05(3) ? O2 Fe1 O2 1_556 . 2_655 162.25(3) ? O2 Fe1 O2 1_556 . 7_555 76.37(3) ? O2 Fe1 O2 1_556 . 8_556 115.92(3) ? O2 Fe1 O2 2_655 . 7_555 115.92(3) ? O2 Fe1 O2 2_655 . 8_556 76.37(3) ? O2 Fe1 O2 7_555 . 8_556 98.48(3) ? O1 P1 O2 . . . 112.72(3) ? O1 P1 O2 . . 4_555 112.72(3) ? O1 P1 O3 . . . 104.33(4) ? O2 P1 O2 . . 4_555 111.76(4) ? O2 P1 O3 . . . 107.37(3) ? O2 P1 O3 4_555 . . 107.37(3) ? Fe1 O1 Fe1 . . 3_656 99.67(3) ? Fe1 O1 P1 . . . 129.900(17) ? Fe1 O1 P1 3_656 . . 129.900(17) ? Fe1 O2 Fe1 1_554 . 7_555 103.63(3) ? Fe1 O2 P1 1_554 . . 120.15(4) ? Fe1 O2 P1 7_555 . . 133.72(5) ? P1 O3 P1 . . 2_555 180 ? #======================================================================= # 11. STRUCTURE-FACTOR LIST loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_include_status 0 0 1 1550.41 1458.86 2.47 o 0 0 2 1825.80 1627.54 3.85 o 0 0 4 1832.53 1831.49 3.47 o 0 0 5 2300.05 2321.00 6.08 o 0 0 6 2.41 2.59 0.52 o 0 0 7 379.99 433.06 4.32 o 0 2 0 34.77 44.53 0.35 o 0 2 1 13816.20 14436.10 7.13 o 0 2 2 1207.77 1229.38 1.91 o 0 2 3 728.91 759.82 1.73 o 0 2 4 1605.54 1609.76 2.60 o 0 2 5 101.86 103.71 1.04 o 0 2 6 743.75 773.75 2.94 o 0 2 7 7.44 8.63 0.52 o 0 4 0 1321.35 1331.30 2.44 o 0 4 1 1411.20 1519.24 2.09 o 0 4 2 890.05 1020.30 2.60 o 0 4 3 398.94 376.31 0.86 o 0 4 4 202.59 205.07 1.21 o 0 4 5 46.90 45.89 0.69 o 0 4 6 87.33 96.11 1.04 o 0 4 7 249.82 255.64 2.93 o 0 6 0 9133.54 9482.43 6.83 o 0 6 1 57.06 49.87 0.52 o 0 6 2 319.19 360.47 1.21 o 0 6 3 612.67 615.70 1.38 o 0 6 4 267.40 275.70 1.55 o 0 6 5 776.34 806.50 4.32 o 0 6 6 29.22 29.16 0.52 o 0 6 7 164.91 180.87 2.24 o 0 8 0 26.67 27.78 0.52 o 0 8 1 3461.46 3610.83 3.31 o 0 8 2 1330.51 1357.25 2.25 o 0 8 3 687.85 712.44 1.90 o 0 8 4 818.78 835.13 3.28 o 0 8 5 55.90 54.52 0.86 o 0 8 6 587.27 586.52 3.80 o 0 10 0 1422.70 1473.94 3.81 o 0 10 1 71.95 76.95 0.86 o 0 10 2 1191.25 1233.29 2.77 o 0 10 3 823.22 848.77 2.77 o 0 10 4 29.71 24.50 0.69 o 0 10 5 226.76 232.85 2.59 o 0 10 6 22.55 20.87 0.86 o 0 12 0 138.24 134.78 1.55 o 0 12 1 285.77 304.69 2.93 o 0 12 2 31.36 33.81 0.69 o 0 12 3 1.76 1.55 0.35 o 0 12 4 42.51 40.37 1.04 o 0 12 5 2.49 3.28 0.52 o 0 14 0 64.57 70.91 2.24 o 0 14 1 223.11 214.89 2.76 o 0 14 2 125.78 130.63 1.55 o 0 14 3 46.66 43.48 1.21 o 1 1 -8 1.31 1.73 0.35 o 1 1 -7 299.74 316.79 2.24 o 1 1 -6 8.58 8.97 0.52 o 1 1 -5 37.37 33.30 0.52 o 1 1 -4 2253.02 2151.79 2.26 o 1 1 -3 44.51 54.18 1.04 o 1 1 -2 607.58 534.07 1.39 o 1 1 -1 131.63 127.18 0.69 o 1 1 0 517.67 510.20 1.57 o 1 1 1 6391.99 6459.31 3.13 o 1 1 2 151.28 158.86 0.69 o 1 1 3 2636.74 2656.43 2.44 o 1 1 4 117.35 112.86 0.69 o 1 1 5 81.30 88.34 0.86 o 1 1 6 431.00 444.51 2.94 o 1 1 7 6.39 7.07 0.52 o 1 3 -8 352.59 359.83 5.35 o 1 3 -7 22.29 27.95 0.86 o 1 3 -6 270.96 292.26 2.07 o 1 3 -5 659.32 678.33 2.07 o 1 3 -4 144.24 145.15 0.69 o 1 3 -3 7905.61 7549.31 10.17 o 1 3 -2 2098.47 2269.02 3.84 o 1 3 -1 573.18 437.76 1.21 o 1 3 0 4507.87 4604.30 4.67 o 1 3 1 6809.12 7470.18 6.34 o 1 3 2 11585.90 11745.80 6.78 o 1 3 3 118.35 121.68 0.69 o 1 3 4 1389.11 1450.66 2.60 o 1 3 5 961.93 1008.63 2.59 o 1 3 6 184.43 192.61 2.24 o 1 3 7 301.01 302.46 4.14 o 1 5 -7 439.29 442.10 3.28 o 1 5 -6 145.07 150.48 1.38 o 1 5 -5 154.02 152.73 1.21 o 1 5 -4 2835.53 2843.00 4.00 o 1 5 -3 234.71 233.09 0.86 o 1 5 -2 3505.02 3456.01 3.50 o 1 5 -1 3460.30 3738.28 4.21 o 1 5 0 3646.74 3612.98 6.86 o 1 5 1 4803.23 4886.73 6.36 o 1 5 2 218.63 230.16 1.04 o 1 5 3 4847.42 5008.29 4.73 o 1 5 4 284.25 290.74 1.38 o 1 5 5 360.88 377.80 2.94 o 1 5 6 574.24 585.63 2.76 o 1 5 7 27.11 26.91 1.38 o 1 7 -7 17.51 18.46 0.86 o 1 7 -6 267.24 254.79 1.90 o 1 7 -5 597.04 596.39 2.94 o 1 7 -4 142.57 150.49 1.21 o 1 7 -3 676.81 686.78 1.90 o 1 7 -2 184.82 186.60 0.86 o 1 7 -1 1894.00 1934.84 2.26 o 1 7 0 795.03 846.15 1.38 o 1 7 1 14.24 10.87 0.17 o 1 7 2 1443.66 1496.50 2.43 o 1 7 3 1.35 1.55 0.17 o 1 7 4 980.98 1003.45 2.77 o 1 7 5 99.04 98.01 1.21 o 1 7 6 25.25 27.26 1.04 o 1 9 -6 16.31 17.60 0.86 o 1 9 -5 48.12 51.93 1.04 o 1 9 -4 109.77 115.10 1.38 o 1 9 -3 701.59 738.32 2.42 o 1 9 -2 11.65 12.94 0.35 o 1 9 -1 10.15 10.01 0.35 o 1 9 0 43.70 40.03 0.52 o 1 9 1 18.14 19.67 0.35 o 1 9 2 732.62 742.59 1.90 o 1 9 3 346.46 363.98 1.55 o 1 9 4 102.58 105.78 1.21 o 1 9 5 74.50 74.54 1.21 o 1 9 6 1.62 1.90 0.35 o 1 11 -5 70.60 72.29 1.55 o 1 11 -4 567.95 588.21 2.76 o 1 11 -3 1.97 2.59 0.17 o 1 11 -2 736.71 763.20 3.63 o 1 11 -1 599.30 615.59 2.59 o 1 11 0 513.35 540.84 1.90 o 1 11 1 490.51 472.57 2.59 o 1 11 2 5.95 6.04 0.35 o 1 11 3 1175.28 1213.62 3.63 o 1 11 4 132.90 137.71 1.73 o 1 11 5 68.64 63.32 1.38 o 1 13 -4 9.22 9.49 0.52 o 1 13 -3 408.36 410.12 3.11 o 1 13 -2 216.09 211.95 2.24 o 1 13 -1 770.65 814.91 3.46 o 1 13 0 462.73 474.76 2.76 o 1 13 1 94.82 91.28 1.38 o 1 13 2 674.43 680.46 3.11 o 1 13 3 106.26 109.57 1.55 o 1 13 4 473.18 466.85 3.97 o 1 15 -2 152.97 152.21 1.73 o 1 15 -1 73.30 72.64 1.73 o 1 15 0 102.67 107.50 2.59 o 1 15 1 184.85 195.03 2.24 o 2 0 -8 237.20 257.36 3.28 o 2 0 -7 37.29 36.75 1.21 o 2 0 -6 1381.51 1415.70 6.23 o 2 0 -5 45.53 53.83 0.86 o 2 0 -4 1515.22 1438.92 2.60 o 2 0 -2 5738.97 5483.28 5.74 o 2 0 -1 20754.10 20904.60 8.80 o 2 0 0 124.70 107.45 0.69 o 2 0 1 2191.61 1863.28 2.28 o 2 0 2 9672.09 9141.81 4.91 o 2 0 3 2582.24 2469.32 3.83 o 2 0 4 1989.97 2070.34 6.07 o 2 0 5 24.06 22.77 0.69 o 2 0 6 1227.87 1247.01 6.40 o 2 0 7 240.95 246.15 5.01 o 2 2 -8 6.22 7.25 0.52 o 2 2 -7 487.55 504.67 2.59 o 2 2 -6 14.44 14.66 0.52 o 2 2 -5 986.26 969.96 2.42 o 2 2 -4 46.63 46.93 0.35 o 2 2 -3 1766.15 1695.80 6.78 o 2 2 -2 6927.53 6555.52 4.68 o 2 2 -1 53.98 59.89 0.69 o 2 2 0 