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#\#CIF_1.1 ################################################################################ # # # This CIF is a part of the B-IncStrDB # # (Bilbao Incommensurate Structures Database) # # http://www.cryst.ehu.eus/bincstrdb/ # # # # Please note that the structure of the CIF file may differ from the one # # deposited, as it may have been modified to comply with the standard. The # # file has been validated against official dictionaries as well as local # # dictionaries including non-standard data names used by SHELXL (Sheldrick, # # G. M. (2008). Acta Cryst. A 64, 112-122) and JANA (Petricek, V., Dusek, M. # # and Palatinus, L. (2014), Z. Kristallogr. 229, 345-352). # # # # For comments and/or criticisms, please e-mail to administrador-bcs@ehu.es # # # ################################################################################ data_I _audit_creation_method 'Jana2006 Version : 23/03/2015' _journal_date_recd_electronic 2016-12-24 _journal_date_from_coeditor 2017-02-15 _journal_date_accepted 2017-02-15 _journal_date_printers_first 2017-04-24 _journal_date_proofs_out 2017-04-24 _journal_date_proofs_in 2017-05-02 _journal_coeditor_code XK5035 _journal_paper_doi https://doi.org/10.1107/S2052520617002657 _journal_techeditor_code B170265 _iucr_compatibility_tag ACTA95 _journal_paper_category FA _journal_coden_ASTM ASBSDK _journal_coden_Cambridge 1743 _journal_name_full 'Acta Crystallographica, Section B' _journal_year 2017 _journal_volume 73 _journal_issue 03 _journal_page_first 369 _journal_page_last 376 _publ_contact_author_name 'Biagioni,Cristian' _publ_contact_author_address ;Dipartimento di Scienze della Terra Universita di Pisa Via Santa Maria 53 Pisa 56126 Italy ; _publ_contact_author_email biagioni@dst.unipi.it _publ_requested_journal 'Acta Crystallographica Section B' _publ_section_title ;Could incommensurability in sulfosalts be more common than thought? The case of meneghinite, CuPb~13~Sb~7~S~24~ ; loop_ _publ_author_name _publ_author_address 'Bindi, Luca' ;Dipartimento di Scienze della Terra Universita di Pisa Via Santa Maria 53 Pisa 56126 Italy ; 'Petricek, Vaclav' ;Institute of Physics ASCR Na Slovance 2 182 21 Praha 6 Czech Republic ; 'Biagioni, Cristian' ;Dipartimento di Scienze della Terra Universita di Pisa Via Santa Maria 53 Pisa 56126 Italy ; 'Plasil, Jakub' ;Institute of Physics ASCR Na Slovance 2 182 21 Praha 6 Czech Republic ; 'Moelo, Yves' ;Institut des Mat\'eriaux Jean Rouxel UMR 6502 CNRS Universit\'e de Nantes 2 rue de la Houssini\`ere 44322 Nantes CEDEX 3 France ; _publ_section_references ; Petricek, V., Dusek, M. & Palatinus L. (2014). Z. Kristallogr. 229(5), 345-352. Palatinus L. & Chapuis G. (2007). J. Appl. Cryst. 40, 786-790. ; _database_code_depnum_ccdc_archive 1533002 _chemical_formula_sum 'Cu0.966 Pb13.196 S24 Sb6.804' _chemical_formula_weight 4393.3 _chemical_absolute_configuration ? _space_group_crystal_system orthorhombic _space_group_ssg_name Pnma(0\b0)00s loop_ _space_group_symop_ssg_id _space_group_symop_ssg_operation_algebraic 1 x1,x2,x3,x4 2 -x1+1/2,-x2,x3+1/2,-x4+1/2 3 -x1,x2+1/2,-x3,x4+1/2 4 x1+1/2,-x2+1/2,-x3+1/2,-x4 5 -x1,-x2,-x3,-x4 6 x1+1/2,x2,-x3+1/2,x4+1/2 7 x1,-x2+1/2,x3,-x4+1/2 8 -x1+1/2,x2+1/2,x3+1/2,x4 _cell_length_a 24.0549(3) _cell_length_b 4.1291(6) _cell_length_c 11.3361(16) _cell_angle_alpha 90(5) _cell_angle_beta 90(6) _cell_angle_gamma 90(5) _cell_volume 1126(2) _cell_modulation_dimension 1 loop_ _cell_wave_vector_seq_id _cell_wave_vector_x _cell_wave_vector_y _cell_wave_vector_z 1 0 0.5433 0 _cell_formula_units_Z 1 _cell_measurement_temperature 297.4 _exptl_crystal_type_of_structure mod _exptl_crystal_density_diffrn 6.4791 _exptl_crystal_F_000 1839 _exptl_absorpt_coefficient_mu 54.685 _diffrn_ambient_temperature 297.4 _diffrn_radiation_type 'Mo K\a' _diffrn_source 'X-ray tube' _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_monochromator graphite _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'Oxford Diffraction CCD' loop_ _diffrn_standard_refln_index_h _diffrn_standard_refln_index_k _diffrn_standard_refln_index_l ? ? ? _diffrn_radiation_probe x-ray _reflns_number_total 6604 _reflns_number_gt 4696 _reflns_threshold_expression I>3\s(I) _refine_ls_structure_factor_coef Fsqd _refine_ls_R_factor_gt 0.0479 _refine_ls_wR_factor_gt 0.1076 _refine_ls_R_factor_all 0.0682 _refine_ls_wR_factor_ref 0.1145 _refine_ls_goodness_of_fit_ref 1.97 _refine_ls_goodness_of_fit_gt 2.21 _refine_ls_number_reflns 6604 _refine_ls_number_parameters 216 _refine_ls_number_constraints 78 _refine_ls_weighting_scheme sigma _refine_ls_weighting_details w=1/(\s^2^(I)+0.0004I^2^) _refine_ls_shift/su_max 0.8073 _refine_ls_shift/su_mean 0.0432 _refine_ls_extinction_method none loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source Cu 0.3201 1.2651 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' Pb -3.3944 10.1111 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' S 0.1246 0.1234 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' Sb -0.5866 1.5461 'International Tables Vol C tables 4.2.6.8 and 6.1.1.1' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_adp_type _atom_site_U_iso_or_equiv _atom_site_site_symmetry_multiplicity _atom_site_occupancy _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_disorder_assembly _atom_site_disorder_group Cu1 Cu 0.247(2) 0.25 -0.209(5) Uani 0.0388(11) 4 