5390.19 5234.03 6.87 o 2 2 1 3069.21 3252.49 2.11 o 2 2 2 1392.08 1338.07 1.56 o 2 2 3 2258.63 2362.24 2.78 o 2 2 4 45.75 44.86 0.52 o 2 2 5 1295.72 1369.30 4.50 o 2 2 6 1.94 2.24 0.35 o 2 2 7 202.03 207.81 3.45 o 2 4 -7 167.99 179.66 1.73 o 2 4 -6 54.28 50.72 0.86 o 2 4 -5 35.51 41.75 0.69 o 2 4 -4 689.76 652.47 1.73 o 2 4 -3 1.09 0.86 0.17 o 2 4 -2 1642.46 1683.76 3.65 o 2 4 -1 1880.20 1861.55 2.62 o 2 4 1 234.57 241.12 1.21 o 2 4 2 0.24 1.21 0.00 o 2 4 3 245.41 257.77 1.21 o 2 4 4 442.81 461.01 1.73 o 2 4 5 90.33 95.59 1.04 o 2 4 6 208.13 202.98 2.24 o 2 4 7 32.47 38.65 1.55 o 2 6 -7 0.71 1.90 0.35 o 2 6 -6 500.01 521.10 2.42 o 2 6 -5 1.21 1.38 0.17 o 2 6 -4 362.07 365.23 1.38 o 2 6 -3 553.84 574.63 1.73 o 2 6 -2 347.86 326.81 1.04 o 2 6 -1 4520.60 4568.47 4.57 o 2 6 0 49.27 45.03 0.69 o 2 6 1 627.15 632.07 1.21 o 2 6 2 1695.56 1698.67 2.08 o 2 6 3 405.03 409.86 1.38 o 2 6 4 556.23 560.44 2.25 o 2 6 5 71.10 70.74 0.86 o 2 6 6 513.28 534.42 5.18 o 2 8 -7 241.29 235.96 2.59 o 2 8 -6 25.01 23.46 0.86 o 2 8 -5 746.93 725.00 3.28 o 2 8 -4 305.79 296.26 2.76 o 2 8 -3 688.10 667.33 2.07 o 2 8 -2 2153.90 2182.45 2.78 o 2 8 -1 76.83 72.13 0.52 o 2 8 0 3803.23 3901.20 3.49 o 2 8 1 1314.17 1335.60 1.91 o 2 8 2 685.42 711.96 1.73 o 2 8 3 871.75 866.08 2.25 o 2 8 4 173.82 176.90 1.38 o 2 8 5 1075.30 1108.68 3.81 o 2 8 6 20.69 22.08 0.86 o 2 10 -6 129.89 108.54 1.73 o 2 10 -5 84.46 79.54 1.38 o 2 10 -4 802.93 781.10 2.94 o 2 10 -3 344.41 350.15 2.07 o 2 10 -2 3.87 5.18 0.35 o 2 10 -1 1847.75 1905.87 3.12 o 2 10 0 391.63 397.36 1.38 o 2 10 1 1019.55 1086.77 2.59 o 2 10 2 308.93 307.31 1.73 o 2 10 3 78.27 78.51 1.21 o 2 10 4 688.91 706.75 3.63 o 2 10 5 61.22 54.69 1.73 o 2 12 -5 59.05 48.31 1.38 o 2 12 -4 0.51 0.52 0.17 < 2 12 -3 15.40 13.46 0.69 o 2 12 -2 186.97 197.27 1.90 o 2 12 -1 87.46 90.41 1.21 o 2 12 0 329.11 355.48 2.59 o 2 12 1 10.17 9.83 0.52 o 2 12 2 2.18 3.80 0.35 o 2 12 3 55.60 54.87 1.21 o 2 12 4 0.29 0.35 0.17 < 2 14 -3 29.17 31.23 0.86 o 2 14 -2 97.55 92.66 1.38 o 2 14 -1 14.07 16.04 0.69 o 2 14 0 403.57 431.01 3.80 o 2 14 1 83.82 85.76 1.73 o 2 14 2 8.93 6.21 0.52 o 3 1 -8 95.37 103.88 1.73 o 3 1 -7 5.70 5.18 0.35 o 3 1 -6 1.38 1.55 0.17 o 3 1 -5 1512.85 1484.90 2.77 o 3 1 -4 243.54 226.01 0.86 o 3 1 -3 527.96 527.03 2.25 o 3 1 -2 3.36 1.38 0.17 o 3 1 -1 4214.40 4366.93 3.38 o 3 1 0 1380.19 1331.44 1.22 o 3 1 1 510.49 501.94 0.87 o 3 1 2 1971.46 1907.86 2.44 o 3 1 3 37.36 44.17 0.52 o 3 1 4 162.38 161.72 1.21 o 3 1 5 296.38 296.08 2.24 o 3 1 6 23.13 22.26 0.86 o 3 1 7 119.23 122.69 2.76 o 3 3 -8 14.39 10.87 0.69 o 3 3 -7 114.16 124.07 1.38 o 3 3 -6 750.28 766.68 2.42 o 3 3 -5 57.49 56.76 0.69 o 3 3 -4 2595.52 2572.57 2.78 o 3 3 -3 21.59 23.81 0.35 o 3 3 -2 3387.40 3265.19 4.03 o 3 3 -1 4356.58 4112.94 4.07 o 3 3 0 4382.16 4493.29 3.36 o 3 3 1 4210.20 4111.89 4.40 o 3 3 2 12.73 11.39 0.17 o 3 3 3 3012.97 2979.16 3.31 o 3 3 4 1588.52 1619.48 3.12 o 3 3 5 94.10 101.11 1.55 o 3 3 6 260.71 274.81 3.28 o 3 3 7 17.39 19.67 1.21 o 3 5 -7 45.56 46.76 1.21 o 3 5 -6 43.11 40.37 0.86 o 3 5 -5 1526.80 1491.70 3.81 o 3 5 -4 44.12 38.47 0.52 o 3 5 -3 2472.91 2390.53 3.48 o 3 5 -2 1068.94 1093.12 1.91 o 3 5 -1 3194.58 3191.39 3.15 o 3 5 0 3058.52 2966.94 5.24 o 3 5 1 338.41 384.18 1.21 o 3 5 2 4988.33 5039.83 4.04 o 3 5 3 440.46 460.68 1.90 o 3 5 4 459.16 465.64 1.73 o 3 5 5 688.43 695.35 3.63 o 3 5 6 84.26 89.55 2.24 o 3 7 -7 141.76 132.71 1.90 o 3 7 -6 112.15 100.60 1.38 o 3 7 -5 174.09 182.08 1.38 o 3 7 -4 936.34 901.34 2.42 o 3 7 -3 219.10 206.97 1.04 o 3 7 -2 823.96 797.35 1.73 o 3 7 -1 7.69 11.21 0.17 o 3 7 0 32.74 35.02 0.35 o 3 7 1 2833.15 2848.07 3.66 o 3 7 2 4.94 6.38 0.17 o 3 7 3 441.34 472.19 1.73 o 3 7 4 50.74 47.62 0.69 o 3 7 5 15.25 16.56 0.52 o 3 7 6 287.59 274.14 3.11 o 3 9 -6 71.14 73.67 1.90 o 3 9 -5 40.32 32.61 0.52 o 3 9 -4 268.52 271.02 2.07 o 3 9 -3 78.29 71.61 1.38 o 3 9 -2 117.71 108.20 0.86 o 3 9 -1 77.50 79.89 0.86 o 3 9 0 1.30 1.04 0.17 o 3 9 1 381.83 382.68 1.55 o 3 9 2 284.90 305.91 1.55 o 3 9 3 273.99 278.79 1.90 o 3 9 4 73.85 70.22 0.86 o 3 9 5 13.65 11.90 0.69 o 3 11 -5 286.60 292.09 3.11 o 3 11 -4 15.70 18.46 0.52 o 3 11 -3 688.54 694.48 3.63 o 3 11 -2 203.93 211.26 1.73 o 3 11 -1 258.94 255.13 2.42 o 3 11 0 469.57 483.59 3.45 o 3 11 1 70.38 64.18 1.04 o 3 11 2 1316.23 1382.95 4.33 o 3 11 3 58.86 51.07 1.04 o 3 11 4 60.83 58.83 1.38 o 3 13 -4 417.99 404.09 3.11 o 3 13 -3 233.21 237.34 2.24 o 3 13 -2 430.27 437.77 2.59 o 3 13 -1 136.66 137.36 2.07 o 3 13 0 155.76 148.59 2.24 o 3 13 1 1072.19 1108.68 5.88 o 3 13 2 99.81 98.01 1.73 o 3 13 3 299.28 310.92 2.76 o 3 15 -1 116.62 115.96 2.07 o 4 0 -8 19.38 20.18 1.04 o 4 0 -7 274.82 285.52 2.42 o 4 0 -6 3.06 3.45 0.35 o 4 0 -5 1198.21 1162.58 2.94 o 4 0 -4 2233.92 2138.37 4.00 o 4 0 -3 221.57 227.74 1.04 o 4 0 -2 5994.52 5905.86 6.21 o 4 0 -1 104.71 77.16 0.52 o 4 0 0 8471.10 8432.82 7.58 o 4 0 1 4409.62 4327.80 5.46 o 4 0 2 1380.23 1354.85 2.60 o 4 0 3 1372.57 1388.73 5.54 o 4 0 4 89.18 81.96 1.38 o 4 0 5 1954.76 2035.35 7.63 o 4 0 6 196.84 186.06 4.49 o 4 2 -8 181.52 193.13 2.24 o 4 2 -7 0.40 0.35 0.17 < 4 2 -6 402.26 395.44 1.73 o 4 2 -5 42.55 41.75 0.52 o 4 2 -4 536.41 515.30 1.56 o 4 2 -3 3338.16 3224.44 2.80 o 4 2 -2 203.88 209.45 0.86 o 4 2 -1 5000.81 4975.11 4.25 o 4 2 0 1291.10 1228.02 2.08 o 4 2 1 2145.51 2188.43 2.96 o 4 2 2 918.70 965.30 1.56 o 4 2 3 114.54 108.37 0.69 o 4 2 4 1703.08 1697.48 4.16 o 4 2 5 6.16 7.07 0.52 o 4 2 6 212.36 204.70 3.28 o 4 4 -7 103.86 97.84 2.07 o 4 4 -6 11.71 14.84 0.35 o 4 4 -5 104.45 88.87 0.86 o 4 4 -4 24.22 24.50 0.52 o 4 4 -3 521.15 541.26 1.90 o 4 4 -2 2944.18 2889.79 3.32 o 4 