0.239(4) d ? ? ? Pb1 Pb 0.125229(14) 0.25 0.15769(3) Uani 0.02675(11) 4 1 d ? ? ? Pb2 Pb 0.064759(19) 0.75 0.46575(4) Uani 0.02537(16) 4 0.48(17) d ? ? ? Sb2 Sb 0.064759(19) 0.75 0.46575(4) Uani 0.02537(16) 4 0.5199(17) d ? ? ? Pb3 Pb 0.025121(19) 0.25 -0.15251(4) Uani 0.02636(16) 4 0.5246(18) d ? ? ? Sb3 Sb 0.025121(19) 0.25 -0.15251(4) Uani 0.02636(16) 4 0.4754(18) d ? ? ? Pb4 Pb 0.215255(15) 0.25 0.48311(4) Uani 0.03405(13) 4 1 d ? ? ? Pb5 Pb 0.15041(2) 0.75 -0.21855(5) Uani 0.02817(16) 4 0.2841 d ? ? ? Sb5 Sb 0.15041(2) 0.75 -0.21855(5) Uani 0.02817(16) 4 0.7159 d ? ? ? S1 S 0.15229(8) 0.75 0.33925(19) Uani 0.0214(6) 4 1 d ? ? ? S2 S -0.06368(9) 0.25 -0.02736(18) Uani 0.0214(6) 4 1 d ? ? ? S3 S 0.23688(9) 0.75 -0.3373(2) Uani 0.0244(6) 4 1 d ? ? ? S4 S -0.02045(9) 0.75 -0.28375(19) Uani 0.024(6) 4 1 d ? ? ? S5 S 0.10735(9) 0.25 0.5944(2) Uani 0.0263(6) 4 1 d ? ? ? S6 S 0.18416(9) 0.25 -0.0896(2) Uani 0.0353(7) 4 1 d ? ? ? loop_ _atom_site_aniso_label _atom_site_aniso_type_symbol _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Cu1 Cu 0.0318(17) 0.0351(18) 0.05(2) 0 -0.0051(14) 0 Pb1 Pb 0.02884(19) 0.02372(18) 0.0277(2) 0 0.00114(13) 0 Pb2 Pb 0.0275(3) 0.0243(3) 0.0244(3) 0 0.00051(18) 0 Sb2 Sb 0.0275(3) 0.0243(3) 0.0244(3) 0 0.00051(18) 0 Pb3 Pb 0.0291(3) 0.0243(3) 0.0257(3) 0 0.00392(18) 0 Sb3 Sb 0.0291(3) 0.0243(3) 0.0257(3) 0 0.00392(18) 0 Pb4 Pb 0.02498(19) 0.0333(2) 0.0439(3) 0 0.00206(15) 0 Pb5 Pb 0.0236(3) 0.0335(3) 0.0275(3) 0 -0.0003(2) 0 Sb5 Sb 0.0236(3) 0.0335(3) 0.0275(3) 0 -0.0003(2) 0 S1 S 0.0222(10) 0.023(10) 0.0189(10) 0 0(8) 0 S2 S 0.024(10) 0.0214(10) 0.0188(10) 0 0.0008(8) 0 S3 S 0.0255(10) 0.0248(10) 0.0229(11) 0 0.0033(8) 0 S4 S 0.0252(10) 0.026(10) 0.0207(11) 0 -0.0007(8) 0 S5 S 0.0273(10) 0.0279(11) 0.0237(11) 0 0.0002(8) 0 S6 S 0.0259(11) 0.0552(15) 0.0247(12) 0 -0.0001(9) 0 loop_ _atom_site_Fourier_wave_vector_seq_id _jana_atom_site_Fourier_wave_vector_q1_coeff 1 1 2 2 loop_ _jana_atom_site_occ_Fourier_absolute_site_label _jana_atom_site_occ_Fourier_absolute Cu1 0.239(4) Pb2 0.4801(17) Sb2 0.5199(17) Pb3 0.5246(18) Sb3 0.4754(18) Pb5 0.2841 Sb5 0.7159 loop_ _atom_site_occ_Fourier_id _atom_site_occ_Fourier_atom_site_label _atom_site_occ_Fourier_wave_vector_seq_id Cu1o1 Cu1 1 Cu1o2 Cu1 2 Pb2o1 Pb2 1 Pb2o2 Pb2 2 Sb2o1 Sb2 1 Sb2o2 Sb2 2 Pb3o1 Pb3 1 Pb3o2 Pb3 2 Sb3o1 Sb3 1 Sb3o2 Sb3 2 Pb5o1 Pb5 1 Pb5o2 Pb5 2 Sb5o1 Sb5 1 Sb5o2 Sb5 2 loop_ _atom_site_occ_Fourier_param_id _atom_site_occ_Fourier_param_cos _atom_site_occ_Fourier_param_sin Cu1o1 0 0.379(5) Cu1o2 -0.174(4) 0 Pb2o1 0 0.548(4) Pb2o2 0(5) 0 Sb2o1 0 -0.548(4) Sb2o2 0(5) 0 Pb3o1 0 0.544(4) Pb3o2 0.056(5) 0 Sb3o1 0 -0.544(4) Sb3o2 -0.056(5) 0 Pb5o1 0 -0.394(4) Pb5o2 -0.126(5) 0 Sb5o1 0 0.394(4) Sb5o2 0.126(5) 0 loop_ _atom_site_displace_Fourier_id _atom_site_displace_Fourier_atom_site_label _atom_site_displace_Fourier_axis _atom_site_displace_Fourier_wave_vector_seq_id Cu1x1 Cu1 x 1 Cu1y1 Cu1 y 1 Cu1z1 Cu1 z 1 Cu1x2 Cu1 x 2 Cu1y2 Cu1 y 2 Cu1z2 Cu1 z 2 Pb1x1 Pb1 x 1 Pb1y1 Pb1 y 1 Pb1z1 Pb1 z 1 Pb1x2 Pb1 x 2 Pb1y2 Pb1 y 2 Pb1z2 Pb1 z 2 Pb2x1 Pb2 x 1 Pb2y1 Pb2 y 1 Pb2z1 Pb2 z 1 Pb2x2 Pb2 x 2 Pb2y2 Pb2 y 2 Pb2z2 Pb2 z 2 Sb2x1 Sb2 x 1 Sb2y1 Sb2 y 1 Sb2z1 Sb2 z 1 Sb2x2 Sb2 x 2 Sb2y2 Sb2 y 2 Sb2z2 Sb2 z 2 Pb3x1 Pb3 x 1 Pb3y1 Pb3 y 1 Pb3z1 Pb3 z 1 Pb3x2 Pb3 x 2 Pb3y2 Pb3 y 2 Pb3z2 Pb3 z 2 Sb3x1 Sb3 x 1 Sb3y1 Sb3 y 1 Sb3z1 Sb3 z 1 Sb3x2 Sb3 x 2 Sb3y2 Sb3 y 2 Sb3z2 Sb3 z 2 Pb4x1 Pb4 x 1 Pb4y1 Pb4 y 1 Pb4z1 Pb4 z 1 Pb4x2 Pb4 x 2 Pb4y2 Pb4 y 2 Pb4z2 Pb4 z 2 Pb5x1 Pb5 x 1 Pb5y1 Pb5 y 1 Pb5z1 Pb5 z 1 Pb5x2 Pb5 x 2 Pb5y2 Pb5 y 2 Pb5z2 Pb5 z 2 Sb5x1 Sb5 x 1 Sb5y1 Sb5 y 1 Sb5z1 Sb5 z 1 Sb5x2 Sb5 x 2 Sb5y2 Sb5 y 2 Sb5z2 Sb5 z 2 S1x1 S1 x 1 S1y1 S1 y 1 S1z1 S1 z 1 S1x2 S1 x 2 S1y2 S1 y 2 S1z2 S1 z 2 S2x1 S2 x 1 S2y1 S2 y 1 S2z1 S2 z 1 S2x2 S2 x 2 S2y2 S2 y 2 S2z2 S2 z 2 S3x1 S3 x 1 S3y1 S3 y 1 S3z1 S3 z 1 S3x2 S3 x 2 S3y2 S3 y 2 S3z2 S3 z 2 S4x1 S4 x 1 S4y1 S4 y 1 S4z1 S4 z 1 S4x2 S4 x 2 S4y2 S4 y 2 S4z2 S4 z 2 S5x1 S5 x 1 S5y1 S5 y 1 S5z1 S5 z 1 S5x2 S5 x 2 S5y2 S5 y 2 S5z2 S5 z 2 S6x1 S6 x 1 S6y1 S6 y 1 S6z1 S6 z 1 S6x2 S6 x 2 S6y2 S6 y 2 S6z2 S6 z 2 loop_ _atom_site_displace_Fourier_param_id _atom_site_displace_Fourier_param_cos _atom_site_displace_Fourier_param_sin Cu1x1 0 0.01(3) Cu1y1 -0.014(17) 0 Cu1z1 0 -0.05(8) Cu1x2 0.0043(13) 0 Cu1y2 0 0.011(13) Cu1z2 -0.02(3) 0 Pb1x1 0 -0.000915(17) Pb1y1 0.0039(9) 0 Pb1z1 0 -0.00257(4) Pb1x2 -0.00048(2) 0 Pb1y2 0 -0.00178(11) Pb1z2 0.00309(4) 0 Pb2x1 0 -0.00573(2) Pb2y1 0.01408(13) 0 Pb2z1 0 -0.00509(5) Pb2x2 -0.00155(3) 0 Pb2y2 0 0.00265(16) Pb2z2 -0.0043(6) 0 Sb2x1 0 -0.00573(2) Sb2y1 0.01408(13) 0 Sb2z1 0 -0.00509(5) Sb2x2 -0.00155(3) 0 Sb2y2 0 0.00265(16) Sb2z2 -0.0043(6) 0 Pb3x1 0 0.00647(2) Pb3y1 -0.00187(12) 0 Pb3z1 0 0.0095(5) Pb3x2 0.00047(3) 0 Pb3y2 0 -0.00186(15) Pb3z2 0.00515(6) 0 Sb3x1 0 0.00647(2) Sb3y1 -0.00187(12) 0 Sb3z1 0 0.0095(5) Sb3x2 0.00047(3) 0 Sb3y2 0 -0.00186(15) Sb3z2 0.00515(6) 0 Pb4x1 0 0.001366(17) Pb4y1 -0.00326(10) 0 Pb4z1 0 0.00588(5) Pb4x2 0.00061(2) 0 Pb4y2 0 -0.00386(13) Pb4z2 0.01081(5) 0 Pb5x1 0 0.0017(2) Pb5y1 -0.02717(16) 0 Pb5z1 0 0.0021(6) Pb5x2 0.00005(3) 0 Pb5y2 0 0.00641(18) Pb5z2 -0.00484(6) 0 Sb5x1 0 0.0017(2) Sb5y1 -0.02717(16) 0 Sb5z1 0 0.0021(6) Sb5x2 0.00005(3) 0 Sb5y2 0 0.00641(18) Sb5z2 -0.00484(6) 0 S1x1 0 0.00301(10) S1y1 -0.0075(6) 0 S1z1 0 0.0011(2) S1x2 -0.00003(12) 0 S1y2 0 -0.0004(7) S1z2 -0.0015(3) 0 S2x1 0 -0.00279(10) S2y1 -0.0104(6) 0 S2z1 0 0(2) S2x2 -0.00122(12) 0 S2y2 0 -0.0012(7) S2z2 0.0021(3) 0 S3x1 0 -0.00467(11) S3y1 0.0025(6) 0 S3z1 0 -0.0047(2) S3x2 -0.00047(12) 0 S3y2 0 -0.0004(7) S3z2 -0.0019(3) 0 S4x1 0 0.00085(10) S4y1 -0.0513(6) 0 S4z1 0 0.0027(2) S4x2 0.00103(13) 0 S4y2 0 -0.0016(7) S4z2 -0.0011(3) 0 S5x1 0 -0.00317(11) S5y1 -0.0575(7) 0 S5z1 0 -0.0019(3) S5x2 -0.00106(13) 0 S5y2 0 0.002(7) S5z2 0.002(3) 0 S6x1 0 0.00084(12) S6y1 0.069(9) 0 S6z1 0 0.0049(3) S6x2 -0.0006(14) 0 S6y2 0 0.0197(9) S6z2 0.0039(3) 0 loop_ _atom_site_U_Fourier_id _atom_site_U_Fourier_atom_site_label _atom_site_U_Fourier_tens_elem _atom_site_U_Fourier_wave_vector_seq_id Pb1U111 Pb1 U11 1 Pb1U221 Pb1 U22 1 Pb1U331 Pb1 U33 1 Pb1U121 Pb1 U12 1 Pb1U131 Pb1 U13 1 Pb1U231 Pb1 U23 1 Pb1U112 Pb1 U11 2 Pb1U222 Pb1 U22 2 Pb1U332 Pb1 U33 2 Pb1U122 Pb1 U12 2 Pb1U132 Pb1 U13 2 Pb1U232 Pb1 U23 2 Pb2U111 Pb2 U11 1 Pb2U221 Pb2 U22 1 Pb2U331 Pb2 U33 1 Pb2U121 Pb2 U12 1 Pb2U131 Pb2 U13 1 Pb2U231 Pb2 U23 1 Pb2U112 Pb2 U11 2 Pb2U222 Pb2 U22 2 Pb2U332 Pb2 U33 2 Pb2U122 Pb2 U12 2 Pb2U132 Pb2 U13 2 Pb2U232 Pb2 U23 2 Sb2U111 Sb2 U11 1 Sb2U221 Sb2 U22 1 Sb2U331 Sb2 U33 1 Sb2U121 Sb2 U12 1 Sb2U131 Sb2 U13 1 Sb2U231 Sb2 U23 1 Sb2U112 Sb2 U11 2 Sb2U222 Sb2 U22 2 Sb2U332 Sb2 U33 2 Sb2U122 Sb2 U12 2 Sb2U132 Sb2 U13 2 Sb2U232 Sb2 U23 2 Pb3U111 Pb3 U11 1 Pb3U221 Pb3 U22 1 Pb3U331 Pb3 U33 1 Pb3U121 Pb3 U12 1 Pb3U131 Pb3 U13 1 Pb3U231 Pb3 U23 1 Pb3U112 Pb3 U11 2 Pb3U222 Pb3 U22 2 Pb3U332 Pb3 U33 2 Pb3U122 Pb3 U12 2 Pb3U132 Pb3 U13 2 Pb3U232 Pb3 U23 2 Sb3U111 Sb3 U11 1 Sb3U221 Sb3 U22 1 Sb3U331 Sb3 U33 1 Sb3U121 Sb3 U12 1 Sb3U131 Sb3 U13 1 Sb3U231 Sb3 U23 1 Sb3U112 Sb3 U11 2 Sb3U222 Sb3 U22 2 Sb3U332 Sb3 U33 2 Sb3U122 Sb3 U12 2 Sb3U132 Sb3 U13 2 Sb3U232 Sb3 U23 2 Pb4U111 Pb4 U11 1 Pb4U221 Pb4 U22 1 Pb4U331 Pb4 U33 1 Pb4U121 Pb4 U12 1 Pb4U131 Pb4 U13 1 Pb4U231 Pb4 U23 1 Pb4U112 Pb4 U11 2 Pb4U222 Pb4 U22 2 Pb4U332 Pb4 U33 2 Pb4U122 Pb4 U12 2 Pb4U132 Pb4 U13 2 Pb4U232 Pb4 U23 2 Pb5U111 Pb5 U11 1 Pb5U221 Pb5 U22 1 Pb5U331 Pb5 U33 1 Pb5U121 Pb5 U12 1 Pb5U131 Pb5 U13 1 Pb5U231 Pb5 U23 1 Pb5U112 Pb5 U11 2 Pb5U222 Pb5 U22 2 Pb5U332 Pb5 U33 2 Pb5U122 Pb5 U12 2 Pb5U132 Pb5 U13 2 Pb5U232 Pb5 U23 2 Sb5U111 Sb5 U11 1 Sb5U221 Sb5 U22 1 Sb5U331 Sb5 U33 1 Sb5U121 Sb5 U12 1 Sb5U131 Sb5 U13 1 Sb5U231 Sb5 U23 1 Sb5U112 Sb5 U11 2 Sb5U222 Sb5 U22 2 Sb5U332 Sb5 U33 2 Sb5U122 Sb5 U12 2 Sb5U132 Sb5 U13 2 Sb5U232 Sb5 U23 2 loop_ _atom_site_U_Fourier_param_id _atom_site_U_Fourier_param_cos _atom_site_U_Fourier_param_sin Pb1U111 0 0.0012(2) Pb1U221 0 0.00131(20) Pb1U331 0 0.0005(3) Pb1U121 0.00111(16) 0 Pb1U131 0 -0.00119(18) Pb1U231 0.00068(17) 0 Pb1U112 -0.0028(3) 0 Pb1U222 -0.0013(3) 0 Pb1U332 0.0003(3) 0 Pb1U122 0 -0.0002(2) Pb1U132 -0.0004(2) 0 Pb1U232 0 -0.0005(2) Pb2U111 0 0.0011(3) Pb2U221 0 0.0016(3) Pb2U331 0 0.0012(4) Pb2U121 -0.0028(2) 0 Pb2U131 0 0.0012(2) Pb2U231 -0.0014(2) 0 Pb2U112 0.0083(4) 0 Pb2U222 0.0023(4) 0 Pb2U332 0.0042(4) 0 Pb2U122 0 0.0006(3) Pb2U132 0.0036(3) 0 Pb2U232 0 0.0015(3) Sb2U111 0 0.0011(3) Sb2U221 0 0.0016(3) Sb2U331 0 0.0012(4) Sb2U121 -0.0028(2) 0 Sb2U131 0 0.0012(2) Sb2U231 -0.0014(2) 0 Sb2U112 0.0083(4) 0 Sb2U222 0.0023(4) 0 Sb2U332 0.0042(4) 0 Sb2U122 0 0.0006(3) Sb2U132 0.0036(3) 0 Sb2U232 0 0.0015(3) Pb3U111 0 0.0029(3) Pb3U221 0 0.0023(3) Pb3U331 0 0.0031(4) Pb3U121 0.0003(2) 0 Pb3U131 0 -0.0002(2) Pb3U231 -0.0013(2) 0 Pb3U112 0.0076(4) 0 Pb3U222 -0.0002(4) 0 Pb3U332 0.0065(4) 0 Pb3U122 0 0.0005(3) Pb3U132 0.0061(3) 0 Pb3U232 0 -0.0004(3) Sb3U111 0 0.0029(3) Sb3U221 0 0.0023(3) Sb3U331 0 0.0031(4) Sb3U121 0.0003(2) 0 Sb3U131 0 -0.0002(2) Sb3U231 -0.0013(2) 0 Sb3U112 0.0076(4) 0 Sb3U222 -0.0002(4) 0 Sb3U332 0.0065(4) 0 Sb3U122 0 0.0005(3) Sb3U132 0.0061(3) 0 Sb3U232 0 -0.0004(3) Pb4U111 0 0(2) Pb4U221 0 -0.0031(2) Pb4U331 0 -0.0128(3) Pb4U121 -0.00145(17) 0 Pb4U131 0 0.0007(2) Pb4U231 -0.0064(2) 0 Pb4U112 -0.0004(3) 0 Pb4U222 -0.0025(3) 0 Pb4U332 -0.0039(3) 0 Pb4U122 0 -0.0004(3) Pb4U132 0.0024(2) 0 Pb4U232 0 0.0013(2) Pb5U111 0 -0.0035(3) Pb5U221 0 -0.0006(4) Pb5U331 0 -0.0011(4) Pb5U121 0.0024(3) 0 Pb5U131 0 -0.0001(2) Pb5U231 0.0092(3) 0 Pb5U112 0.0007(5) 0 Pb5U222 0.0092(5) 0 Pb5U332 0.0059(5) 0 Pb5U122 0 0.0006(3) Pb5U132 0.0008(3) 0 Pb5U232 0 0.0007(3) Sb5U111 0 -0.0035(3) Sb5U221 0 -0.0006(4) Sb5U331 0 -0.0011(4) Sb5U121 0.0024(3) 0 Sb5U131 0 -0.0001(2) Sb5U231 0.0092(3) 0 Sb5U112 0.0007(5) 0 Sb5U222 0.0092(5) 0 Sb5U332 0.0059(5) 0 Sb5U122 0 0.0006(3) Sb5U132 0.0008(3) 0 Sb5U232 0 0.0007(3) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_ssg_symmetry_1 _geom_bond_site_ssg_symmetry_2 _geom_bond_distance_av _geom_bond_distance_min _geom_bond_distance_max _geom_bond_publ_flag Cu1 Pb4 ? 1_5545 3.22(9) 3.14(14) 3.32(14) ? Cu1 Pb4 ? 2_5545 3.35(8) 3.1(11) 3.46(11) ? Cu1 Pb4 ? 2_5645 3.35(8) 3.1(11) 3.46(11) ? Cu1 Pb5 ? 1_5455 3.29(8) 3.16(10) 3.34(10) ? Cu1 Pb5 ? ? 3.29(8) 3.15(10) 3.34(10) ? Cu1 S1 ? 2_5645 2.41(8) 2.39(13) 2.45(13) ? Cu1 S3 ? 1_5455 2.36(8) 2.29(9) 2.52(9) ? Cu1 S3 ? ? 2.37(8) 2.29(9) 2.52(9) ? Cu1 S6 ? ? 2.42(9) 2.29(13) 2.48(13) ? Pb1 S1 ? 1_5455 2.988(3) 2.949(4) 3.042(4) ? Pb1 S1 ? ? 2.988(3) 2.949(4) 3.042(4) ? Pb1 S2 ? 3_5455 2.939(3) 2.859(4) 2.987(4) ? Pb1 S2 ? 3_5555 2.939(3) 2.859(4) 2.987(4) ? Pb1 S4 ? 3_5455 2.901(4) 2.891(6) 2.907(6) ? Pb2 Pb2 ? 3_5465 3.7609(11) 3.7302(13) 3.9507(13) ? Pb2 Pb2 ? 3_5565 3.7626(11) 3.7302(13) 3.9506(13) ? Pb2 Sb2 ? ? 0 0 0 ? Pb2 S1 ? ? 2.587(3) 2.445(6) 2.673(6) ? Pb2 S4 ? 3_5455 3.044(4) 2.89(5) 3.342(5) ? Pb2 S4 ? 3_5555 3.045(4) 2.89(5) 3.337(5) ? Pb2 S5 ? ? 2.802(4) 2.496(4) 2.983(4) ? Pb2 S5 ? 1_5655 2.803(4) 2.49(4) 2.983(4) ? Sb2 S1 ? ? 2.529(3) 2.411(6) 2.66(6) ? Sb2 S5 ? ? 2.684(4) 2.427(4) 2.982(4) ? Sb2 S5 ? 1_5655 2.686(4) 2.427(4) 2.983(4) ? Pb3 Sb3 ? ? 0 0 0 ? Pb3 Pb5 ? 1_5455 3.694(11) 3.6708(13) 3.747(13) ? Pb3 Pb5 ? ? 3.6944(11) 3.6708(13) 3.748(13) ? Pb3 S2 ? ? 2.597(3) 2.462(6) 2.68(6) ? Pb3 S2 ? 3_5455 3.01(3) 2.936(4) 3.199(4) ? Pb3 S2 ? 3_5555 3.01(3) 2.936(4) 3.2(4) ? Pb3 S4 ? 1_5455 2.838(4) 2.517(4) 3.013(4) ? Pb3 S4 ? ? 2.838(4) 2.52(4) 3.013(4) ? Sb3 S2 ? ? 2.544(3) 2.438(6) 2.665(6) ? Sb3 S4 ? 1_5455 2.717(4) 2.452(4) 2.993(4) ? Sb3 S4 ? ? 2.717(4) 2.452(4) 2.994(4) ? Pb4 S1 ? 1_5455 3.037(3) 2.89(4) 3.137(4) ? Pb4 S1 ? ? 3.037(3) 2.89(4) 3.136(4) ? Pb4 S3 ? 1_5465 2.948(4) 2.83(4) 3.076(4) ? Pb4 S3 ? 1_5565 2.947(4) 2.83(4) 3.076(4) ? Pb4 S5 ? ? 2.893(4) 2.843(6) 2.953(6) ? Pb5 Sb5 ? ? 0 0 0 ? Pb5 S3 ? ? 2.519(4) 2.429(6) 2.596(6) ? Pb5 S5 ? 1_5545 3.047(4) 2.894(5) 3.284(5) ? Pb5 S5 ? 1_5645 3.045(4) 2.894(5) 3.28(5) ? Pb5 S6 ? ? 2.781(4) 2.532(5) 2.996(5) ? Pb5 S6 ? 1_5655 2.78(4) 2.529(5) 2.996(5) ? Sb5 S3 ? ? 2.481(4) 2.419(6) 2.596(6) ? Sb5 S6 ? ? 2.658(4) 2.411(5) 2.996(5) ? Sb5 S6 ? 1_5655 2.658(4) 2.411(5) 2.996(5) ? loop_ _refln_index_h _refln_index_k _refln_index_l _refln_index_m_1 _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_include_status 0 0 0 2 525.0 335.0 27.0 o 2 0 0 2 211.0 176.0 14.0 o 4 0 0 2 163.0 108.0 11.0 o 5 0 0 1 19271.0 20636.0 179.0 o 6 0 0 0 1645.0 1653.0 101.0 o 6 0 0 2 22.0 14.0 7.0 < 7 0 0 1 3731.0 3907.0 70.0 o 8 0 0 0 22599.0 24881.0 310.0 o 8 0 0 2 5.0 15.0 8.0 < 9 0 0 1 819.0 710.0 30.0 o 10 0 0 0 44956.0 49927.0 455.0 o 10 0 0 2 481.0 705.0 37.0 o 11 0 0 1 24.0 39.0 10.0 o 12 0 0 0 121235.0 123957.0 637.0 o 12 0 0 2 63.0 162.0 22.0 o 13 0 0 1 23.0 32.0 9.0 o 14 0 0 0 85369.0 86792.0 764.0 o 14 0 0 2 18.0 53.0 14.0 o 15 0 0 1 8551.0 8630.0 159.0 o 16 0 0 0 2900.0 2994.0 120.0 o 16 0 0 2 46.0 51.0 15.0 o 17 0 0 1 4270.0 4290.0 104.0 o 18 0 0 0 1142.0 1209.0 99.0 o 18 0 0 2 235.0 245.0 32.0 o 19 0 0 1 95.0 95.0 21.0 o 20 0 0 0 33476.0 34350.0 458.0 o 20 0 0 2 563.0 554.0 48.0 o 21 0 0 1 194.0 180.0 30.0 o 22 0 0 0 47139.0 46096.0 552.0 o 22 0 0 2 2.0 466.0 81.0 o 23 0 0 1 33.0 29.0 16.0 < 24 0 0 0 7627.0 7921.0 238.0 o 24 0 0 2 5.0 45.0 29.0 < 25 0 0 1 189.0 187.0 34.0 o 26 0 0 0 6615.0 6645.0 282.0 o 26 0 0 2 10.0 21.0 19.0 < 27 0 0 1 294.0 396.0 48.0 o 28 0 0 0 1044.0 990.0 110.0 o 28 0 0 2 93.0 39.0 22.0 < 29 0 0 1 2710.0 2986.0 139.0 o 30 0 0 0 8900.0 8622.0 342.0 o 30 0 0 2 4.0 30.0 27.0 < 1 1 0 1 247.0 211.0 12.0 o 2 1 0 0 15198.0 16405.0 125.0 o 2 1 0 2 523.0 733.0 30.0 o 3 1 0 1 1502.0 1464.0 42.0 o 4 1 0 0 31387.0 33374.0 169.0 o 4 1 0 2 1.0 27.0 10.0 < 5 1 0 -1 1231.0 1244.0 50.0 o 5 1 0 1 99.0 93.0 11.0 o 6 1 0 -2 34.0 47.0 11.0 o 6 1 0 0 15210.0 15012.0 151.0 o 6 1 0 2 21.0 18.0 9.0 < 7 1 0 -1 247.0 220.0 17.0 o 7 1 0 1 4281.0 4283.0 87.0 o 8 1 0 -2 7.0 15.0 6.0 < 8 1 0 0 39990.0 39050.0 237.0 o 8 1 0 2 116.0 120.0 21.0 o 9 1 0 -1 154.0 144.0 14.0 o 9 1 0 1 31.0 46.0 11.0 o 10 1 0 -2 52.0 97.0 14.0 o 10 1 0 0 547434.0 492973.0 1040.0 o 10 1 0 2 206.0 150.0 25.0 o 11 1 0 -1 245.0 186.0 18.0 o 11 1 0 1 173.0 204.0 22.0 o 12 1 0 -2 2.0 87.0 18.0 o 12 1 0 0 261839.0 243919.0 642.0 o 12 1 0 2 599.0 421.0 40.0 o 13 1 0 -1 293.0 323.0 25.0 o 13 1 0 1 17.0 50.0 22.0 < 14 1 0 -2 257.0 324.0 27.0 o 14 1 0 0 6461.0 6074.0 101.0 o 14 1 0 2 202.0 210.0 32.0 o 15 1 0 -1 3318.0 3317.0 96.0 o 15 1 0 1 2516.0 2528.0 86.0 o 16 1 0 -2 3.0 27.0 15.0 < 16 1 0 0 1932.0 2073.0 75.0 o 16 1 0 2 92.0 52.0 17.0 < 17 1 0 -1 6237.0 6429.0 127.0 o 17 1 0 1 9413.0 9927.0 182.0 o 18 1 0 -2 57.0 70.0 18.0 o 18 1 0 0 7018.0 7255.0 159.0 o 18 1 0 2 24.0 -10.0 20.0 < 19 1 0 -1 3396.0 3430.0 110.0 o 19 1 0 1 4778.0 4628.0 159.0 o 20 1 0 -2 22.0 71.0 24.0 < 20 1 0 0 624.0 711.0 53.0 o 20 1 0 2 77.0 136.0 51.0 < 21 1 0 -1 155.0 154.0 29.0 o 21 1 0 1 1.0 -1.0 26.0 < 22 1 0 -2 11.0 114.0 34.0 o 22 1 0 0 172598.0 164595.0 1083.0 o 22 1 0 2 23.0 65.0 36.0 < 23 1 0 -1 255.0 314.0 44.0 o 23 1 0 1 131.0 166.0 41.0 o 24 1 0 -2 2.0 44.0 25.0 < 24 1 0 0 20878.0 20721.0 343.0 o 24 1 0 2 9.0 35.0 41.0 < 25 1 0 -1 1105.0 1064.0 69.0 o 25 1 0 1 1098.0 1060.0 93.0 o 26 1 0 -2 21.0 83.0 32.0 < 26 1 0 0 1955.0 1800.0 104.0 o 26 1 0 2 34.0 140.0 44.0 o 27 1 0 -1 6837.0 6329.0 172.0 o 27 1 0 1 6598.0 6649.0 293.0 o 28 1 0 -2 34.0 37.0 26.0 < 28 1 0 0 621.0 508.0 50.0 o 28 1 0 2 21.0 27.0 44.0 < 29 1 0 -1 1862.0 1952.0 113.0 o 29 1 0 1 722.0 701.0 94.0 o 30 1 0 -2 79.0 41.0 29.0 < 30 1 0 0 2666.0 2705.0 176.0 o 0 2 0 0 1374240.0 898501.0 1390.0 o 0 2 0 2 805.0 402.0 50.0 o 1 2 0 -1 633.0 622.0 21.0 o 1 2 0 1 2.0 8.0 11.0 < 2 2 0 -2 236.0 239.0 25.0 o 2 2 0 0 1030.0 1030.0 35.0 o 2 2 0 2 11.0 94.0 21.0 o 3 2 0 -1 318.0 340.0 19.0 o 3 2 0 1 479.0 545.0 30.0 o 4 2 0 -2 6.0 20.0 7.0 < 4 2 0 0 2356.0 2252.0 54.0 o 4 2 0 2 444.0 462.0 39.0 o 5 2 0 -1 5970.0 5975.0 85.0 o 5 2 0 1 14358.0 14816.0 158.0 o 6 2 0 -2 31.0 37.0 7.0 o 6 2 0 0 259.0 246.0 21.0 o 6 2 0 2 144.0 114.0 18.0 o 7 2 0 -1 486.0 487.0 28.0 o 7 2 0 1 3279.0 3004.0 78.0 o 8 2 0 -2 41.0 19.0 8.0 < 8 2 0 0 13891.0 13970.0 167.0 o 8 2 0 2 27.0 55.0 21.0 < 9 2 0 -1 2468.0 2546.0 67.0 o 9 2 0 1 28.0 34.0 19.0 < 10 2 0 -2 63.0 182.0 23.0 o 10 2 0 0 26630.0 26831.0 287.0 o 10 2 0 2 698.0 1617.0 