4 -1 223.03 220.68 0.86 o 4 4 0 4.43 6.04 0.17 o 4 4 1 89.23 86.63 0.52 o 4 4 2 41.10 40.89 0.52 o 4 4 3 535.87 545.10 1.90 o 4 4 4 297.55 288.14 1.55 o 4 4 5 110.82 109.92 1.90 o 4 4 6 6.85 7.76 0.86 o 4 6 -7 113.64 119.24 2.42 o 4 6 -6 24.38 18.11 0.69 o 4 6 -5 425.18 432.25 2.25 o 4 6 -4 509.97 521.18 1.90 o 4 6 -3 1.48 1.38 0.17 o 4 6 -2 1698.26 1743.12 2.60 o 4 6 -1 11.53 12.42 0.35 o 4 6 0 1716.28 1689.17 2.60 o 4 6 1 854.20 859.36 1.73 o 4 6 2 147.60 151.70 1.04 o 4 6 3 455.33 451.48 1.73 o 4 6 4 1.83 3.28 0.17 o 4 6 5 789.97 797.15 4.15 o 4 6 6 34.12 32.43 1.55 o 4 8 -7 18.31 19.32 1.38 o 4 8 -6 420.08 404.43 3.11 o 4 8 -5 53.19 52.10 0.86 o 4 8 -4 259.39 262.90 1.55 o 4 8 -3 1422.44 1437.88 3.98 o 4 8 -2 72.10 68.50 0.69 o 4 8 -1 2535.27 2517.54 4.17 o 4 8 0 523.72 539.55 1.90 o 4 8 1 706.26 703.30 1.90 o 4 8 2 916.90 921.66 2.25 o 4 8 3 299.93 296.59 1.73 o 4 8 4 1140.07 1146.74 3.98 o 4 8 5 10.30 8.80 0.52 o 4 10 -6 43.65 38.65 0.86 o 4 10 -5 258.13 244.08 2.07 o 4 10 -4 62.35 51.93 0.86 o 4 10 -3 18.11 16.91 0.52 o 4 10 -2 1867.29 1846.15 6.76 o 4 10 -1 136.90 141.34 1.73 o 4 10 0 370.40 365.89 2.07 o 4 10 1 207.43 212.64 1.55 o 4 10 2 400.37 408.21 1.90 o 4 10 3 852.84 878.69 3.63 o 4 10 4 5.26 6.38 0.52 o 4 12 -5 3.64 5.35 0.69 o 4 12 -4 5.26 3.45 0.52 o 4 12 -3 150.88 128.22 2.07 o 4 12 -2 43.91 46.93 1.04 o 4 12 -1 198.60 201.76 2.07 o 4 12 0 0.16 1.04 0.17 o 4 12 1 22.61 22.43 0.52 o 4 12 2 66.03 71.09 1.21 o 4 12 3 0.42 1.04 0.35 < 4 14 -2 1.76 2.59 0.35 o 4 14 -1 252.15 263.76 2.93 o 4 14 0 5.18 4.83 0.52 o 4 14 1 12.92 10.01 0.69 o 5 1 -8 0.32 0.00 0.17 < 5 1 -7 2.74 3.80 0.35 o 5 1 -6 318.25 312.66 1.55 o 5 1 -5 147.73 139.79 0.86 o 5 1 -4 365.33 360.94 1.38 o 5 1 -3 144.72 132.55 0.69 o 5 1 -2 580.44 597.75 1.21 o 5 1 -1 565.27 541.60 1.38 o 5 1 0 814.04 787.22 1.56 o 5 1 1 3378.48 3275.98 2.97 o 5 1 2 7.79 9.14 0.17 o 5 1 3 124.90 125.63 1.04 o 5 1 4 81.66 80.75 1.21 o 5 1 5 1.36 1.38 0.17 o 5 1 6 227.35 226.29 3.45 o 5 3 -7 318.25 330.27 2.76 o 5 3 -6 2.83 3.45 0.17 o 5 3 -5 552.89 554.72 2.42 o 5 3 -4 109.23 109.23 1.21 o 5 3 -3 2377.97 2305.63 3.48 o 5 3 -2 1406.26 1397.59 2.25 o 5 3 -1 190.05 210.27 0.86 o 5 3 0 3771.06 3685.84 3.50 o 5 3 1 91.65 85.76 0.52 o 5 3 2 3383.31 3320.73 4.01 o 5 3 3 569.66 563.59 1.73 o 5 3 4 92.64 95.08 1.38 o 5 3 5 433.71 438.98 4.14 o 5 3 6 98.86 100.08 2.42 o 5 5 -7 19.26 21.56 0.86 o 5 5 -6 577.41 582.35 2.59 o 5 5 -5 16.21 14.49 0.35 o 5 5 -4 1022.62 950.38 3.46 o 5 5 -3 327.72 324.29 1.73 o 5 5 -2 1276.82 1260.13 2.25 o 5 5 -1 2072.82 2069.81 2.78 o 5 5 0 96.89 102.68 0.69 o 5 5 1 4018.71 4063.07 5.24 o 5 5 2 234.45 236.67 1.04 o 5 5 3 582.65 564.95 2.59 o 5 5 4 636.11 629.43 2.76 o 5 5 5 166.07 158.26 2.93 o 5 5 6 366.50 317.54 6.04 o 5 7 -7 23.23 19.67 0.69 o 5 7 -6 12.44 15.01 0.69 o 5 7 -5 609.97 576.01 2.25 o 5 7 -4 5.08 3.45 0.35 o 5 7 -3 154.25 141.17 1.21 o 5 7 -2 28.09 26.57 0.52 o 5 7 -1 228.68 225.79 1.21 o 5 7 0 2060.76 2043.31 3.47 o 5 7 1 145.58 135.82 1.04 o 5 7 2 296.29 307.99 1.90 o 5 7 3 169.12 165.16 1.38 o 5 7 4 134.99 133.91 1.38 o 5 7 5 165.36 151.53 2.93 o 5 9 -6 45.55 37.61 0.69 o 5 9 -5 78.45 88.00 1.21 o 5 9 -4 20.55 18.63 0.52 o 5 9 -3 195.15 211.43 1.73 o 5 9 -2 4.98 5.87 0.35 o 5 9 -1 25.47 21.05 0.52 o 5 9 0 365.03 335.67 2.59 o 5 9 1 98.13 102.15 1.21 o 5 9 2 251.31 245.12 1.90 o 5 9 3 5.83 5.69 0.35 o 5 9 4 7.30 8.45 0.69 o 5 11 -5 20.30 21.22 0.69 o 5 11 -4 290.10 290.37 3.11 o 5 11 -3 20.98 21.56 0.69 o 5 11 -2 223.11 239.06 1.90 o 5 11 -1 511.42 505.39 3.80 o 5 11 0 55.63 54.35 1.21 o 5 11 1 780.52 772.07 3.63 o 5 11 2 20.57 19.67 0.86 o 5 11 3 143.39 135.81 2.24 o 5 13 -3 159.48 155.15 2.42 o 5 13 -2 105.15 100.43 1.38 o 5 13 -1 257.50 278.09 2.93 o 5 13 0 778.47 794.55 5.19 o 5 13 1 11.83 11.56 0.52 o 5 13 2 245.39 260.48 3.11 o 6 0 -7 0.67 0.69 0.17 o 6 0 -6 869.63 874.58 3.80 o 6 0 -5 259.33 246.68 2.07 o 6 0 -4 3.70 3.45 0.17 o 6 0 -3 2136.44 2091.41 3.65 o 6 0 -2 797.61 714.06 2.42 o 6 0 -1 2797.45 2788.86 4.88 o 6 0 0 1017.23 1034.52 2.60 o 6 0 1 423.42 423.73 1.55 o 6 0 2 2379.66 2381.94 5.21 o 6 0 3 134.47 127.18 1.21 o 6 0 4 1552.49 1493.90 6.93 o 6 0 5 68.67 61.08 2.59 o 6 0 6 57.63 50.21 2.59 o 6 2 -7 276.34 277.76 2.59 o 6 2 -6 0.62 0.69 0.17 o 6 2 -5 224.06 219.90 1.90 o 6 2 -4 747.16 716.01 2.07 o 6 2 -3 10.14 13.46 0.35 o 6 2 -2 1903.46 1884.19 3.12 o 6 2 -1 594.06 577.70 1.73 o 6 2 0 655.44 668.20 1.90 o 6 2 1 730.99 741.21 2.59 o 6 2 2 76.71 71.95 0.69 o 6 2 3 1842.65 1822.14 3.99 o 6 2 4 2.97 3.28 0.35 o 6 2 5 224.37 220.42 3.45 o 6 4 -7 75.92 91.10 1.21 o 6 4 -6 41.54 36.75 0.52 o 6 4 -5 1.52 2.07 0.35 o 6 4 -4 25.22 27.60 0.69 o 6 4 -3 745.13 705.34 2.77 o 6 4 -2 391.61 397.07 2.07 o 6 4 -1 3.20 3.11 0.17 o 6 4 0 28.80 28.98 0.52 o 6 4 1 52.26 51.24 0.52 o 6 4 2 217.33 221.80 1.21 o 6 4 3 545.78 542.08 3.11 o 6 4 4 237.16 231.30 2.24 o 6 4 5 1.43 1.04 0.52 < 6 6 -7 5.91 2.93 0.35 o 6 6 -6 333.52 352.38 2.76 o 6 6 -5 68.63 71.43 0.86 o 6 6 -4 32.63 30.36 0.52 o 6 6 -3 871.84 910.70 2.77 o 6 6 -2 44.73 44.86 0.69 o 6 6 -1 827.05 827.02 2.42 o 6 6 0 121.68 124.94 1.04 o 6 6 1 74.89 74.19 0.69 o 6 6 2 767.99 749.97 2.42 o 6 6 3 2.47 2.42 0.17 o 6 6 4 562.84 569.03 5.36 o 6 6 5 7.03 5.52 0.69 o 6 8 -6 2.04 3.11 0.35 o 6 8 -5 150.58 160.49 1.73 o 6 8 -4 724.26 736.02 2.94 o 6 8 -3 20.89 18.46 0.52 o 6 8 -2 1025.66 1030.48 4.67 o 6 8 -1 203.75 210.92 2.07 o 6 8 0 678.69 686.56 4.49 o 6 8 1 728.18 712.89 3.11 o 6 8 2 175.62 179.32 1.73 o 6 8 3 893.93 857.68 3.28 o 6 8 4 13.98 13.63 0.86 o 6 10 -5 59.73 54.00 1.21 o 6 10 -4 56.11 52.62 1.38 o 6 10 -3 781.69 769.13 3.98 o 6 10 -2 