94.0 o 11 2 0 -1 85.0 96.0 19.0 o 11 2 0 1 6.0 18.0 14.0 < 12 2 0 -2 15.0 149.0 21.0 o 12 2 0 0 76459.0 74293.0 460.0 o 12 2 0 2 125.0 396.0 55.0 o 13 2 0 -1 56.0 69.0 15.0 o 13 2 0 1 79.0 107.0 20.0 o 14 2 0 -2 10.0 14.0 9.0 < 14 2 0 0 53692.0 52541.0 439.0 o 14 2 0 2 26.0 161.0 30.0 o 15 2 0 -1 2580.0 2457.0 83.0 o 15 2 0 1 6808.0 6449.0 185.0 o 16 2 0 -2 1.0 12.0 12.0 < 16 2 0 0 1417.0 1413.0 79.0 o 16 2 0 2 29.0 -3.0 23.0 < 17 2 0 -1 9102.0 9241.0 175.0 o 17 2 0 1 653.0 753.0 60.0 o 18 2 0 -2 215.0 183.0 27.0 o 18 2 0 0 797.0 826.0 64.0 o 18 2 0 2 98.0 79.0 21.0 o 19 2 0 -1 444.0 628.0 66.0 o 19 2 0 1 600.0 701.0 58.0 o 20 2 0 -2 169.0 147.0 27.0 o 20 2 0 0 23956.0 24256.0 376.0 o 20 2 0 2 719.0 607.0 69.0 o 21 2 0 -1 5.0 6.0 33.0 < 21 2 0 1 257.0 294.0 43.0 o 22 2 0 -2 3.0 491.0 87.0 o 22 2 0 0 32246.0 31130.0 503.0 o 22 2 0 2 1.0 227.0 62.0 o 23 2 0 -1 81.0 66.0 29.0 < 23 2 0 1 11.0 -53.0 37.0 < 24 2 0 -2 125.0 197.0 42.0 o 24 2 0 0 4077.0 3922.0 177.0 o 24 2 0 2 118.0 155.0 39.0 o 25 2 0 -1 692.0 665.0 71.0 o 25 2 0 1 5.0 -18.0 26.0 < 26 2 0 -2 0.0 7.0 16.0 < 26 2 0 0 4637.0 5008.0 255.0 o 27 2 0 -1 150.0 228.0 50.0 o 27 2 0 1 284.0 321.0 74.0 o 28 2 0 -2 100.0 60.0 22.0 < 28 2 0 0 431.0 405.0 83.0 o 29 2 0 -1 1068.0 1168.0 120.0 o 30 2 0 -2 11.0 -25.0 25.0 < 1 3 0 -1 15.0 15.0 9.0 < 1 3 0 1 33.0 35.0 28.0 < 2 3 0 -2 36.0 9.0 7.0 < 2 3 0 0 5470.0 5512.0 109.0 o 2 3 0 2 612.0 837.0 76.0 o 3 3 0 -1 708.0 904.0 39.0 o 3 3 0 1 1027.0 904.0 59.0 o 4 3 0 -2 4.0 8.0 6.0 < 4 3 0 0 9702.0 9767.0 151.0 o 4 3 0 2 16.0 18.0 19.0 < 5 3 0 -1 1546.0 1839.0 54.0 o 5 3 0 1 200.0 196.0 25.0 o 6 3 0 -2 66.0 74.0 13.0 o 6 3 0 0 2364.0 2407.0 74.0 o 6 3 0 2 2.0 1.0 17.0 < 7 3 0 -1 1550.0 1596.0 57.0 o 7 3 0 1 3653.0 3695.0 103.0 o 8 3 0 -2 5.0 1.0 7.0 < 8 3 0 0 10381.0 10191.0 153.0 o 8 3 0 2 151.0 168.0 34.0 o 9 3 0 -1 354.0 449.0 35.0 o 9 3 0 1 16.0 33.0 16.0 < 10 3 0 -2 10.0 24.0 12.0 < 10 3 0 0 215400.0 203420.0 770.0 o 10 3 0 2 96.0 133.0 38.0 o 11 3 0 -1 127.0 139.0 25.0 o 11 3 0 1 101.0 188.0 29.0 o 12 3 0 -2 14.0 96.0 24.0 o 12 3 0 0 89570.0 87641.0 561.0 o 12 3 0 2 840.0 685.0 70.0 o 13 3 0 -1 414.0 355.0 37.0 o 13 3 0 1 16.0 54.0 28.0 < 14 3 0 -2 126.0 202.0 31.0 o 14 3 0 0 2454.0 2361.0 97.0 o 14 3 0 2 34.0 105.0 38.0 < 15 3 0 -1 1862.0 1907.0 90.0 o 15 3 0 1 1003.0 1032.0 71.0 o 16 3 0 -2 0.0 18.0 17.0 < 16 3 0 0 1298.0 1427.0 86.0 o 16 3 0 2 111.0 120.0 36.0 o 17 3 0 -1 1408.0 1354.0 75.0 o 17 3 0 1 5557.0 5733.0 181.0 o 18 3 0 -2 78.0 110.0 26.0 o 18 3 0 0 2304.0 2210.0 106.0 o 18 3 0 2 73.0 32.0 30.0 < 19 3 0 -1 836.0 774.0 63.0 o 19 3 0 1 2274.0 2379.0 133.0 o 20 3 0 -2 3.0 51.0 44.0 < 20 3 0 0 169.0 257.0 40.0 o 20 3 0 2 52.0 215.0 72.0 < 21 3 0 -1 449.0 492.0 53.0 o 21 3 0 1 7.0 -5.0 37.0 < 22 3 0 -2 16.0 51.0 40.0 < 22 3 0 0 79720.0 78168.0 736.0 o 23 3 0 -1 228.0 260.0 52.0 o 23 3 0 1 64.0 -23.0 117.0 < 24 3 0 -2 29.0 106.0 43.0 < 24 3 0 0 8561.0 8274.0 324.0 o 25 3 0 -1 547.0 627.0 77.0 o 26 3 0 -2 2.0 21.0 42.0 < 27 3 0 -1 3520.0 3385.0 228.0 o 28 3 0 -2 45.0 74.0 50.0 < 0 4 0 -2 324.0 168.0 29.0 o 0 4 0 0 312918.0 283127.0 1891.0 o 0 4 0 2 364.0 253.0 66.0 o 1 4 0 -1 424.0 310.0 37.0 o 1 4 0 1 7.0 9.0 21.0 < 2 4 0 -2 84.0 118.0 15.0 o 2 4 0 0 999.0 1059.0 84.0 o 2 4 0 2 14.0 51.0 27.0 < 3 4 0 -1 24.0 74.0 20.0 o 3 4 0 1 329.0 360.0 50.0 o 4 4 0 -2 0.0 36.0 16.0 < 4 4 0 0 616.0 583.0 61.0 o 4 4 0 2 224.0 244.0 46.0 o 5 4 0 -1 578.0 645.0 44.0 o 5 4 0 1 4667.0 4780.0 183.0 o 6 4 0 -2 0.0 16.0 13.0 < 6 4 0 0 17.0 57.0 18.0 o 6 4 0 2 62.0 17.0 31.0 < 7 4 0 -1 81.0 90.0 20.0 o 7 4 0 1 1013.0 1069.0 89.0 o 8 4 0 -2 40.0 47.0 14.0 o 8 4 0 0 4350.0 4424.0 136.0 o 8 4 0 2 15.0 45.0 51.0 < 9 4 0 -1 1210.0 1379.0 60.0 o 9 4 0 1 0.0 -26.0 29.0 < 10 4 0 -2 2.0 342.0 47.0 o 10 4 0 0 8104.0 8334.0 210.0 o 11 4 0 -1 19.0 25.0 18.0 < 11 4 0 1 1.0 -7.0 28.0 < 12 4 0 -2 16.0 105.0 32.0 o 12 4 0 0 23616.0 23403.0 358.0 o 13 4 0 -1 20.0 96.0 28.0 o 13 4 0 1 169.0 289.0 54.0 o 14 4 0 -2 1.0 28.0 18.0 < 14 4 0 0 15758.0 15828.0 301.0 o 15 4 0 -1 214.0 232.0 37.0 o 15 4 0 1 2081.0 1895.0 152.0 o 16 4 0 -2 20.0 1.0 22.0 < 16 4 0 0 89.0 74.0 27.0 < 17 4 0 -1 6132.0 6518.0 208.0 o 18 4 0 -2 114.0 69.0 28.0 < 18 4 0 0 233.0 266.0 57.0 o 19 4 0 -1 685.0 648.0 65.0 o 20 4 0 -2 28.0 3.0 26.0 < 20 4 0 0 9744.0 9144.0 295.0 o 21 4 0 -1 20.0 12.0 37.0 < 22 4 0 -2 5.0 254.0 72.0 o 23 4 0 -1 39.0 -83.0 69.0 < 24 4 0 -2 25.0 45.0 66.0 < 26 4 0 -2 0.0 -39.0 73.0 < 1 5 0 -1 11.0 -20.0 20.0 < 2 5 0 -2 36.0 71.0 30.0 < 2 5 0 0 1340.0 1132.0 93.0 o 3 5 0 -1 396.0 429.0 55.0 o 4 5 0 -2 9.0 40.0 23.0 < 4 5 0 0 1928.0 1835.0 120.0 o 5 5 0 -1 421.0 781.0 76.0 o 6 5 0 -2 68.0 47.0 20.0 < 6 5 0 0 24.0 69.0 29.0 < 7 5 0 -1 1618.0 1417.0 100.0 o 8 5 0 -2 1.0 52.0 22.0 < 8 5 0 0 983.0 1032.0 90.0 o 9 5 0 -1 73.0 184.0 39.0 o 10 5 0 -2 29.0 34.0 18.0 < 11 5 0 -1 12.0 11.0 23.0 < 12 5 0 -2 36.0 127.0 34.0 o 13 5 0 -1 180.0 167.0 40.0 o 14 5 0 -2 39.0 110.0 30.0 o 15 5 0 -1 482.0 562.0 69.0 o 16 5 0 -2 7.0 -6.0 25.0 < 17 5 0 -1 132.0 164.0 43.0 o 18 5 0 -2 4.0 36.0 39.0 < 20 5 0 -2 1.0 60.0 28.0 < 1 0 1 2 16.0 15.0 6.0 < 2 0 1 2 233.0 233.0 14.0 o 3 0 1 2 223.0 176.0 11.0 o 4 0 1 1 272.0 244.0 22.0 o 4 0 1 2 5.0 19.0 6.0 o 5 0 1 0 19291.0 19296.0 342.0 o 5 0 1 1 217.0 188.0 13.0 o 5 0 1 2 54.0 32.0 5.0 o 6 0 1 0 39901.0 42560.0 236.0 o 6 0 1 1 182.0 196.0 13.0 o 6 0 1 2 447.0 456.0 16.0 o 7 0 1 0 340187.0 326291.0 769.0 o 7 0 1 1 1550.0 