1.90 1.55 0.17 o 6 10 -1 264.52 273.78 2.07 o 6 10 0 309.26 305.75 2.93 o 6 10 1 413.89 429.29 3.63 o 6 10 2 412.51 426.01 3.63 o 6 10 3 5.52 4.31 0.52 o 6 12 -4 92.91 85.76 1.73 o 6 12 -3 37.85 43.99 1.04 o 6 12 -2 91.87 89.21 1.38 o 6 12 -1 0.24 0.17 0.17 < 6 12 0 50.60 51.59 1.38 o 6 12 1 24.68 26.57 0.86 o 6 12 2 6.70 7.42 0.52 o 7 1 -7 99.06 98.35 1.73 o 7 1 -6 63.42 57.45 0.86 o 7 1 -5 433.82 439.51 2.07 o 7 1 -4 24.00 25.36 0.69 o 7 1 -3 236.47 228.55 1.73 o 7 1 -2 84.26 82.65 1.04 o 7 1 -1 38.13 37.61 0.52 o 7 1 0 1468.48 1444.39 2.60 o 7 1 1 1.23 1.55 0.17 o 7 1 2 22.99 21.74 0.52 o 7 1 3 120.05 115.44 1.21 o 7 1 4 19.91 19.84 0.69 o 7 1 5 217.84 188.31 3.28 o 7 3 -7 26.71 25.53 0.69 o 7 3 -6 370.85 390.40 2.07 o 7 3 -5 38.56 42.96 1.04 o 7 3 -4 1009.59 1001.42 4.32 o 7 3 -3 26.61 22.43 0.52 o 7 3 -2 172.93 172.60 1.38 o 7 3 -1 2387.79 2394.16 3.99 o 7 3 0 140.12 133.58 1.04 o 7 3 1 1105.78 1089.16 2.60 o 7 3 2 239.25 243.04 1.73 o 7 3 3 227.10 219.90 1.73 o 7 3 4 608.33 575.48 5.36 o 7 3 5 49.03 47.45 1.73 o 7 5 -7 214.99 217.82 3.28 o 7 5 -6 0.71 0.86 0.17 o 7 5 -5 475.12 470.46 2.76 o 7 5 -4 23.08 22.95 0.69 o 7 5 -3 697.14 691.28 3.63 o 7 5 -2 746.45 736.70 3.11 o 7 5 -1 48.89 49.17 0.69 o 7 5 0 1893.70 1895.13 3.47 o 7 5 1 158.95 164.12 1.21 o 7 5 2 489.80 487.07 2.42 o 7 5 3 498.21 502.10 2.94 o 7 5 4 147.77 159.98 3.11 o 7 7 -6 161.81 136.68 1.90 o 7 7 -5 33.95 41.92 1.04 o 7 7 -4 177.75 171.55 2.24 o 7 7 -3 56.68 53.83 1.04 o 7 7 -2 114.76 107.50 1.38 o 7 7 -1 557.11 549.53 2.94 o 7 7 0 136.26 136.50 1.38 o 7 7 1 421.67 434.31 2.24 o 7 7 2 217.83 218.00 1.73 o 7 7 3 64.13 70.74 1.55 o 7 7 4 51.72 51.59 1.73 o 7 9 -5 4.48 1.90 0.35 o 7 9 -4 96.25 111.47 1.90 o 7 9 -3 14.68 13.63 0.69 o 7 9 -2 4.44 4.31 0.35 o 7 9 -1 340.34 348.41 3.11 o 7 9 0 62.42 64.01 1.21 o 7 9 1 82.80 82.48 1.04 o 7 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1.73 o 8 4 -1 0.23 0.35 0.17 < 8 4 0 10.02 10.35 0.35 o 8 4 1 29.15 29.85 0.52 o 8 4 2 212.15 203.15 1.90 o 8 4 3 279.85 275.51 3.45 o 8 4 4 0.01 0.17 0.17 < 8 6 -6 4.13 6.21 0.52 o 8 6 -5 11.24 7.42 0.52 o 8 6 -4 577.54 623.29 4.32 o 8 6 -3 0.62 1.04 0.17 o 8 6 -2 269.16 264.81 2.59 o 8 6 -1 5.29 7.76 0.35 o 8 6 0 205.98 212.64 1.38 o 8 6 1 536.71 554.31 2.76 o 8 6 2 9.07 9.14 0.52 o 8 6 3 296.65 291.07 3.97 o 8 8 -5 272.23 266.54 3.11 o 8 8 -4 1.17 1.38 0.35 o 8 8 -3 438.36 481.82 3.97 o 8 8 -2 82.10 91.45 1.38 o 8 8 -1 508.37 491.74 3.97 o 8 8 0 284.73 276.73 1.73 o 8 8 1 69.09 72.64 1.55 o 8 8 2 650.40 638.96 4.15 o 8 8 3 32.11 28.29 1.21 o 8 10 -4 196.56 185.02 2.59 o 8 10 -3 0.79 0.86 0.17 o 8 10 -2 307.57 311.44 3.11 o 8 10 -1 150.05 156.70 2.42 o 8 10 0 137.51 124.94 1.73 o 8 10 1 179.62 179.49 2.07 o 9 1 -6 97.81 97.15 1.90 o 9 1 -5 28.35 32.95 1.04 o 9 1 -4 43.56 50.03 1.21 o 9 1 -3 186.50 191.23 1.73 o 9 1 -2 80.93 77.99 1.21 o 9 1 -1 697.29 674.48 2.25 o 9 1 0 71.36 63.32 0.69 o 9 1 1 120.25 115.96 1.04 o 9 1 2 53.24 51.07 0.86 o 9 1 3 23.36 20.18 0.86 o 9 3 -6 4.05 5.18 0.69 o 9 3 -5 178.69 170.86 3.45 o 9 3 -4 15.62 19.67 1.21 o 9 3 -3 90.06 104.05 1.21 o 9 3 -2 1285.13 1315.06 4.33 o 9 3 -1 12.27 13.46 0.35 o 9 3 0 546.33 547.42 2.07 o 9 3 1 132.13 141.50 1.55 o 9 3 2 381.53 383.85 3.97 o 9 3 3 281.15 272.76 3.63 o 9 5 -6 148.99 156.87 2.42 o 9 5 -5 3.28 3.11 0.52 o 9 5 -4 239.05 241.83 2.93 o 9 5 -3 320.67 328.37 1.73 o 9 5 -2 1.57 2.42 0.35 o 9 5 -1 964.35 984.41 4.15 o 9 5 0 49.57 53.14 0.86 o 9 5 1 398.89 400.27 2.07 o 9 5 2 208.62 206.95 2.59 o 9 5 3 118.00 123.90 2.76 o 9 7 -5 156.93 153.42 2.42 o 9 7 -4 13.33 8.28 0.69 o 9 7 -3 1.38 0.35 0.17 < 9 7 -2 226.43 219.04 2.59 o 9 7 -1 24.09 19.67 0.86 o 9 7 0 370.53 360.70 3.45 o 9 7 1 37.49 36.92 0.86 o 9 7 2 21.17 23.46 1.21 o 9 9 -4 7.52 6.56 0.69 o 9 9 -3 0.64 3.28 0.35 o 9 9 -2 167.53 173.62 3.45 o 9 9 -1 78.47 73.68 1.73 o 9 9 0 45.33 43.48 1.04 o 9 9 1 2.11 3.11 0.35 o 10 0 -6 15.69 23.98 1.55 o 10 0 -5 329.35 338.57 5.18 o 10 0 -4 3.23 1.73 0.52 o 10 0 -3 203.09 208.49 2.07 o 10 0 -2 117.16 128.38 1.90 o 10 0 -1 325.39 331.48 2.59 o 10 0 0 658.05 641.90 3.63 o 10 0 1 12.21 13.46 0.86 o 10 0 2 611.89 611.09 5.36 o 10 2 -5 1.70 2.42 0.69 o 10 2 -4 192.46 189.68 3.62 o 10 2 -3 6.99 7.94 0.35 o 10 2 -2 210.85 218.16 1.90 o 10 2 -1 159.90 159.46 1.38 o 10 2 0 4.96 4.83 0.35 o 10 2 1 601.72 603.29 3.46 o 10 2 2 3.03 2.24 0.35 o 10 4 -5 41.64 40.54 1.21 o 10 4 -4 24.86 20.53 1.21 o 10 4 -3 82.50 72.99 1.55 o 10 4 -2 11.83 16.56 0.69 o 10 4 -1 3.10 3.97 0.17 o 10 4 0 71.02 77.30 1.73 o 10 4 1 90.53 89.38 1.55 o 10 4 2 169.38 165.51 2.42 o 10 6 -4 6.09 6.73 0.69 o 10 6 -3 90.26 88.00 1.73 o 10 6 -2 14.26 19.15 0.86 o 10 6 -1 116.34 120.45 2.07 o 10 6 0 209.96 203.84 2.76 o 10 6 1 32.77 34.68 1.04 o 10 8 -3 31.24 30.19 1.04 o 10 8 -2 212.51 215.23 2.76 o 10 8 -1 86.78 85.76 1.73 o 10 8 0 30.19 34.16 1.21 o 11 1 -5 84.19 97.49 2.07 o 11 1 -4 21.94 24.84 1.04 o 11 1 -3 17.31 23.29 1.04 o 11 1 -2 129.51 129.42 2.42 o 11 1 -1 2.15 1.38 0.35 o 11 1 0 62.38 68.15 1.21 o 11 1 1 23.71 21.91 0.69 o 11 3 -4 71.54 76.44 2.42 o 11 3 -3 236.63 220.77 4.14 o 11 3 -2 4.40 3.28 0.35 o 11 3 -1 240.70 264.27 3.28 o 11 3 0 119.23 126.14 1.73 o 11 3 1 148.06 144.96 1.90 o 11 5 -4 64.32 65.22 2.24 o 11 5 -3 1.26 2.59 0.52 o 11 5 -2 331.72 331.32 3.45 o 11 5 -1 30.28 32.26 1.21 o 11 5 0 170.47 178.11 2.07 o 12 0 -2 160.01 152.04 3.80 o 12 0 -1 119.22 126.32 2.59 o 12 2 -2 9.41 11.56 0.69 o #------------------------------------------------------------------------------- # STOE DATA #------------------------------------------------------------------------------- #_STOE_detector_size_x '8.0 cm' #_STOE_detector_size_y '7.7 cm' #_STOE_detector_pixelsize_x '0.075 mm' #_STOE_detector_pixelsize_y '0.075 mm' #_STOE_detector_distance '80.0 mm' #_STOE_measurement_tube_power '49.8 W' #_STOE_measurement_total_run_number 21 #_STOE_measurement_total_frame_number 1492 #_STOE_measurement_min_exposure_per_frame '40.0 s' #_STOE_measurement_max_exposure_per_frame '40.0 s' #_STOE_measurement_mean_exposure_per_frame '40.0 s' #_STOE_measurement_total_exposure_time '16.6 h' #_STOE_evaluation_integration_A 15.1 #_STOE_evaluation_integration_B -1.0 #_STOE_evaluation_integration_EMS 0.037 #_STOE_evaluation_LANA_point_group '2/m' #_STOE_evaluation_LANA_FS_max_order 3 #_STOE_evaluation_LANA_DXS_max_order - #_STOE_evaluation_LANA_DYS_max_order - #_STOE_evaluation_LANA_BIS_l_even_max 4 #_STOE_evaluation_LANA_BIS_l_odd_max 1 #_STOE_evaluation_LANA_BOS_l_even_max 4 #_STOE_evaluation_LANA_BOS_l_odd_max 1 #_STOE_evaluation_LANA_OR_c1 0.035 #_STOE_evaluation_LANA_OR_c2 0 #_STOE_evaluation_LANA_OR_c3 0 #_STOE_evaluation_LANA_OR_c4 0.7 #_STOE_evaluation_LANA_max_2theta_available 81.4 #_STOE_evaluation_LANA_max_2theta_desired 81.4 #_STOE_evaluation_LANA_number_refls_total 3712 #_STOE_evaluation_LANA_number_refls_outliers 586 #_STOE_evaluation_LANA_number_refls_after_OR 3126 #_STOE_evaluation_LANA_number_refls_unique 816 #_STOE_evaluation_LANA_number_refls_written 3126 #_STOE_evaluation_LANA_completeness 98.4 #_STOE_evaluation_LANA_mean_redundancy 3.8 #_STOE_evaluation_LANA_table #; #---------------------------------------------------------------------------- #2Theta 11.0 19.4 27.8 36.2 44.6 53.0 61.4 69.8 78.2 #---------------------------------------------------------------------------- #<Resolution> 3.43 2.04 1.45 1.13 0.93 0.80 0.70 0.62 0.57 #N(total) 13 53 142 470 617 586 660 667 504 #<Redundancy> 1.6 2.7 3.3 6.2 5.8 4.3 3.9 3.3 2.5 #Complet. [%%] 100.0 94.7 90.5 100.0 100.0 99.1 99.3 99.4 97.2 #<I/sigma> 782.4 457.3 371.8 170.1 125.3 90.6 51.4 35.5 18.3 #R(int) 0.021 0.009 0.010 0.011 0.014 0.013 0.015 0.018 0.044 #---------------------------------------------------------------------------- #; #======================================================================= data_beta_split #======================================================================= # 5. CHEMICAL DATA _chemical_name_systematic ? _chemical_name_common ? _chemical_formula_moiety ? _chemical_formula_structural ? _chemical_formula_analytical ? _chemical_formula_iupac ? _chemical_formula_sum 'Fe2 O7 P2' _chemical_formula_weight 285.6 _chemical_melting_point ? _chemical_compound_source ? _chemical_absolute_configuration . #======================================================================= # 6. CRYSTAL DATA _space_group_crystal_system monoclinic _space_group_name_H-M_alt 'C 1 2/m 1' _space_group_name_Hall '-C 2y' _space_group_IT_number 12 loop_ _space_group_symop_id _space_group_symop_operation_xyz 1 x,y,z 2 -x,y,-z 3 -x,-y,-z 4 x,-y,z 5 x+1/2,y+1/2,z 6 -x+1/2,y+1/2,-z 7 -x+1/2,-y+1/2,-z 8 x+1/2,-y+1/2,z _cell_length_a 6.6154(6) _cell_length_b 8.4624(10) _cell_length_c 4.4920(4) _cell_angle_alpha 90 _cell_angle_beta 103.502(7) _cell_angle_gamma 90 _cell_volume 244.52(4) loop_ _twin_individual_id _twin_individual_mass_fraction_refined _twin_individual_twin_matrix_11 _twin_individual_twin_matrix_12 _twin_individual_twin_matrix_13 _twin_individual_twin_matrix_21 _twin_individual_twin_matrix_22 _twin_individual_twin_matrix_23 _twin_individual_twin_matrix_31 _twin_individual_twin_matrix_32 _twin_individual_twin_matrix_33 ? ? ? ? ? ? ? ? ? ? ? _cell_formula_units_Z 2 _cell_measurement_temperature 470 _cell_measurement_reflns_used 6240 _cell_measurement_theta_min 3.98 _cell_measurement_theta_max 40.76 _cell_special_details ? _exptl_crystal_density_diffrn 3.8795 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_F_000 276 _exptl_crystal_type_of_structure cryst _exptl_absorpt_coefficient_mu 6.566 _exptl_crystal_description 'fragment' _exptl_crystal_colour 'light-brownish' _exptl_crystal_size_max 0.110 _exptl_crystal_size_mid 0.070 _exptl_crystal_size_min 0.040 _exptl_crystal_size_rad 0.030 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; STOE LANA, absorption correction by scaling of reflection intensities. J. Koziskova, F. Hahn, J. Richter, J. Kozisek, "Comparison of different absorption corrections on the model structure of tetrakis(\m~2~-acetato)- diaqua-di-copper(II)", Acta Chimica Slovaca, vol. 9, no. 2, 2016, pp. 136 - 140. Afterwards a spherical absorption correction was performed within STOE LANA. ; _exptl_absorpt_correction_T_min 0.4724 _exptl_absorpt_correction_T_max 0.5578 #======================================================================= # 7. EXPERIMENTAL DATA _diffrn_measurement_device 'Eulerian 4-circle diffractometer' _diffrn_measurement_device_type 'STOE STADIVARI' _diffrn_detector 'EIGER2 1M CDTE' _diffrn_detector_type ? _diffrn_detector_area_resol_mean 13.33 _diffrn_source 'Axo_Mo' _diffrn_source_type ? _diffrn_radiation_probe x-ray _diffrn_source_target ? _diffrn_source_voltage 60 _diffrn_source_current 0.830 _diffrn_source_power 0.050 _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_monochromator 'Graded multilayer mirror' _diffrn_radiation_polarisn_norm -90 _diffrn_radiation_collimation '1.2 0.6 mm diameter' _diffrn_ambient_temperature 470 _diffrn_measurement_method 'rotation method, \w scans' _diffrn_measurement_details ; 1492 frames, detector distance = 80 mm ; _diffrn_reflns_number 3414 _diffrn_reflns_theta_min 3.98 _diffrn_reflns_theta_max 40.82 _diffrn_reflns_theta_full 40.82 _diffrn_measured_fraction_theta_max 