1534.0 33.0 o 7 0 1 2 0.0 2.0 5.0 < 8 0 1 0 63820.0 66231.0 365.0 o 8 0 1 1 13.0 25.0 5.0 o 8 0 1 2 232.0 258.0 13.0 o 9 0 1 0 5273.0 5907.0 88.0 o 9 0 1 1 78.0 59.0 8.0 o 9 0 1 2 1.0 10.0 7.0 < 10 0 1 0 3262.0 3484.0 72.0 o 10 0 1 1 341.0 345.0 15.0 o 10 0 1 2 44.0 32.0 7.0 o 11 0 1 0 9890.0 10853.0 133.0 o 11 0 1 1 60.0 92.0 11.0 o 11 0 1 2 117.0 156.0 11.0 o 12 0 1 0 1891.0 2235.0 61.0 o 12 0 1 1 3793.0 3776.0 58.0 o 12 0 1 2 45.0 63.0 8.0 o 13 0 1 0 64383.0 67531.0 321.0 o 13 0 1 1 2172.0 2288.0 48.0 o 13 0 1 2 50.0 44.0 8.0 o 14 0 1 0 103854.0 103243.0 421.0 o 14 0 1 1 277.0 297.0 20.0 o 14 0 1 2 64.0 79.0 12.0 o 15 0 1 0 6087.0 6227.0 110.0 o 15 0 1 1 1260.0 1301.0 42.0 o 15 0 1 2 22.0 75.0 15.0 o 16 0 1 0 1654.0 1878.0 71.0 o 16 0 1 1 347.0 330.0 22.0 o 16 0 1 2 0.0 28.0 12.0 < 17 0 1 0 19.0 93.0 25.0 o 17 0 1 1 745.0 753.0 37.0 o 17 0 1 2 3.0 94.0 19.0 o 18 0 1 0 40981.0 42492.0 385.0 o 18 0 1 1 527.0 526.0 28.0 o 18 0 1 2 7.0 24.0 13.0 < 19 0 1 0 78582.0 78607.0 530.0 o 19 0 1 1 579.0 632.0 35.0 o 19 0 1 2 35.0 80.0 15.0 o 20 0 1 0 5177.0 5440.0 143.0 o 20 0 1 1 1811.0 1987.0 66.0 o 20 0 1 2 7.0 3.0 10.0 < 21 0 1 0 7584.0 7674.0 172.0 o 21 0 1 1 246.0 293.0 30.0 o 21 0 1 2 156.0 167.0 19.0 o 22 0 1 0 24944.0 25528.0 293.0 o 22 0 1 1 3522.0 3573.0 92.0 o 22 0 1 2 31.0 30.0 13.0 < 23 0 1 0 659.0 690.0 57.0 o 23 0 1 1 1082.0 1045.0 51.0 o 23 0 1 2 54.0 44.0 18.0 < 24 0 1 0 8174.0 8339.0 190.0 o 24 0 1 1 3156.0 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716.0 47.0 o 5 2 9 0 368.0 349.0 39.0 o 5 2 9 1 42.0 23.0 26.0 < 5 2 9 2 113.0 79.0 31.0 < 6 2 9 -2 15.0 10.0 20.0 < 6 2 9 -1 87.0 103.0 26.0 o 6 2 9 0 38.0 104.0 27.0 o 6 2 9 1 220.0 198.0 36.0 o 6 2 9 2 39.0 65.0 33.0 < 7 2 9 -2 175.0 133.0 26.0 o 7 2 9 -1 35.0 104.0 27.0 o 7 2 9 0 278.0 282.0 31.0 o 7 2 9 1 282.0 297.0 41.0 o 7 2 9 2 0.0 -28.0 32.0 < 8 2 9 -2 4.0 32.0 37.0 < 8 2 9 -1 1100.0 1066.0 57.0 o 8 2 9 0 14401.0 14501.0 211.0 o 8 2 9 1 245.0 203.0 33.0 o 8 2 9 2 29.0 55.0 35.0 < 9 2 9 -2 1299.0 1364.0 69.0 o 9 2 9 -1 54.0 79.0 24.0 o 9 2 9 0 45616.0 45456.0 375.0 o 9 2 9 1 399.0 319.0 37.0 o 9 2 9 2 319.0 427.0 63.0 o 10 2 9 -2 775.0 725.0 72.0 o 10 2 9 -1 93.0 94.0 24.0 o 10 2 9 0 1952.0 2160.0 83.0 o 10 2 9 1 339.0 291.0 36.0 o 10 2 9 2 161.0 306.0 53.0 o 11 2 9 -2 105.0 147.0 37.0 o 11 2 9 -1 29.0 47.0 18.0 < 11 2 9 0 889.0 940.0 55.0 o 11 2 9 1 143.0 104.0 27.0 o 11 2 9 2 319.0 178.0 35.0 o 12 2 9 -2 269.0 217.0 33.0 o 12 2 9 -1 15.0 34.0 19.0 < 12 2 9 0 24757.0 24067.0 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34.0 < 10 3 10 -2 283.0 348.0 43.0 o 10 3 10 -1 6.0 -32.0 22.0 < 10 3 10 0 12124.0 11906.0 256.0 o 10 3 10 1 427.0 324.0 72.0 o 11 3 10 -2 0.0 24.0 23.0 < 11 3 10 -1 129.0 105.0 29.0 o 11 3 10 0 879.0 598.0 54.0 o 11 3 10 1 3.0 28.0 62.0 < 12 3 10 -2 798.0 697.0 55.0 o 12 3 10 -1 443.0 385.0 44.0 o 12 3 10 0 5449.0 5151.0 169.0 o 13 3 10 -2 20.0 78.0 29.0 < 13 3 10 -1 869.0 829.0 63.0 o 13 3 10 0 5121.0 5892.0 221.0 o 14 3 10 -2 10.0 -14.0 22.0 < 14 3 10 -1 591.0 583.0 54.0 o 14 3 10 0 230.0 266.0 68.0 o 15 3 10 -2 28.0 -1.0 27.0 < 15 3 10 -1 455.0 453.0 49.0 o 16 3 10 -2 48.0 0.0 28.0 < 16 3 10 -1 61.0 14.0 22.0 < 17 3 10 -2 35.0 -19.0 35.0 < 17 3 10 -1 250.0 151.0 36.0 o 18 3 10 -2 275.0 165.0 34.0 o 18 3 10 -1 68.0 27.0 30.0 < 19 3 10 -2 145.0 216.0 39.0 o 20 3 10 -2 104.0 128.0 43.0 < 0 4 10 -2 36.0 135.0 54.0 < 0 4 10 -1 200.0 83.0 46.0 < 1 4 10 -2 77.0 -41.0 28.0 < 1 4 10 -1 14.0 -40.0 29.0 < 2 4 10 -2 319.0 227.0 39.0 o 2 4 10 -1 46.0 -9.0 27.0 < 3 4 10 -2 96.0 133.0 37.0 o 3 4 10 -1 315.0 241.0 43.0 o 3 4 10 0 672.0 755.0 172.0 o 4 4 10 -2 159.0 66.0 33.0 < 4 4 10 -1 199.0 146.0 31.0 o 5 4 10 -2 61.0 51.0 28.0 < 5 4 10 -1 163.0 178.0 40.0 o 6 4 10 -2 74.0 43.0 30.0 < 6 4 10 -1 196.0 117.0 35.0 o 7 4 10 -2 3.0 -73.0 33.0 < 7 4 10 -1 760.0 767.0 70.0 o 8 4 10 -2 6.0 101.0 38.0 < 8 4 10 -1 25.0 -59.0 35.0 < 9 4 10 -2 168.0 233.0 43.0 o 9 4 10 -1 402.0 220.0 42.0 o 10 4 10 -2 185.0 239.0 42.0 o 10 4 10 -1 31.0 33.0 48.0 < 11 4 10 -2 64.0 21.0 25.0 < 11 4 10 -1 62.0 -136.0 86.0 < 12 4 10 -2 335.0 364.0 49.0 o 13 4 10 -2 31.0 244.0 54.0 o 14 4 10 -2 52.0 38.0 36.0 < 15 4 10 -2 77.0 23.0 41.0 < 1 5 10 -2 56.0 104.0 55.0 < 2 5 10 -2 181.0 115.0 58.0 < 3 5 10 -2 8.0 -72.0 72.0 < 1 0 11 0 1034.0 1158.0 110.0 o 1 0 11 1 223.0 291.0 37.0 o 1 0 11 2 3.0 20.0 20.0 < 2 0 11 0 3934.0 3989.0 180.0 o 2 0 11 1 58.0 36.0 20.0 < 2 0 11 2 0.0 -6.0 21.0 < 3 0 11 0 6296.0 6548.0 231.0 o 3 0 11 1 45.0 37.0 20.0 < 3 0 11 2 1.0 25.0 21.0 < 4 0 11 0 10658.0 10716.0 297.0 o 4 0 11 1 16.0 12.0 21.0 < 4 0 11 2 309.0 271.0 38.0 o 5 0 11 0 689.0 816.0 86.0 o 5 0 11 1 89.0 100.0 26.0 o 5 0 11 2 1620.0 1736.0 89.0 o 6 0 11 0 100806.0 99009.0 916.0 o 6 0 11 1 383.0 314.0 37.0 o 6 0 11 2 439.0 414.0 51.0 o 7 0 11 0 7210.0 6848.0 243.0 o 7 0 11 1 91.0 59.0 22.0 < 7 0 11 2 482.0 609.0 53.0 o 8 0 11 0 3712.0 3318.0 168.0 o 8 0 11 1 5.0 26.0 26.0 < 8 0 11 2 301.0 318.0 37.0 o 9 0 11 0 4046.0 4023.0 215.0 o 9 0 11 1 61.0 58.0 27.0 < 9 0 11 2 353.0 365.0 45.0 o 10 0 11 0 624.0 662.0 88.0 o 10 0 11 1 2359.0 2105.0 101.0 o 10 0 11 2 25.0 16.0 24.0 < 11 0 11 0 5279.0 5116.0 241.0 o 11 0 11 1 1500.0 1581.0 88.0 o 11 0 11 2 11.0 84.0 29.0 < 12 0 11 0 218.0 226.0 51.0 o 12 0 11 1 1988.0 1972.0 97.0 o 12 0 11 2 14.0 29.0 27.0 < 13 0 11 0 118.0 81.0 39.0 < 13 0 11 1 463.0 386.0 48.0 o 13 0 11 2 80.0 114.0 35.0 o 14 0 11 0 7080.0 6075.0 260.0 o 14 0 11 1 516.0 466.0 54.0 o 14 0 11 2 144.0 141.0 32.0 o 15 0 11 0 6148.0 5906.0 259.0 o 15 0 11 1 52.0 91.0 32.0 < 15 0 11 2 148.0 171.0 47.0 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21.0 < 4 1 11 -1 609.0 495.0 44.0 o 4 1 11 0 23482.0 24031.0 301.0 o 4 1 11 1 133.0 174.0 28.0 o 4 1 11 2 22.0 592.0 63.0 o 5 1 11 -2 1181.0 1047.0 69.0 o 5 1 11 -1 73.0 124.0 27.0 o 5 1 11 0 21292.0 22981.0 311.0 o 5 1 11 1 64.0 132.0 27.0 o 5 1 11 2 483.0 457.0 45.0 o 6 1 11 -2 86.0 335.0 51.0 o 6 1 11 -1 3.0 -32.0 24.0 < 6 1 11 0 21584.0 22615.0 310.0 o 6 1 11 1 11.0 15.0 26.0 < 6 1 11 2 132.0 903.0 72.0 o 7 1 11 -2 248.0 210.0 37.0 o 7 1 11 -1 17.0 20.0 25.0 < 7 1 11 0 158.0 260.0 36.0 o 7 1 11 1 2.0 74.0 26.0 < 7 1 11 2 285.0 318.0 43.0 o 8 1 11 -2 244.0 172.0 34.0 o 8 1 11 -1 5.0 -45.0 28.0 < 8 1 11 0 245.0 376.0 41.0 o 8 1 11 1 8.0 60.0 25.0 < 8 1 11 2 196.0 251.0 33.0 o 9 1 11 -2 124.0 83.0 24.0 o 9 1 11 -1 29.0 26.0 25.0 < 9 1 11 0 1069.0 1127.0 75.0 o 9 1 11 1 23.0 28.0 21.0 < 9 1 11 2 37.0 53.0 31.0 < 10 1 11 -2 52.0 27.0 27.0 < 10 1 11 -1 512.0 494.0 52.0 o 10 1 11 0 706.0 685.0 57.0 o 10 1 11 1 1972.0 2029.0 94.0 o 10 1 11 2 36.0 32.0 26.0 < 11 1 11 -2 185.0 246.0 43.0 o 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5 3 11 -2 952.0 947.0 58.0 o 5 3 11 -1 34.0 59.0 27.0 < 5 3 11 0 8892.0 9155.0 246.0 o 6 3 11 -2 45.0 191.0 43.0 o 6 3 11 -1 0.0 39.0 25.0 < 6 3 11 0 10419.0 10487.0 243.0 o 7 3 11 -2 209.0 293.0 38.0 o 7 3 11 -1 32.0 9.0 26.0 < 7 3 11 0 45.0 40.0 39.0 < 8 3 11 -2 146.0 117.0 26.0 o 8 3 11 -1 11.0 15.0 24.0 < 8 3 11 0 141.0 74.0 38.0 < 9 3 11 -2 86.0 101.0 26.0 o 9 3 11 -1 19.0 3.0 27.0 < 9 3 11 0 429.0 457.0 55.0 o 10 3 11 -2 27.0 74.0 25.0 < 10 3 11 -1 20.0 10.0 25.0 < 10 3 11 0 314.0 144.0 38.0 o 11 3 11 -2 121.0 192.0 37.0 o 11 3 11 -1 167.0 175.0 32.0 o 11 3 11 0 1230.0 1314.0 150.0 o 12 3 11 -2 50.0 103.0 27.0 o 12 3 11 -1 897.0 895.0 67.0 o 13 3 11 -2 77.0 136.0 34.0 o 13 3 11 -1 33.0 101.0 32.0 o 14 3 11 -2 11.0 92.0 38.0 < 14 3 11 -1 126.0 57.0 34.0 < 15 3 11 -2 521.0 570.0 67.0 o 15 3 11 -1 1.0 -51.0 38.0 < 16 3 11 -2 307.0 307.0 58.0 o 17 3 11 -2 84.0 172.0 47.0 o 18 3 11 -2 3.0 -158.0 127.0 < 1 4 11 -2 1.0 -19.0 30.0 < 1 4 11 -1 50.0 72.0 48.0 < 2 4 11 -2 0.0 -72.0 30.0 < 2 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448.0 397.0 44.0 o 7 0 12 2 9.0 45.0 27.0 < 8 0 12 0 19937.0 19607.0 466.0 o 8 0 12 1 346.0 442.0 49.0 o 8 0 12 2 29.0 24.0 18.0 < 9 0 12 0 9634.0 9530.0 327.0 o 9 0 12 1 493.0 550.0 55.0 o 9 0 12 2 0.0 49.0 32.0 < 10 0 12 0 7487.0 7668.0 292.0 o 10 0 12 1 4.0 -16.0 24.0 < 10 0 12 2 1.0 46.0 27.0 < 11 0 12 0 672.0 606.0 82.0 o 11 0 12 1 18.0 0.0 28.0 < 11 0 12 2 20.0 4.0 29.0 < 12 0 12 0 5132.0 4824.0 233.0 o 12 0 12 1 24.0 27.0 25.0 < 12 0 12 2 301.0 702.0 62.0 o 13 0 12 0 14820.0 13714.0 394.0 o 13 0 12 1 10.0 14.0 26.0 < 13 0 12 2 64.0 50.0 27.0 < 14 0 12 0 4312.0 4072.0 216.0 o 14 0 12 1 892.0 757.0 65.0 o 14 0 12 2 765.0 842.0 68.0 o 15 0 12 0 2890.0 2601.0 175.0 o 15 0 12 1 176.0 143.0 34.0 o 15 0 12 2 41.0 143.0 54.0 < 16 0 12 0 179.0 195.0 63.0 o 16 0 12 1 81.0 66.0 28.0 < 16 0 12 2 237.0 151.0 53.0 < 17 0 12 1 352.0 249.0 113.0 < 17 0 12 2 93.0 37.0 49.0 < 1 1 12 -2 3.0 14.0 24.0 < 1 1 12 -1 13.0 16.0 19.0 < 1 1 12 0 187.0 262.0 40.0 o 1 1 12 1 9.0 55.0 27.0 < 1 1 12 2 7.0 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< 1 3 12 -2 0.0 34.0 29.0 < 1 3 12 -1 29.0 31.0 25.0 < 1 3 12 0 108.0 51.0 57.0 < 2 3 12 -2 10.0 71.0 25.0 < 2 3 12 -1 6.0 3.0 22.0 < 2 3 12 0 14565.0 15505.0 592.0 o 3 3 12 -2 52.0 107.0 31.0 o 3 3 12 -1 11.0 8.0 27.0 < 3 3 12 0 14813.0 15342.0 588.0 o 4 3 12 -2 123.0 189.0 33.0 o 4 3 12 -1 195.0 176.0 38.0 o 4 3 12 0 1112.0 825.0 128.0 o 5 3 12 -2 56.0 145.0 33.0 o 5 3 12 -1 5.0 9.0 30.0 < 5 3 12 0 247.0 108.0 42.0 < 6 3 12 -2 269.0 301.0 41.0 o 6 3 12 -1 268.0 250.0 37.0 o 6 3 12 0 226.0 227.0 114.0 < 7 3 12 -2 53.0 1062.0 69.0 o 7 3 12 -1 971.0 937.0 63.0 o 8 3 12 -2 937.0 1204.0 75.0 o 8 3 12 -1 349.0 466.0 45.0 o 9 3 12 -2 353.0 558.0 55.0 o 9 3 12 -1 5.0 26.0 26.0 < 10 3 12 -2 116.0 149.0 39.0 o 10 3 12 -1 141.0 133.0 35.0 o 11 3 12 -2 2.0 47.0 25.0 < 11 3 12 -1 133.0 178.0 63.0 < 12 3 12 -2 28.0 73.0 32.0 < 13 3 12 -2 48.0 87.0 34.0 < 14 3 12 -2 166.0 258.0 72.0 o 0 4 12 -2 282.0 200.0 96.0 < 1 4 12 -2 142.0 139.0 63.0 < 2 4 12 -2 458.0 553.0 121.0 o 3 4 12 -2 73.0 130.0 63.0 < 4 4 12 -2 20.0 19.0 81.0 < 5 4 12 -2 1.0 -50.0 45.0 < 6 4 12 -2 4.0 -13.0 63.0 < 7 4 12 -2 1.0 12.0 73.0 < 1 0 13 0 25587.0 27391.0 522.0 o 1 0 13 1 83.0 76.0 29.0 < 1 0 13 2 10.0 -3.0 25.0 < 2 0 13 0 9969.0 10620.0 325.0 o 2 0 13 1 34.0 97.0 34.0 < 2 0 13 2 13.0 23.0 30.0 < 3 0 13 0 3.0 -27.0 30.0 < 3 0 13 1 540.0 632.0 63.0 o 3 0 13 2 80.0 88.0 29.0 o 4 0 13 0 553.0 582.0 75.0 o 4 0 13 1 1360.0 1310.0 88.0 o 4 0 13 2 8.0 37.0 30.0 < 5 0 13 0 2566.0 2697.0 193.0 o 5 0 13 1 1202.0 1257.0 76.0 o 5 0 13 2 205.0 225.0 37.0 o 6 0 13 0 96.0 102.0 44.0 < 6 0 13 1 581.0 648.0 55.0 o 6 0 13 2 15.0 40.0 21.0 < 7 0 13 0 3257.0 3185.0 183.0 o 7 0 13 1 43.0 49.0 22.0 < 7 0 13 2 436.0 507.0 48.0 o 8 0 13 0 432.0 566.0 78.0 o 8 0 13 1 287.0 335.0 40.0 o 8 0 13 2 2.0 45.0 28.0 < 9 0 13 0 478.0 539.0 78.0 o 9 0 13 1 173.0 116.0 29.0 o 9 0 13 2 294.0 446.0 50.0 o 10 0 13 0 758.0 749.0 92.0 o 10 0 13 1 61.0 38.0 24.0 < 10 0 13 2 347.0 375.0 48.0 o 11 0 13 0 3299.0 2849.0 183.0 o 11 0 13 1 16.0 37.0 29.0 < 11 0 13 2 267.0 664.0 62.0 o 12 0 13 0 11815.0 