0.99 _diffrn_measured_fraction_theta_full 0.99 _diffrn_reflns_av_R_equivalents 0.0119 _diffrn_reflns_av_unetI/netI 0.0032 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_l_min -8 _diffrn_reflns_limit_l_max 3 _diffrn_reflns_reduction_process ? _diffrn_standards_number ? _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% ? loop_ _diffrn_standard_refln_index_h _diffrn_standard_refln_index_k _diffrn_standard_refln_index_l ? ? ? #_diffrn_reflns_av_sigmaI/netI 0.0032 #======================================================================= # 8. REFINEMENT DATA _refine_special_details ? _reflns_number_total 826 _reflns_number_gt 815 _reflns_threshold_expression 'I>3\s(I)' _refine_ls_structure_factor_coef Fsqd _refine_ls_R_factor_gt 0.0188 _refine_ls_wR_factor_gt 0.0792 _refine_ls_R_factor_all 0.0189 _refine_ls_wR_factor_ref 0.0800 _refine_ls_goodness_of_fit_ref 1.8208 _refine_ls_goodness_of_fit_gt 1.8170 _refine_ls_restrained_S_gt ? _refine_ls_restrained_S_all ? _refine_ls_number_reflns 826 _refine_ls_number_parameters 33 _refine_ls_number_restraints 0 _refine_ls_number_constraints 0 _refine_ls_weighting_scheme sigma _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.04P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_hydrogen_treatment ? _refine_ls_shift/su_max 0.0102 _refine_ls_shift/su_mean 0.0019 _refine_diff_density_max 0.58 _refine_diff_density_min -0.68 _refine_ls_extinction_method 'B-C type 1 Gaussian isotropic (Becker & Coppens, 1974)' _refine_ls_extinction_coef 320(90) _refine_ls_extinction_expression ? _refine_ls_abs_structure_details ? _refine_ls_abs_structure_Flack ? _refine_ls_abs_structure_Rogers ? loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Fe 0.3463 0.8444 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' O 0.0106 0.0060 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' P 0.1023 0.0942 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' _computing_data_collection ; X-Area Pilatus3_SV 1.31.194.0 (STOE, 2023) ; _computing_cell_refinement ; X-Area Recipe 2.0.2 (STOE, 2024) ; _computing_data_reduction ; X-Area Integrate 2.5.18.0 (STOE, 2024) X-Area LANA 2.8.4 (STOE, 2024) ; _computing_publication_material ; STOE & Cie GmbH, X-Area, software package for collecting single-crystal or multi-domain crystal data on STOE area-detector diffractometers, for image processing, for the correction and scaling of reflection intensities and for outlier rejection, version 2.4, Darmstadt 2024 ; #======================================================================= # 9. ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_adp_type _atom_site_U_iso_or_equiv _atom_site_site_symmetry_multiplicity _atom_site_occupancy _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_disorder_assembly _atom_site_disorder_group Fe1 Fe 0.5 0.190938(17) 0.5 Uani 0.01500(7) 4 1 d . . . P1 P 0.21350(4) 0 -0.09111(6) Uani 0.00970(9) 4 1 d . . . O1 O 0.37350(13) 0 0.21293(18) Uani 0.01317(18) 4 1 d . . . O2 O 0.22246(12) 0.14872(8) -0.27746(16) Uani 0.01839(17) 8 1 d . . . O3 O 0 0.0268(5) 0 Uani 0.0338(13) 4 0.5 d . . . loop_ _atom_site_aniso_label _atom_site_aniso_type_symbol _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Fe1 Fe 0.01565(12) 0.00994(12) 0.01656(13) 0 -0.00198(8) 0 P1 P 0.00869(14) 0.01253(15) 0.00775(14) 0 0.00166(9) 0 O1 O 0.0140(3) 0.0151(3) 0.0088(3) 0 -0.0006(2) 0 O2 O 0.0261(3) 0.0132(3) 0.0146(3) 0.0051(2) 0.0023(2) 0.00333(18) O3 O 0.0112(5) 0.053(4) 0.0413(11) 0 0.0139(7) 0 #======================================================================= # 10. MOLECULAR GEOMETRY loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_1 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Fe1 O1 . . 2.1142(6) ? Fe1 O1 . 2_656 2.1142(6) ? Fe1 O2 . 1_556 2.3141(9) ? Fe1 O2 . 2_655 2.3141(9) ? Fe1 O2 . 7_555 2.0782(8) ? Fe1 O2 . 8_556 2.0782(8) ? P1 O1 . . 1.5201(8) ? P1 O2 . . 1.5203(8) ? P1 O2 . 4_555 1.5203(8) ? P1 O3 . . 1.5759(7) ? P1 O3 . 3_555 1.5759(7) ? O3 O3 . 3_555 0.453(6) ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_2 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag O1 Fe1 O1 . . 2_656 80.32(2) ? O1 Fe1 O2 . . 1_556 84.52(3) ? O1 Fe1 O2 . . 2_655 81.92(3) ? O1 Fe1 O2 . . 7_555 94.05(3) ? O1 Fe1 O2 . . 8_556 158.02(3) ? O1 Fe1 O2 2_656 . 1_556 81.92(3) ? O1 Fe1 O2 2_656 . 2_655 84.52(3) ? O1 Fe1 O2 2_656 . 7_555 158.02(3) ? O1 Fe1 O2 2_656 . 8_556 94.05(3) ? O2 Fe1 O2 1_556 . 2_655 162.24(3) ? O2 Fe1 O2 1_556 . 7_555 76.37(3) ? O2 Fe1 O2 1_556 . 8_556 115.92(3) ? O2 Fe1 O2 2_655 . 7_555 115.92(3) ? O2 Fe1 O2 2_655 . 8_556 76.37(3) ? O2 Fe1 O2 7_555 . 8_556 98.48(3) ? O1 P1 O2 . . . 112.72(3) ? O1 P1 O2 . . 4_555 112.72(3) ? O1 P1 O3 . . . 104.18(4) ? O1 P1 O3 . . 3_555 104.18(4) ? O2 P1 O2 . . 4_555 111.75(4) ? O2 P1 O3 . . . 100.16(15) ? O2 P1 O3 . . 3_555 114.49(14) ? O2 P1 O3 4_555 . . 114.49(14) ? O2 P1 O3 4_555 . 3_555 100.16(15) ? O3 P1 O3 . . 3_555 16.5(2) ? Fe1 O1 Fe1 . . 3_656 99.68(3) ? Fe1 O1 P1 . . . 129.898(17) ? Fe1 O1 P1 3_656 . . 129.898(17) ? Fe1 O2 Fe1 1_554 . 7_555 103.63(3) ? Fe1 O2 P1 1_554 . . 120.17(4) ? Fe1 O2 P1 7_555 . . 133.71(5) ? P1 O3 P1 . . 2_555 163.5(3) ? P1 O3 O3 . . 3_555 81.73(16) ? P1 O3 O3 2_555 . 3_555 81.73(16) ? #======================================================================= # 11. STRUCTURE-FACTOR LIST loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_include_status 0 0 1 1550.06 1461.13 2.48 o 0 0 2 1824.54 1630.61 3.85 o 0 0 4 1833.22 1835.40 3.48 o 0 0 5 2305.12 2325.98 6.09 o 0 0 6 2.40 2.59 0.52 o 0 0 7 381.84 434.06 4.33 o 0 2 0 36.99 44.64 0.35 o 0 2 1 13853.20 14411.80 7.12 o 0 2 2 1202.30 1231.89 1.92 o 0 2 3 732.39 761.53 1.73 o 0 2 4 1605.74 1613.25 2.61 o 0 2 5 101.82 103.95 1.04 o 0 2 6 746.05 775.53 2.94 o 0 2 7 7.47 8.65 0.52 o 0 4 0 1339.94 1334.17 2.44 o 0 4 1 1428.99 1522.51 2.09 o 0 4 2 902.02 1022.61 2.61 o 0 4 3 395.20 377.17 0.87 o 0 4 4 201.67 205.55 1.21 o 0 4 5 46.75 46.00 0.69 o 0 4 6 87.21 96.33 1.04 o 0 4 7 250.59 256.24 2.94 o 0 6 0 9153.56 9492.51 6.84 o 0 6 1 56.33 49.98 0.52 o 0 6 2 319.49 361.30 1.21 o 0 6 3 612.13 617.10 1.39 o 0 6 4 268.65 276.35 1.56 o 0 6 5 777.44 808.35 4.33 o 0 6 6 29.45 29.22 0.52 o 0 6 7 165.58 181.29 2.25 o 0 8 0 27.86 27.84 0.52 o 0 8 1 3444.97 3617.76 3.32 o 0 8 2 1344.68 1360.31 2.26 o 0 8 3 684.00 714.06 1.91 o 0 8 4 822.29 837.04 3.29 o 0 8 5 55.37 54.65 0.86 o 0 8 6 591.02 587.87 3.81 o 0 10 0 1402.72 1477.14 3.82 o 0 10 1 76.00 77.14 0.86 o 0 10 2 1181.83 1236.03 2.77 o 0 10 3 834.76 850.72 2.77 o 0 10 4 28.48 24.56 0.69 o 0 10 5 228.76 233.39 2.60 o 0 10 6 22.40 20.92 0.86 o 0 12 0 133.78 135.09 1.56 o 0 12 1 279.80 305.40 2.94 o 0 12 2 33.64 33.89 0.69 o 0 12 3 1.44 1.56 0.35 o 0 12 4 43.75 40.47 1.04 o 0 12 5 2.63 3.29 0.52 o 0 14 0 63.90 71.08 2.25 o 0 14 1 219.64 215.39 2.77 o 0 14 2 130.04 130.94 1.56 o 0 14 3 45.81 43.58 1.21 o 1 1 -8 1.31 1.73 0.35 o 1 1 -7 300.05 317.52 2.25 o 1 1 -6 8.42 8.99 0.52 o 1 1 -5 37.68 33.38 0.52 o 1 1 -4 2255.60 2156.29 2.27 o 1 1 -3 44.45 54.31 1.04 o 1 1 -2 607.23 535.24 1.39 o 1 1 -1 132.65 127.48 0.69 o 1 1 0 515.48 511.22 1.57 o 1 1 1 6400.12 6461.00 3.13 o 1 1 2 151.88 159.23 0.69 o 1 1 3 2636.02 2661.64 2.45 o 1 1 4 117.13 113.13 0.69 o 1 1 5 81.51 88.55 0.86 o 1 1 6 432.05 445.54 2.94 o 1 1 7 6.51 7.09 0.52 o 1 3 -8 353.71 360.66 5.36 o 1 3 -7 22.47 28.01 0.86 o 1 3 -6 271.85 292.94 2.08 o 1 3 -5 659.37 679.88 2.08 o 1 3 -4 145.05 145.49 0.69 o 1 3 -3 7895.62 7558.33 10.18 o 1 3 -2 2115.52 2273.63 3.85 o 1 3 -1 561.31 438.68 1.22 o 1 3 0 4542.97 4610.43 4.67 o 1 3 1 6778.99 7474.19 6.34 o 1 3 2 11617.90 11752.20 6.78 o 1 3 3 120.37 121.96 0.69 o 1 3 4 1393.48 1453.88 2.60 o 1 3 5 963.01 1010.91 2.60 o 1 3 6 185.12 193.06 2.25 o 1 3 7 301.70 303.17 4.15 o 1 5 -7 440.45 443.13 3.29 o 1 5 -6 145.40 150.83 1.38 o 1 5 -5 154.95 153.09 1.21 o 1 5 -4 2834.95 2848.87 4.01 o 1 5 -3 236.89 233.63 0.87 o 1 5 -2 3491.96 3462.16 3.51 o 1 5 -1 3484.82 3745.28 4.22 o 1 5 0 3627.85 3618.72 6.87 o 1 5 1 4821.85 4894.78 6.37 o 1 5 2 215.63 230.70 1.04 o 1 5 3 4863.49 5017.59 4.74 o 1 5 4 283.57 291.42 1.38 o 1 5 5 362.04 378.67 2.94 o 1 5 6 574.88 586.97 2.77 o 1 5 7 27.26 26.98 1.38 o 1 7 -7 17.56 18.50 0.86 o 1 7 -6 267.61 255.38 1.90 o 1 7 -5 600.59 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3.11 o 5 11 -3 19.44 21.62 0.69 o 5 11 -2 229.52 239.62 1.90 o 5 11 -1 504.40 506.55 3.81 o 5 11 0 58.68 54.48 1.21 o 5 11 1 772.34 773.81 3.64 o 5 11 2 21.55 19.71 0.86 o 5 11 3 141.75 136.13 2.25 o 5 13 -3 162.54 155.51 2.42 o 5 13 -2 102.12 100.66 1.38 o 5 13 -1 264.10 278.74 2.94 o 5 13 0 774.63 796.36 5.20 o 5 13 1 12.45 11.59 0.52 o 5 13 2 242.30 261.08 3.11 o 6 0 -7 0.66 0.69 0.17 o 6 0 -6 868.48 876.57 3.81 o 6 0 -5 261.20 247.26 2.08 o 6 0 -4 3.70 3.46 0.17 o 6 0 -3 2143.75 2095.90 3.65 o 6 0 -2 796.11 715.67 2.43 o 6 0 -1 2801.88 2794.54 4.89 o 6 0 0 1015.97 1036.83 2.60 o 6 0 1 425.23 424.71 1.56 o 6 0 2 2382.08 2387.01 5.22 o 6 0 3 135.32 127.48 1.21 o 6 0 4 1553.41 1497.22 6.94 o 6 0 5 68.82 61.22 2.59 o 6 0 6 57.83 50.33 2.59 o 6 2 -7 276.82 278.40 2.60 o 6 2 -6 0.62 0.69 0.17 o 6 2 -5 224.39 220.42 1.90 o 6 2 -4 748.96 717.65 2.08 o 6 2 -3 10.01 13.49 0.35 o 6 2 -2 1902.14 1888.21 3.13 o 6 2 -1 596.39 579.02 1.73 o 6 2 0 655.17 669.72 1.91 o 6 2 1 732.99 742.90 2.60 o 6 2 2 76.59 72.12 0.69 o 6 2 3 1846.11 1826.15 4.00 o 6 2 4 2.97 3.29 0.35 o 6 2 5 224.83 220.93 3.46 o 6 4 -7 76.15 91.32 1.21 o 6 4 -6 41.96 36.83 0.52 o 6 4 -5 1.58 2.07 0.35 o 6 4 -4 24.89 27.67 0.69 o 6 4 -3 741.92 706.94 2.77 o 6 4 -2 388.31 397.99 2.08 o 6 4 -1 2.89 3.11 0.17 o 6 4 0 29.94 29.05 0.52 o 6 4 1 51.49 51.36 0.52 o 6 4 2 218.62 222.32 1.21 o 6 4 3 548.72 543.33 3.12 o 6 4 4 238.50 231.84 2.25 o 6 4 5 1.46 1.04 0.52 < 6 6 -7 5.94 2.94 0.35 o 6 6 -6 333.97 353.20 2.77 o 6 6 -5 68.90 71.60 0.86 o 6 6 -4 32.52 30.44 0.52 o 6 6 -3 872.59 912.77 2.77 o 6 6 -2 45.02 44.96 0.69 o 6 6 -1 826.56 828.90 2.43 o 6 6 0 122.25 125.23 1.04 o 6 6 1 74.74 74.37 0.69 o 6 6 2 769.94 751.69 2.43 o 6 6 3 2.46 2.42 0.17 o 6 6 4 564.28 570.34 5.37 o 6 6 5 7.00 5.53 0.69 o 6 8 -6 2.15 3.11 0.35 o 6 8 -5 149.67 160.87 1.73 o 6 8 -4 731.37 737.72 2.94 o 6 8 -3 20.02 18.50 0.52 o 6 8 -2 1033.41 1032.83 4.68 o 6 8 -1 201.23 211.41 2.08 o 6 8 0 686.48 688.15 4.50 o 6 8 1 724.96 714.52 3.12 o 6 8 2 177.36 179.73 1.73 o 6 8 3 892.93 859.63 3.29 o 6 8 4 14.24 13.66 0.86 o 6 10 -5 61.46 54.13 1.21 o 6 10 -4 54.37 52.75 1.38 o 6 10 -3 793.76 770.91 3.98 o 6 10 -2 1.73 1.56 0.17 o 6 10 -1 270.41 274.42 2.08 o 6 10 0 304.68 306.45 2.94 o 6 10 1 422.13 430.29 3.63 o 6 10 2 408.59 426.99 3.63 o 6 10 3 5.36 4.32 0.52 o 6 12 -4 95.70 85.96 1.73 o 6 12 -3 39.78 44.10 1.04 o 6 12 -2 95.36 89.42 1.38 o 6 12 -1 0.15 0.17 0.17 < 6 12 0 52.92 51.71 1.38 o 6 12 1 23.39 26.63 0.86 o 6 12 2 6.16 7.44 0.52 o 7 1 -7 99.39 98.59 1.73 o 7 1 -6 63.28 57.59 0.86 o 7 1 -5 433.30 440.53 2.08 o 7 1 -4 23.80 25.42 0.69 o 7 1 -3 236.12 229.09 1.73 o 7 1 -2 85.15 82.85 1.04 o 7 1 -1 38.46 37.70 0.52 o 7 1 0 1471.60 1447.58 2.60 o 7 1 1 1.29 1.56 0.17 o 7 1 2 23.25 21.79 0.52 o 7 1 3 119.96 115.71 1.21 o 7 1 4 20.11 19.89 0.69 o 7 1 5 218.44 188.75 3.29 o 7 3 -7 26.64 25.59 0.69 o 7 3 -6 372.48 391.30 2.08 o 7 3 -5 