10847.0 356.0 o 12 0 13 1 27.0 18.0 27.0 < 12 0 13 2 637.0 538.0 76.0 o 13 0 13 0 2738.0 3102.0 272.0 o 13 0 13 1 154.0 128.0 43.0 < 13 0 13 2 0.0 -35.0 33.0 < 0 1 13 -2 1261.0 1084.0 105.0 o 0 1 13 -1 11.0 20.0 42.0 < 0 1 13 0 1474.0 1708.0 154.0 o 0 1 13 1 36.0 47.0 37.0 < 0 1 13 2 1320.0 1146.0 121.0 o 1 1 13 -2 622.0 768.0 68.0 o 1 1 13 -1 129.0 71.0 27.0 < 1 1 13 0 1011.0 1125.0 81.0 o 1 1 13 1 185.0 185.0 35.0 o 1 1 13 2 350.0 458.0 68.0 o 2 1 13 -2 170.0 193.0 36.0 o 2 1 13 -1 5.0 -13.0 28.0 < 2 1 13 0 2046.0 2202.0 114.0 o 2 1 13 1 128.0 134.0 31.0 o 2 1 13 2 114.0 169.0 47.0 o 3 1 13 -2 100.0 155.0 26.0 o 3 1 13 -1 110.0 95.0 31.0 o 3 1 13 0 426.0 532.0 58.0 o 3 1 13 1 160.0 192.0 33.0 o 3 1 13 2 141.0 207.0 37.0 o 4 1 13 -2 174.0 120.0 36.0 o 4 1 13 -1 16.0 51.0 30.0 < 4 1 13 0 3588.0 3952.0 155.0 o 4 1 13 1 117.0 226.0 43.0 o 4 1 13 2 159.0 196.0 37.0 o 5 1 13 -2 28.0 47.0 24.0 < 5 1 13 -1 595.0 620.0 57.0 o 5 1 13 0 2247.0 2491.0 107.0 o 5 1 13 1 258.0 414.0 52.0 o 5 1 13 2 25.0 67.0 36.0 < 6 1 13 -2 69.0 29.0 24.0 < 6 1 13 -1 201.0 164.0 29.0 o 6 1 13 0 1674.0 1812.0 92.0 o 6 1 13 1 463.0 452.0 48.0 o 6 1 13 2 77.0 44.0 31.0 < 7 1 13 -2 1.0 -19.0 28.0 < 7 1 13 -1 771.0 660.0 53.0 o 7 1 13 0 756.0 722.0 58.0 o 7 1 13 1 196.0 217.0 34.0 o 7 1 13 2 1.0 58.0 46.0 < 8 1 13 -2 50.0 38.0 28.0 < 8 1 13 -1 210.0 236.0 33.0 o 8 1 13 0 476.0 482.0 46.0 o 8 1 13 1 307.0 377.0 40.0 o 9 1 13 -2 4.0 -7.0 25.0 < 9 1 13 -1 42.0 124.0 31.0 o 9 1 13 0 10789.0 10619.0 216.0 o 9 1 13 1 40.0 73.0 27.0 < 10 1 13 -2 158.0 109.0 29.0 o 10 1 13 -1 20.0 32.0 30.0 < 10 1 13 0 2102.0 2327.0 103.0 o 10 1 13 1 27.0 42.0 27.0 < 11 1 13 -2 34.0 153.0 44.0 o 11 1 13 -1 232.0 154.0 37.0 o 11 1 13 0 13839.0 13613.0 246.0 o 11 1 13 1 153.0 193.0 36.0 o 12 1 13 -2 28.0 42.0 37.0 < 12 1 13 -1 22.0 -3.0 27.0 < 12 1 13 0 7349.0 7431.0 214.0 o 12 1 13 1 12.0 55.0 60.0 < 13 1 13 -2 576.0 510.0 113.0 o 13 1 13 -1 32.0 34.0 38.0 < 13 1 13 0 1926.0 2010.0 204.0 o 1 2 13 -2 5.0 39.0 27.0 < 1 2 13 -1 134.0 169.0 36.0 o 1 2 13 0 17729.0 19825.0 335.0 o 2 2 13 -2 16.0 19.0 27.0 < 2 2 13 -1 21.0 9.0 26.0 < 2 2 13 0 7608.0 8758.0 223.0 o 3 2 13 -2 43.0 114.0 30.0 o 3 2 13 -1 550.0 779.0 64.0 o 3 2 13 0 23.0 49.0 35.0 < 4 2 13 -2 7.0 37.0 27.0 < 4 2 13 -1 959.0 1221.0 74.0 o 4 2 13 0 384.0 454.0 46.0 o 5 2 13 -2 173.0 233.0 36.0 o 5 2 13 -1 1900.0 2064.0 96.0 o 5 2 13 0 1964.0 2381.0 111.0 o 6 2 13 -2 29.0 57.0 24.0 < 6 2 13 -1 137.0 219.0 36.0 o 6 2 13 0 78.0 95.0 28.0 o 7 2 13 -2 444.0 477.0 49.0 o 7 2 13 -1 27.0 20.0 27.0 < 7 2 13 0 2221.0 2658.0 130.0 o 8 2 13 -2 4.0 28.0 23.0 < 8 2 13 -1 687.0 659.0 55.0 o 8 2 13 0 317.0 559.0 77.0 o 9 2 13 -2 426.0 611.0 60.0 o 9 2 13 -1 31.0 81.0 28.0 < 10 2 13 -2 289.0 261.0 37.0 o 10 2 13 -1 14.0 44.0 25.0 < 11 2 13 -2 237.0 265.0 42.0 o 11 2 13 -1 4.0 7.0 27.0 < 12 2 13 -2 532.0 424.0 61.0 o 12 2 13 -1 5.0 58.0 41.0 < 13 2 13 -2 0.0 6.0 34.0 < 0 3 13 -2 802.0 692.0 95.0 o 1 3 13 -2 455.0 697.0 69.0 o 2 3 13 -2 143.0 207.0 39.0 o 3 3 13 -2 42.0 73.0 28.0 < 4 3 13 -2 99.0 135.0 33.0 o 5 3 13 -2 17.0 73.0 27.0 < 6 3 13 -2 35.0 60.0 27.0 < 7 3 13 -2 1.0 13.0 42.0 < 8 3 13 -2 28.0 76.0 34.0 < 9 3 13 -2 8.0 -5.0 41.0 < 10 3 13 -2 70.0 83.0 74.0 < 0 0 14 0 1961.0 2190.0 207.0 o 0 0 14 1 118.0 103.0 44.0 < 0 0 14 2 60.0 38.0 33.0 < 1 0 14 0 52.0 27.0 34.0 < 1 0 14 1 115.0 96.0 26.0 o 1 0 14 2 19.0 -10.0 27.0 < 2 0 14 0 371.0 471.0 70.0 o 2 0 14 1 562.0 481.0 57.0 o 2 0 14 2 32.0 29.0 30.0 < 3 0 14 0 3547.0 3729.0 228.0 o 3 0 14 1 9.0 2.0 26.0 < 3 0 14 2 102.0 51.0 36.0 < 4 0 14 0 45.0 -15.0 34.0 < 4 0 14 1 19.0 44.0 27.0 < 4 0 14 2 1203.0 1331.0 122.0 o 5 0 14 0 1395.0 1389.0 140.0 o 5 0 14 1 34.0 5.0 21.0 < 5 0 14 2 303.0 394.0 71.0 o 6 0 14 0 11130.0 11780.0 412.0 o 6 0 14 1 46.0 10.0 30.0 < 6 0 14 2 87.0 108.0 56.0 < 7 0 14 0 10099.0 12165.0 718.0 o 7 0 14 1 45.0 75.0 35.0 < 7 0 14 2 5.0 154.0 56.0 < 8 0 14 0 8115.0 7461.0 386.0 o 8 0 14 1 2.0 -33.0 47.0 < 8 0 14 2 141.0 141.0 74.0 < 9 0 14 0 439.0 281.0 108.0 < 9 0 14 1 239.0 150.0 58.0 < 1 1 14 -2 5.0 -14.0 20.0 < 1 1 14 -1 1872.0 2119.0 121.0 o 1 1 14 0 415.0 327.0 46.0 o 1 1 14 1 2438.0 2877.0 192.0 o 2 1 14 -2 51.0 75.0 26.0 < 2 1 14 -1 272.0 198.0 34.0 o 2 1 14 0 1375.0 1447.0 101.0 o 2 1 14 1 792.0 674.0 92.0 o 3 1 14 -2 36.0 44.0 32.0 < 3 1 14 -1 129.0 104.0 32.0 o 3 1 14 0 5905.0 5907.0 206.0 o 3 1 14 1 163.0 210.0 57.0 o 4 1 14 -2 415.0 444.0 55.0 o 4 1 14 -1 9.0 -5.0 27.0 < 4 1 14 0 11625.0 12254.0 367.0 o 4 1 14 1 52.0 87.0 37.0 < 5 1 14 -2 37.0 43.0 28.0 < 5 1 14 -1 203.0 156.0 30.0 o 5 1 14 0 13711.0 15105.0 394.0 o 5 1 14 1 94.0 23.0 46.0 < 6 1 14 -2 463.0 626.0 72.0 o 6 1 14 -1 22.0 72.0 35.0 < 6 1 14 0 9246.0 10834.0 384.0 o 7 1 14 -2 275.0 325.0 91.0 o 7 1 14 -1 1.0 27.0 36.0 < 7 1 14 0 8587.0 8617.0 254.0 o 8 1 14 -2 6.0 167.0 76.0 < 8 1 14 -1 132.0 55.0 57.0 < 8 1 14 0 39.0 -7.0 45.0 < 9 1 14 -2 36.0 -46.0 44.0 < 9 1 14 -1 37.0 81.0 52.0 < 9 1 14 0 3.0 -63.0 47.0 < 0 2 14 -2 70.0 93.0 39.0 < 0 2 14 -1 76.0 81.0 55.0 < 1 2 14 -2 3.0 -40.0 29.0 < 1 2 14 -1 227.0 148.0 55.0 < 2 2 14 -2 72.0 63.0 28.0 < 2 2 14 -1 454.0 454.0 79.0 o 3 2 14 -2 85.0 65.0 28.0 < 3 2 14 -1 4.0 -75.0 39.0 < 4 2 14 -2 1066.0 1204.0 106.0 o 4 2 14 -1 7.0 -55.0 35.0 < 5 2 14 -2 424.0 388.0 69.0 o 5 2 14 -1 54.0 31.0 43.0 < 6 2 14 -2 45.0 75.0 38.0 < 6 2 14 -1 8.0 -27.0 39.0 < 7 2 14 -2 3.0 110.0 48.0 < 8 2 14 -2 123.0 154.0 47.0 o 9 2 14 -2 6.0 40.0 52.0 <