38.23 43.06 1.04 o 7 3 -4 1012.82 1003.69 4.33 o 7 3 -3 26.48 22.48 0.52 o 7 3 -2 174.84 173.00 1.38 o 7 3 -1 2386.00 2399.23 4.00 o 7 3 0 141.31 133.89 1.04 o 7 3 1 1104.83 1091.61 2.60 o 7 3 2 240.04 243.61 1.73 o 7 3 3 227.58 220.41 1.73 o 7 3 4 610.79 576.81 5.37 o 7 3 5 49.01 47.56 1.73 o 7 5 -7 216.25 218.33 3.29 o 7 5 -6 0.70 0.86 0.17 o 7 5 -5 477.23 471.55 2.77 o 7 5 -4 22.94 23.00 0.69 o 7 5 -3 701.55 692.87 3.64 o 7 5 -2 744.84 738.37 3.12 o 7 5 -1 49.55 49.29 0.69 o 7 5 0 1892.55 1899.26 3.47 o 7 5 1 160.61 164.51 1.21 o 7 5 2 489.96 488.19 2.42 o 7 5 3 499.64 503.26 2.94 o 7 5 4 147.77 160.35 3.11 o 7 7 -6 161.89 137.00 1.90 o 7 7 -5 33.54 42.02 1.04 o 7 7 -4 177.30 171.95 2.25 o 7 7 -3 57.54 53.96 1.04 o 7 7 -2 113.97 107.76 1.38 o 7 7 -1 560.34 550.79 2.94 o 7 7 0 137.62 136.82 1.38 o 7 7 1 424.45 435.32 2.25 o 7 7 2 218.16 218.50 1.73 o 7 7 3 64.54 70.91 1.56 o 7 7 4 51.46 51.71 1.73 o 7 9 -5 4.14 1.90 0.35 o 7 9 -4 94.30 111.73 1.90 o 7 9 -3 13.66 13.66 0.69 o 7 9 -2 5.14 4.32 0.35 o 7 9 -1 346.60 349.23 3.12 o 7 9 0 64.77 64.16 1.21 o 7 9 1 84.94 82.67 1.04 o 7 9 2 0.11 0.17 0.17 < 7 9 3 5.18 3.98 0.69 o 7 11 -4 4.68 8.13 0.69 o 7 11 -3 217.30 229.75 2.77 o 7 11 -2 283.36 279.27 2.94 o 7 11 -1 2.81 3.29 0.35 o 7 11 0 407.97 417.30 3.81 o 7 11 1 37.89 35.97 1.04 o 7 11 2 212.55 211.58 2.42 o 8 0 -7 196.30 189.78 2.77 o 8 0 -6 35.41 31.30 1.04 o 8 0 -5 3.87 2.77 0.35 o 8 0 -4 1488.91 1532.51 8.68 o 8 0 -3 46.84 41.50 0.86 o 8 0 -2 977.10 914.77 3.29 o 8 0 -1 65.28 65.89 0.86 o 8 0 0 820.06 835.88 2.95 o 8 0 1 1454.55 1427.66 5.03 o 8 0 2 34.43 33.89 1.04 o 8 0 3 742.03 743.45 4.68 o 8 0 4 117.80 106.72 2.25 o 8 2 -7 2.47 3.46 0.35 o 8 2 -6 31.42 30.09 1.21 o 8 2 -5 376.46 381.44 2.42 o 8 2 -4 29.17 29.40 0.86 o 8 2 -3 986.71 957.17 3.12 o 8 2 -2 7.96 7.61 0.35 o 8 2 -1 588.50 580.31 1.90 o 8 2 0 242.62 245.34 1.21 o 8 2 1 101.79 102.56 1.04 o 8 2 2 981.70 990.86 3.99 o 8 2 3 1.89 2.08 0.17 o 8 2 4 204.48 190.82 2.60 o 8 4 -6 10.72 11.41 0.69 o 8 4 -5 49.43 64.50 1.21 o 8 4 -4 198.78 177.84 2.42 o 8 4 -3 277.95 277.20 2.08 o 8 4 -2 204.92 204.32 1.73 o 8 4 -1 0.29 0.35 0.17 < 8 4 0 10.27 10.38 0.35 o 8 4 1 28.88 29.92 0.52 o 8 4 2 211.84 203.62 1.90 o 8 4 3 280.68 276.16 3.46 o 8 4 4 0.01 0.17 0.17 < 8 6 -6 4.23 6.23 0.52 o 8 6 -5 11.31 7.44 0.52 o 8 6 -4 578.91 624.73 4.33 o 8 6 -3 0.62 1.04 0.17 o 8 6 -2 270.11 265.42 2.60 o 8 6 -1 5.29 7.78 0.35 o 8 6 0 206.54 213.14 1.38 o 8 6 1 537.95 555.59 2.77 o 8 6 2 9.13 9.16 0.52 o 8 6 3 297.40 291.74 3.98 o 8 8 -5 271.30 267.15 3.11 o 8 8 -4 1.12 1.38 0.35 o 8 8 -3 435.81 482.93 3.98 o 8 8 -2 84.54 91.66 1.38 o 8 8 -1 505.47 492.88 3.98 o 8 8 0 287.73 277.37 1.73 o 8 8 1 68.00 72.81 1.56 o 8 8 2 655.72 640.44 4.16 o 8 8 3 31.94 28.36 1.21 o 8 10 -4 193.88 185.45 2.59 o 8 10 -3 0.76 0.86 0.17 o 8 10 -2 302.83 312.16 3.11 o 8 10 -1 154.62 157.07 2.42 o 8 10 0 134.76 125.23 1.73 o 8 10 1 182.88 179.91 2.08 o 9 1 -6 98.56 97.37 1.90 o 9 1 -5 28.56 33.03 1.04 o 9 1 -4 44.11 50.15 1.21 o 9 1 -3 186.24 191.68 1.73 o 9 1 -2 80.73 78.17 1.21 o 9 1 -1 696.87 676.02 2.25 o 9 1 0 70.92 63.47 0.69 o 9 1 1 120.08 116.23 1.04 o 9 1 2 53.79 51.19 0.86 o 9 1 3 23.12 20.23 0.86 o 9 3 -6 4.07 5.19 0.69 o 9 3 -5 179.27 171.26 3.46 o 9 3 -4 16.01 19.71 1.21 o 9 3 -3 89.54 104.29 1.21 o 9 3 -2 1289.67 1318.02 4.34 o 9 3 -1 12.46 13.49 0.35 o 9 3 0 548.81 548.68 2.08 o 9 3 1 132.26 141.84 1.56 o 9 3 2 382.89 384.74 3.98 o 9 3 3 282.12 273.39 3.63 o 9 5 -6 149.38 157.24 2.42 o 9 5 -5 3.41 3.11 0.52 o 9 5 -4 238.67 242.39 2.94 o 9 5 -3 322.83 329.14 1.73 o 9 5 -2 1.57 2.42 0.35 o 9 5 -1 969.78 986.66 4.16 o 9 5 0 49.41 53.26 0.86 o 9 5 1 400.51 401.20 2.08 o 9 5 2 208.68 207.43 2.60 o 9 5 3 118.53 124.19 2.77 o 9 7 -5 158.00 153.78 2.42 o 9 7 -4 13.11 8.30 0.69 o 9 7 -3 1.46 0.35 0.17 < 9 7 -2 226.24 219.55 2.60 o 9 7 -1 23.69 19.71 0.86 o 9 7 0 370.27 361.54 3.46 o 9 7 1 37.92 37.01 0.86 o 9 7 2 20.99 23.52 1.21 o 9 9 -4 8.14 6.57 0.69 o 9 9 -3 0.82 3.29 0.35 o 9 9 -2 164.90 174.02 3.46 o 9 9 -1 76.51 73.85 1.73 o 9 9 0 43.98 43.58 1.04 o 9 9 1 2.37 3.11 0.35 o 10 0 -6 15.37 24.04 1.56 o 10 0 -5 331.60 339.35 5.19 o 10 0 -4 3.14 1.73 0.52 o 10 0 -3 205.52 208.98 2.08 o 10 0 -2 116.64 128.68 1.90 o 10 0 -1 327.34 332.25 2.60 o 10 0 0 657.80 643.37 3.64 o 10 0 1 12.01 13.49 0.86 o 10 0 2 612.57 612.49 5.37 o 10 2 -5 1.75 2.42 0.69 o 10 2 -4 193.64 190.12 3.63 o 10 2 -3 7.00 7.95 0.35 o 10 2 -2 211.54 218.67 1.90 o 10 2 -1 160.20 159.83 1.38 o 10 2 0 5.01 4.84 0.35 o 10 2 1 603.12 604.68 3.46 o 10 2 2 3.00 2.25 0.35 o 10 4 -5 41.71 40.64 1.21 o 10 4 -4 24.65 20.58 1.21 o 10 4 -3 81.89 73.16 1.56 o 10 4 -2 11.62 16.60 0.69 o 10 4 -1 3.22 3.98 0.17 o 10 4 0 71.91 77.48 1.73 o 10 4 1 91.11 89.59 1.56 o 10 4 2 170.09 165.89 2.42 o 10 6 -4 6.05 6.74 0.69 o 10 6 -3 90.57 88.21 1.73 o 10 6 -2 14.32 19.19 0.86 o 10 6 -1 116.48 120.73 2.08 o 10 6 0 210.82 204.32 2.77 o 10 6 1 32.91 34.76 1.04 o 10 8 -3 30.55 30.26 1.04 o 10 8 -2 215.32 215.74 2.77 o 10 8 -1 85.65 85.96 1.73 o 10 8 0 31.09 34.24 1.21 o 11 1 -5 83.65 97.72 2.08 o 11 1 -4 22.38 24.90 1.04 o 11 1 -3 17.72 23.34 1.04 o 11 1 -2 131.01 129.73 2.42 o 11 1 -1 2.26 1.38 0.35 o 11 1 0 63.15 68.31 1.21 o 11 1 1 23.48 21.96 0.69 o 11 3 -4 71.66 76.61 2.42 o 11 3 -3 237.36 221.28 4.15 o 11 3 -2 4.33 3.29 0.35 o 11 3 -1 241.37 264.89 3.29 o 11 3 0 119.66 126.44 1.73 o 11 3 1 148.48 145.30 1.90 o 11 5 -4 64.41 65.37 2.25 o 11 5 -3 1.32 2.59 0.52 o 11 5 -2 332.20 332.09 3.46 o 11 5 -1 30.58 32.34 1.21 o 11 5 0 170.59 178.52 2.08 o 12 0 -2 159.07 152.40 3.81 o 12 0 -1 121.05 126.61 2.59 o 12 2 -2 9.64 11.59 0.69 o